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材料导报  2021, Vol. 35 Issue (6): 6035-6041    https://doi.org/10.11896/cldb.19120136
  无机非金属及其复合材料 |
氧化锆添加量对四氧化三铁基复合材料性能的影响
张莲芝, 吴张永, 王庭有, 朱启晨, 郭翠霞, 蔡晓明, 莫子勇
昆明理工大学机电工程学院,昆明 650500
The Influence of the Zirconia Content on the Properties of Ferroferric Oxide Matrix Composites
ZHANG Lianzhi, WU Zhangyong, WANG Tingyou, ZHU Qichen, GUO Cuixia, CAI Xiaoming, MO Ziyong
Faculty of Mechanical and Electrical Engineering, Kunming University of Science and Technology, Kunming 650500, China
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摘要 采用高能球磨法制备Fe3O4/ZrO2复合磁性颗粒,对复合磁性颗粒的包覆机理进行深入研究。通过XRD、FT-IR、VSM、SEM等测试手段对样品的结构、光学性质、磁性能和形貌等进行表征,并将各性能进行定性和定量分析。结果表明:当ZrO2含量为2.13%时,Fe3O4/ZrO2复合材料摩擦因数的波动最稳,其硬度达最大值10.01 GPa;此外,随着ZrO2含量的增加,样品的比饱和磁化强度和剩余磁化强度明显降低,复合磁性颗粒的粒径越来越大,并且出现ZrO2颗粒的团聚现象。对于表面活性剂,相比于PEG2000,CTAB能使Fe3O4/ZrO2复合磁性颗粒桥接更紧密、性能更好。因此,在表面活性剂CTAB的修饰下,ZrO2加入量为2.13%时,可使Fe3O4/ZrO2复合磁性颗粒有较好的综合性能。
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张莲芝
吴张永
王庭有
朱启晨
郭翠霞
蔡晓明
莫子勇
关键词:  复合材料  表面活性剂  磁性磨粒  复合加工  高精密加工    
Abstract: Fe3O4/ZrO2 magnetic composite particles were prepared by high-energy ball milling, the principles of coating of magnetic composite particles were deeply studied. The crystalline structures, light absorption properties, magnetic properties and morphologies of composite samples were characterized using XRD, FT-IR, VSM, SEM measurement, respectively, and the properties of composite samples were analysed qualitatively and quantitatively. The results showed that the friction factor was the most stable, and the hardness reached a maximum of 10.01 GPa with the Fe3O4/ZrO2 composites containing 2.13% ZrO2. In addition, with the increase of ZrO2 content, the specific saturation magnetization and the residual magnetization of the composites decreased significantly, larger magnetic composite particles were generated, and ZrO2 particles agglome-ration occurred. Compared to PEG2000, the Fe3O4/ZrO2 magnetic composite particles could be more tightly linked by CTAB, so that magnetic composite particles have better performance. Therefore, the best comprehensive performance is achieved with the Fe3O4/ZrO2 composites containing 2.13% ZrO2 and coated CTAB.
Key words:  composites    surfactant    magnetic abrasives    compound processing    high precision machining
               出版日期:  2021-03-25      发布日期:  2021-03-23
ZTFLH:  TB383  
基金资助: 国家自然科学基金(51165012)
通讯作者:  zhyongwu63@163.com   
作者简介:  张莲芝,博士研究生,研究方向为磁性复合材料的特种加工。以第一作者在国内外重要期刊发表文章6篇,申请发明专利3项。
吴张永,教授,主要研究方向为水基液压传动技术、电液数字控制技术,昆明理工大学机电工程学院功能流体应用与矿山机电工程研究所所长。主持及参与科研项目20余项,发表论文50余篇,获发明专利13项。
引用本文:    
张莲芝, 吴张永, 王庭有, 朱启晨, 郭翠霞, 蔡晓明, 莫子勇. 氧化锆添加量对四氧化三铁基复合材料性能的影响[J]. 材料导报, 2021, 35(6): 6035-6041.
ZHANG Lianzhi, WU Zhangyong, WANG Tingyou, ZHU Qichen, GUO Cuixia, CAI Xiaoming, MO Ziyong. The Influence of the Zirconia Content on the Properties of Ferroferric Oxide Matrix Composites. Materials Reports, 2021, 35(6): 6035-6041.
链接本文:  
http://www.mater-rep.com/CN/10.11896/cldb.19120136  或          http://www.mater-rep.com/CN/Y2021/V35/I6/6035
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