多尺度实验测试评价高强钢氢脆的研究进展

doi:10.11896/cldb.22110194

材料导报

2024, Vol. 38

Issue (10): 22110194-11 https://doi.org/10.11896/cldb.22110194

金属与金属基复合材料

多尺度实验测试评价高强钢氢脆的研究进展

周华生, 曹燕, 章小峰^*, 吴迪, 赵鑫磊, 邢梅, 林方敏, 江雅

安徽工业大学冶金工程学院,安徽马鞍山 243002

Research Progress of Studying Hydrogen Embrittlement in High-strength Steel by Multiscale Experiments and Evaluation Methods

ZHOU Huasheng, CAO Yan, ZHANG Xiaofeng^*, WU Di, ZHAO Xinlei, XING Mei, LIN Fangmin, JIANG Ya

School of Metallurgical Engineering, Anhui University of Technology, Ma’anshan 243002, Anhui, China

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摘要氢脆是高强钢中普遍存在的现象,也是其研发过程中必须攻克的难题。为了深入理解高强钢的氢脆与其缺陷之间的关系,发展了许多测试评价方法,如宏观尺度的慢应变速率拉伸、线性增加应力、恒载荷拉伸这类力学实验以及检测氢含量的热脱附光谱法和电化学氢渗透法,根据高强钢的塑性损失、最大断裂应力、断裂时间、应力强度因子、氢的俘获能和扩散速率等参数直接进行氢脆敏感性的评价。但宏观尺度的实验无法深入地研究高强钢发生氢脆的机理,通过介观、微观尺度的实验和表征手段,如压痕法、纳米压痕法、微悬臂梁弯曲实验、原子探针技术、氢微印技术、扫描开尔文探针显微镜等,从局部测试高强钢性能变化和准确检测氢被俘获的位置,能够在解释氢脆机理和认识氢与高强钢中缺陷之间相互作用的问题上提供更加准确的依据。本文介绍、对比了上述这些实验方法并调研了多尺度实验测试评价高强钢氢脆的研究进展,总结了高强钢氢脆研究现状和主流的测试评价方法,为深入探索高强钢氢脆提供了思路。

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	林方敏
	江雅

关键词: 高强钢氢脆多尺度缺陷多尺度实验

Abstract: Hydrogen embrittlement is both a common phenomenon in high-strength steel (HSS) and an urgent problem that must be solved inthe deve-lopment of HSS. To deeply study the relationship between hydrogen embrittlement and defects of HSS, researchers have developed many macroscale experiments and evaluation methods, such as slow strain rate tensile, linear increase stress, constant load tensile, thermal desorption spectroscopy, and electrochemical hydrogen permeation. These methods are directly used to evaluate the hydrogen embrittlement susceptibility of HSS, which accords with HSS’s parameters like plastic loss, maximum fracture stress, fracture time, stress intensity factor, hydrogen capture energy, and diffusion rate. However, these macroscale experiments cannot accurately explain the causes of HSS’s hydrogen embrittlement in depth. Therefore, researchers have also developed some mesoscale and microscale experiments to locally test changes in HSS’s pro-perties and accurately detect the position where the hydrogen atom was captured. These mesoscale and microscale experiments and characte-rization means include the indentation method, nanoindentation method, micro cantilever bending experiment, atomic probe technology, hydrogen micro-printing technology, scanning Kelvin probe microscope, and so on, which provide a more accurate basis for explaining the mechanism of hydrogen embrittlement and understanding the interaction between hydrogen and HSS’s defects. In this paper, we introduce and compare the above experiments, investigate the research progress of multiscale test evaluation of HSS’s hydrogen embrittlement. Then, we summarize the current research status and mainstream test evaluation methods of HSS’s hydrogen embrittlement so that we provide some ideas on how to use these experiments to further explore HSS’s hydrogen embrittlement.

Key words: high-strength steel hydrogen embrittlement multiscale defects multiscale experiments

出版日期: 2024-05-25 发布日期: 2024-05-28

ZTFLH:

TG111.91

基金资助: 安徽省自然科学基金面上项目(2108085ME143);安徽省高校自然科学基金重大项目(KJ2021ZD0045)

通讯作者: *章小峰,安徽工业大学冶金工程学院副教授。1998年本科毕业于武汉科技大学,2008年7月在华中科技大学材料加工工程专业取得博士学位,同年8月到安徽工业大学任职。任职期间,于2013—2016年在南京理工大学进行博士后研究工作。主要从事先进汽车用钢材料组织性能控制方面的研究工作。近年来,在先进钢铁材料领域发表论文50余篇。egzxf@ahut.edu.cn

作者简介: 周华生,2021年7月于安徽工业大学获得工学学士学位。现为安徽工业大学冶金工程学院材料与化工专业硕士研究生,在章小峰和曹燕两位老师的指导下进行研究。主要从事高强钢氢脆领域的相关研究。

引用本文:

周华生, 曹燕, 章小峰, 吴迪, 赵鑫磊, 邢梅, 林方敏, 江雅. 多尺度实验测试评价高强钢氢脆的研究进展[J]. 材料导报, 2024, 38(10): 22110194-11.
ZHOU Huasheng, CAO Yan, ZHANG Xiaofeng, WU Di, ZHAO Xinlei, XING Mei, LIN Fangmin, JIANG Ya. Research Progress of Studying Hydrogen Embrittlement in High-strength Steel by Multiscale Experiments and Evaluation Methods. Materials Reports, 2024, 38(10): 22110194-11.

链接本文:

http://www.mater-rep.com/CN/10.11896/cldb.22110194 或 http://www.mater-rep.com/CN/Y2024/V38/I10/22110194

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