ODS钢中纳米氧化物析出长大机制的研究进展

doi:10.11896/cldb.21100060

材料导报

2023, Vol. 37

Issue (18): 21100060-7 https://doi.org/10.11896/cldb.21100060

金属与金属基复合材料

ODS钢中纳米氧化物析出长大机制的研究进展

张孟超, 李慧^*

上海大学微结构重点实验室,上海 200444

Recent Progress on the Precipitation and Growth Mechanism of Nano-oxides in ODS Steels

ZHANG Mengchao, LI Hui^*

Key Laboratory of Microstructure, Shanghai University, Shanghai 200444, China

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摘要纳米氧化物弥散强化(Oxide dispersion strengthened,ODS)钢得益于基体中弥散分布的超高数量密度的纳米氧化物粒子,具有优异的综合服役性能,被视为第四代裂变堆包壳以及未来聚变堆包层的优选结构材料。传统制备ODS钢最主要的方法是机械合金化(Mechanical alloying,MA)等先进粉末冶金技术,且对其制备样品中氧化物粒子性质的研究较为深入。由于机械合金化在工程应用上有一定局限性,近年来提出以液态金属(Liquid metal,LM)路线制备ODS钢。目前液态金属路线中的真空熔炼法是最常用也是相对比较成功的方法,但与机械合金化相比仍有一定的差距。本文主要总结了机械合金化制备的ODS钢中纳米氧化物的析出机制、长大行为以及其他元素的添加对其产生的影响等,同时对液态金属路线的工艺进程及真空熔炼法的研究现状进行概述,并对机械合金化未来所需解决的问题和液态金属路线的后续发展、工艺优化等进行了展望,为液态金属路线的后续研究工作提供参考。

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	张孟超
	李慧

关键词: ODS钢纳米氧化物析出机制合金元素

Abstract: Nano-oxide dispersion strengthened (ODS) steel has excellent high temperature mechanical properties and radiation resistance, due to the strengthening effects of ultra-high number density of nano-oxide particles dispersed in the matrix. It has been generally used as a candidate structural material for cladding of fourth-generation fission reactors and future fusion reactors. The main manufacture process of ODS steel is advanced powder metallurgy technology, such as mechanical alloying (MA). Due to the limitations of mechanical alloying in engineering applications, the liquid metal (LM) route has been proposed to prepare ODS steel. Recently, the vacuum melting method is the most commonly used liquid metal route, and gives many interesting results. However, there are still many drawbacks compared with mechanical alloying, especially the tailoring of the oxide distribution. The current paper mainly discusses the precipitation mechanism and growth behavior of oxide particles, and the effects of the alloying elements on the nano-oxides in ODS steel prepared by mechanical alloying. An overview of the process of liquid metal route and the recent results of vacuum smelting method is also mentioned in the paper. Topics that need to be addressed in the future mechanical alloying investigation, and the further development and process optimization of the liquid metal route are prospected, which is expected to provide as a reference for the subsequent research work of the liquid metal route.

Key words: ODS steel nano-oxide precipitation mechanism alloying element

出版日期: 2023-09-25 发布日期: 2023-09-18

ZTFLH:

TG142

基金资助: 国家磁约束核聚变能研究发展专项(2018YFE0306102)

通讯作者: *李慧,上海大学材料科学与工程学院副研究员、博士研究生导师。2006年于东北大学理学院材料物理专业本科毕业,2009年于上海大学材料科学与工程学院材料学专业硕士毕业,2011年于上海大学材料科学与工程学院材料学专业博士毕业,毕业后到上海大学工作至今。目前主要从事核材料、晶界工程、析出强化合金等方面的研究工作。发表论文50余篇,包括Materials Characterization等。huili@shu.edu.cn

作者简介: 张孟超,2018年6月毕业于南阳理工学院,获得工学学士学位。现为上海大学材料科学与工程学院博士研究生,在李慧副研究员的指导下进行研究。目前主要研究领域为核材料。

引用本文:

张孟超, 李慧. ODS钢中纳米氧化物析出长大机制的研究进展[J]. 材料导报, 2023, 37(18): 21100060-7.
ZHANG Mengchao, LI Hui. Recent Progress on the Precipitation and Growth Mechanism of Nano-oxides in ODS Steels. Materials Reports, 2023, 37(18): 21100060-7.

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http://www.mater-rep.com/CN/10.11896/cldb.21100060 或 http://www.mater-rep.com/CN/Y2023/V37/I18/21100060

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