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材料导报  2023, Vol. 37 Issue (11): 21060160-9    https://doi.org/10.11896/cldb.21060160
  无机非金属及其复合材料 |
硅基陶瓷前驱体用于耐高温连接材料研究进展
陈楚童1,2, 罗永明1, 徐彩虹1,2
1 中国科学院化学研究所,中国科学院极端环境高分子材料重点实验室,北京 100190
2 中国科学院大学化学与化工学院,北京 100049
Research Progress of Silicon-based Ceramic Precursors for High-temperature Connection Materials
CHEN Chutong1,2, LUO Yongming1, XU Caihong1,2
1 CAS Key Laboratory of Science and Technology on High-tech Polymer Materials, Chinese Academy of Sciences Institute of Chemistry, Beijing 100190,China
2 School of Chemistry and Chemical Engineering, University of Chinese Academy of Sciences, Beijing 100049,China
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摘要 硅基陶瓷前驱体聚合物具有与一般高分子聚合物相似的加工工艺特性,并可在高温下转化为陶瓷材料,在航空航天等领域有着广泛的应用。与传统的机械连接、焊接等连接技术相比,硅基陶瓷前驱体应用于耐高温连接材料具有工艺简单、应力分布均匀、连接温度低等优势。陶瓷前驱体用于连接材料可分为两种情况:经固化及高温热解处理后再使用的连接材料称为耐高温连接剂;固化后不经热解而直接使用的连接材料称为耐高温胶粘剂。本文对包括聚碳硅烷、聚硅氮烷和聚硅氧烷在内的硅基陶瓷前驱体用作耐高温连接剂和耐高温胶粘剂的研究进展分别进行了概括总结,并对其优缺点进行了分析,最后指出了硅基陶瓷前驱体用于耐高温连接材料研究仍存在的问题和今后的发展方向。
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陈楚童
罗永明
徐彩虹
关键词:  耐高温  胶粘剂  连接剂  陶瓷前驱体  硅基聚合物    
Abstract: Silicon-based ceramic precursors have similar processing characteristics to common polymers and can be transformed into ceramic materials at high temperature, which have a broad application in aerospace and other fields. Compared with traditional mechanical connection, such as welding and other connection technologies, the use of silicon-based ceramic precursors as jointing materials has advantages of simple process, uniform stress distribution, and low connection temperature. Ceramic precursors as jointing material can be categorized as either high temperature resistant joint agents or adhesives. The former undergoes curing and high temperature heat treatment before use, while the latter is directly used after curation. This paper summarizes the research progress of silicon-based ceramic precursors including polycarbosilane, polysilazane and polysiloxane as high temperature resistant joint agents or adhesives, and analyzes their advantages and shortcomings. We also suggest the unsolved issues and future research direction in the field of silicon-based ceramic precursors for high-temperature connection materials.
Key words:  high-temperature resistance    adhesive    joint agent    ceramic precursor    silicon-based polymer
出版日期:  2023-06-10      发布日期:  2023-06-19
ZTFLH:  TQ174.75  
基金资助: 山东省重大科技创新工程(2019JZZY010316);山东省自然科学基金氟硅材料联合基金(ZR2020LFG012)
通讯作者:  罗永明,通信作者,中国科学院化学研究所副研究员。1995年本科毕业于北京科技大学,1998年在北京科技大学取得硕士学位。2001年在清华大学取得博士学位。主要从事陶瓷前驱体的应用工艺与材料性能的研究。
徐彩虹,通信作者,中国科学院化学研究所研究员、博士研究生导师。1990年7月本科毕业于长春地质学院,1997年7月在山东大学高分子化学与物理专业取得硕士学位,2001年7月在中国科学院化学研究所高分子化学与物理专业取得博士学位。2001—2002年在日本京都大学化学研究所进行博士后研究。2005年入选中科院“百人计划”。主要从事含硅聚合物新材料的设计、合成及应用研究。   
作者简介:  陈楚童,2019年毕业于北京化工大学,获得工学学士学位。现为中国科学院化学研究所硕士研究生,在徐彩虹研究员的指导下进行研究。目前主要研究方向为有机硅高分子。
引用本文:    
陈楚童, 罗永明, 徐彩虹. 硅基陶瓷前驱体用于耐高温连接材料研究进展[J]. 材料导报, 2023, 37(11): 21060160-9.
CHEN Chutong, LUO Yongming, XU Caihong. Research Progress of Silicon-based Ceramic Precursors for High-temperature Connection Materials. Materials Reports, 2023, 37(11): 21060160-9.
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http://www.mater-rep.com/CN/10.11896/cldb.21060160  或          http://www.mater-rep.com/CN/Y2023/V37/I11/21060160
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