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材料导报  2022, Vol. 36 Issue (19): 20110267-8    https://doi.org/10.11896/cldb.20110267
  金属与金属基复合材料 |
ODS钢在热加工过程中纳米氧化物演化行为的研究进展
汪建强1,2,3, 徐斌1,3, 谢碧君1,3, 张健杨1,3, 孙明月1,3
1 中国科学院金属研究所核材料与安全评价重点实验室,沈阳 110016
2 中国科学技术大学材料科学与工程学院,合肥 230026
3 中国科学院金属研究所材料科学沈阳国家实验室,沈阳 110016
Nano-oxides Evolvement in ODS Steel During Thermo-Mechanical Processing: a Review
WANG Jianqiang1,2,3, XU Bin1,3, XIE Bijun1,3, ZHANG Jianyang1,3, SUN Mingyue1,3
1 Key Laboratory of Nuclear Materials and Safety Assessment, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, China
2 School of Materials Science and Engineering, University of Science and Technology of China, Hefei 230026, China
3 Shenyang National Laboratory for Materials Science, Institute of Metal Research, Chinese Academy of Sciences, Shenyang 110016, China
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摘要 与第二、三代核能系统相比,第四代核能系统和核聚变堆的运行温度更高、辐照剂量更强以及腐蚀环境更为严苛,因此开发高性能核电材料迫在眉睫。氧化物弥散强化(Oxide dispersion strengthened, ODS)钢含有高密度的弥散纳米氧化物和空位尾闾,使其具有优异的抗高温蠕变和抗辐照肿胀的性能,因此被认为是第四代核裂变堆包壳管和核聚变堆包层结构最有前景的候选材料之一。
ODS钢优异的性能源于其独特的微观组织结构,尤其是弥散分布的纳米氧化物。在热变形过程中,纳米氧化物形态变化不大,但在冷变形过程中,纳米氧化物会发生明显的塑性变形,后续的高温退火处理使其溶解再析出。合理调控合金元素可以提高纳米氧化物的稳定性和减小纳米氧化物尺寸,但晶界与纳米氧化物的相互作用会使纳米氧化物丧失界面关系而加速粗化,并且在晶界附近区域会出现无析出区。由于ODS钢中纳米氧化物的演化行为复杂,调控纳米氧化物的尺寸和弥散分布程度仍有待进一步研究。
本文归纳了ODS钢在热加工过程中纳米氧化物演化行为的研究进展,分别对纳米氧化物的塑性变形机制、纳米氧化物的溶解再析出机制、纳米氧化物的热稳定性和纳米氧化物与晶界的相互作用进行了总结及分析,并对存在的问题进行了总结和展望,以期为ODS钢在第四代核能系统包壳管和核聚变堆包层结构中的应用提供参考。
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汪建强
徐斌
谢碧君
张健杨
孙明月
关键词:  ODS钢  纳米氧化物  演变机制  塑性变形  稳定性    
Abstract: Compared to the second and third generation nuclear power systems, the fourth generation nuclear systems and fusion reactors have higher operating temperature and irradiation dose, and harsher chemical corrosion environment. The development of high-performance nuclear power materials is one of the key factors to promote the development of nuclear energy. Oxide dispersion strengthened (ODS) steel contains high-density dispersed nano-oxides and vacancy sinks, exhibiting excellent high-temperature creep performance and irradiation swelling resistance. Therefore, ODS steel has been considered as one of the most promising materials for fourth-generation nuclear fission reactor cladding tube and nuclear fusion reactor blanket.
The excellent properties of ODS steel are derived from its unique microstructure, especially dispersed nano-oxides. Nano-oxides change little during thermal deformation, but nano-oxides undergo obvious plastic deformation during cold deformation, which can be dissolved and then precipitated after high temperature annealing treatment. Reasonable control of alloying elements can improve the stability and reduce the size of nano-oxides, but the interaction between grain boundaries and nano-oxides causes nano-oxides to lose the interface relationship and accelerate coarsening, and there is precipitate free zone near the grain boundaries. Due to the complex evolution mechanisms of nano-oxides in ODS steel, the control of the size and the dispersion degree of nano-oxides deserves further study.
This paper reviews the research progress on evolution mechanisms of nano-oxides in ODS steel during thermo-mechanical processing. Plastic deformation mechanism, dissolution and then reprecipitation mechanism, high-temperature stability and interaction between nano-oxides and grain boundary of nano-oxides are analyzed and summarized, respectively. Then, existing problems are pointed out, ending with a conclusion and prospect. It is expected to provide a reference for the application of ODS steel in the fourth-generation nuclear energy system cladding tube and fusion reactor cladding blanket.
Key words:  ODS steel    nano-oxides    evolution mechanism    plastic deformation    stability
出版日期:  2022-10-10      发布日期:  2022-10-12
ZTFLH:  TG142.1  
基金资助: 国家重点研究开发项目(2018YFA0702900);国家自然科学基金项目(51774265);国家科技重大专项(2019ZX06004010);中国科学院战略性先导科技专项(XDC04000000);中核集团领创项目;中国科学院跨学科创新团队和中国科学院青年创新促进会项目;兴辽英才百千万人才工程领军人才项目
通讯作者:  mysun@imr.ac.cn   
作者简介:  汪建强,2019年6月毕业于大连交通大学,获得工学硕士学位。现为中国科学技术大学材料科学与工程学院(中国科学院金属研究所)博士研究生,在孙明月研究员的指导下进行研究。目前主要研究领域为大尺寸ODS钢构筑成形技术。
孙明月,中国科学院金属研究所先进钢铁材料研究部研究员、博士研究生导师。2003年本科毕业于重庆大学,2009年在中国科学院金属研究所取得博士学位。担任国家重大专项项目负责人、国家重点研发计划课题负责人,入选科技部“创新人才推进计划重点领域创新团队”核心成员、辽宁省百千万人才工程“百层次”人才、辽宁省“兴辽英才”计划领军人才,山东省“泰山产业领军人才”等。荣获辽宁省技术发明一等奖、陈嘉庚青年科学家奖励、中国金属学会冶金青年科技奖、中国科学院青年科学家奖、中国科学院卢嘉锡青年科技奖等10余项奖励。主要从事特殊钢与大锻件均质化成形的研究工作,提出了金属构筑成形技术,通过金属构筑成形技术解决了大铸锭凝固过程的尺寸效应问题,开创了大尺寸构件新型制造学科方向。在国内外期刊上发表论文60余篇,授权发明专利50余项。
引用本文:    
汪建强, 徐斌, 谢碧君, 张健杨, 孙明月. ODS钢在热加工过程中纳米氧化物演化行为的研究进展[J]. 材料导报, 2022, 36(19): 20110267-8.
WANG Jianqiang, XU Bin, XIE Bijun, ZHANG Jianyang, SUN Mingyue. Nano-oxides Evolvement in ODS Steel During Thermo-Mechanical Processing: a Review. Materials Reports, 2022, 36(19): 20110267-8.
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http://www.mater-rep.com/CN/10.11896/cldb.20110267  或          http://www.mater-rep.com/CN/Y2022/V36/I19/20110267
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