热等静压温度对雾化合金粉制备的9Cr-ODS钢组织和性能的影响

doi:10.11896/cldb.19090133

材料导报

2021, Vol. 35

Issue (8): 8169-8178 https://doi.org/10.11896/cldb.19090133

金属与金属基复合材料

热等静压温度对雾化合金粉制备的9Cr-ODS钢组织和性能的影响

谢锐¹, 吕铮², 徐长伟¹, 刘春明²

1 沈阳建筑大学材料科学与工程学院,沈阳 110168
2 东北大学材料科学与工程学院,材料各向异性与织构教育部重点实验室,沈阳 110819

The Effects of Hot Isostatic Pressing Temperature on Microstructures and Properties of 9Cr-ODS Steels Produced by Atomization Alloy Powder

XIE Rui¹, LYU Zheng², XU Changwei¹, LIU Chunming²

1 School of Material Science and Engineering, Shenyang Jianzhu University, Shenyang 110168, China
2 Key Laboratory for Anisotropy and Texture of Materials (Ministry of Education), School of Material Science and Engineering, Northeastern University, Shenyang 110819, China

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摘要本实验以雾化合金粉制备的9Cr-ODS钢为研究对象,首先利用激光粒度仪、XRD、SEM、EDS等实验手段研究氧化物弥散强化钢雾化合金粉的球磨工艺,再利用EBSD、HAADF、SAXS等实验方法研究热等静压温度对雾化合金粉制备的9Cr-ODS钢的微观结构和力学性能的影响。实验结果表明雾化合金粉经过8 h球磨可以符合制备ODS钢的各项要求。900 ℃、1 100 ℃、1 200 ℃热等静压成型的9Cr-ODS钢的晶粒尺寸分别为0.36 μm、0.94 μm和1.66 μm。小角度X射线散射结果表明,在900 ℃、1 100 ℃和1 200 ℃ HIP成型的样品中,富Y、Ti、O析出相的分布密度最高值分别为3.94×10²² /m³、1.03×10²² /m³和8.66×10²¹ /m³。雾化合金粉制备的9Cr-ODS钢中的富Al、Ti、Cr氧化物相的分布密度随着热等静压温度的升高而降低。在雾化合金粉制备的ODS钢样品中均发现了富Y、Ti、O纳米析出相,且成型温度越高,富Y、Ti、O纳米析出相的分布密度越低。900 ℃热等静压成型样品的力学性能较为优异,成型温度升高,样品的力学性能逐渐下降。

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关键词: 雾化合金粉氧化物弥散强化钢球磨热等静压温度

Abstract: In this paper 9Cr-ODS steels produced by atomization alloy powders were studied. The milling technology of atomization alloy powders were studied firstly by laser particle size analyzer, XRD, SEM, EDS and so on. The EBSD, TEM, HAADF and SAXS were applied to study the effect of hot isostatic pressing temperatures on the microstructure and mechanical properties of 9Cr-ODS steels. The experiment data show that the alloy powder can meet the requirements of preparing ODS steels after 8 h ball milling. The grain sizes of atomization alloy powders 9Cr-ODS steels hot isostatic pressing at 900 ℃, 1 100 ℃ and 1 200 ℃ are 0.36 μm, 0.94 μm and 1.66 μm, respectively. The small angle X-ray scattering results show that the distribution densities of Y, Ti, O enrich nano-precipitates in the 9Cr-ODS steels produced by atomization alloy powders are 3.94×10²²/m³, 1.03×10²²/m³ and 8.66×10²¹/m³. The distribution densities of Al, Ti, Cr oxides decrease as hot isostatic pressing temperatures rise. The Y, Ti, O enrich nano-precipitates are found in the 9Cr-ODS steels produced by atomization alloy powders. As the hot isostatic pressing temperatures rise, the distribution densities Y, Ti, O enrich nano-precipitates decreased. The sample of 9Cr-ODS steel hot isostatic pressing at 900 ℃ display excellent mechanical properties. The mechanical properties decrease as hot isostatic pressing temperature rise.

Key words: atomization alloy powder oxide dispersion strengthen ball milling HIP temperatures

出版日期: 2021-04-25 发布日期: 2021-05-10

ZTFLH:

TB31

基金资助: 国家自然科学基金/青年科学基金(51601031);辽宁省自然科学基金面上项目(2017540306)

通讯作者: xierui198479@126.com

作者简介: 谢锐,沈阳建筑大学讲师。2007年于沈阳建筑大学获得无机非金属材料工程学士学位,2010年9月至2015年7于东北大学获得材料学博士学位。博士毕业后继续在东北大学冶金工程博士后流动站工作。工作期限为2015年10月至2018年3月。2018年3月博士后出站到沈阳建筑大学任教工作。至今,已公开发表学术论文超过15篇,获得国家专利授权两项。研究领域主要围绕国家重点发展的先进金属材料、核反应堆用金属结构材料。同时,他的研究还获得了国家自然科学基金青年科学家基金项目、国家重大研发专项子课题、辽宁省自然科学基金等项目的支持。

引用本文:

谢锐, 吕铮, 徐长伟, 刘春明. 热等静压温度对雾化合金粉制备的9Cr-ODS钢组织和性能的影响[J]. 材料导报, 2021, 35(8): 8169-8178.
XIE Rui, LYU Zheng, XU Changwei, LIU Chunming. The Effects of Hot Isostatic Pressing Temperature on Microstructures and Properties of 9Cr-ODS Steels Produced by Atomization Alloy Powder. Materials Reports, 2021, 35(8): 8169-8178.

链接本文:

http://www.mater-rep.com/CN/10.11896/cldb.19090133 或 http://www.mater-rep.com/CN/Y2021/V35/I8/8169

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