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材料导报  2021, Vol. 35 Issue (12): 12141-12146    https://doi.org/10.11896/cldb.20040050
  金属与金属基复合材料 |
高温退火时间对含铌低温取向电工钢二次再结晶行为的影响
梁锦钰, 冯运莉, 段阳会, 李杰
华北理工大学冶金与能源学院,河北省现代冶金技术重点实验室,唐山 063210
Effect of High Temperature Annealing Time on Secondary Recrystallization Behavior of Nb-containing Low Temperature Grain-oriented Electrical Steel
LIANG Jinyu, FENG Yunli, DUAN Yanghui, LI Jie
Hebei Key Laboratory of Modern Metallurgy Technology, College of Metallurgy and Energy, North China University of Science and Technology, Tangshan 063210, China
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摘要 利用OM、SEM、EDS、EBSD等技术观察和分析二次再结晶中断抽出试样的组织和取向。结果表明:高温退火保温时间达到5 h时,部分晶粒发生了二次再结晶,随着二次再结晶持续时间的延长,发生二次再结晶晶粒的数量显著增多,达到25 h时基本形成了完全的二次再结晶组织。Goss织构随保温时间的延长逐渐增多,而{111}〈112〉织构和{411}〈148〉织构含量显著降低,Goss织构含量在退火保温25 h时达到91.1%,其强度达到284.771;抑制剂随高温退火时间的延长逐渐粗化,其对晶界的钉扎逐渐减弱直到完全失去抑制作用。
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梁锦钰
冯运莉
段阳会
李杰
关键词:  含铌低温取向电工钢  高温退火  二次再结晶  织构    
Abstract: OM, SE, EDS, EBSD and other techniques were used to observe and analyze the structure and orientation of the secondary recrystallization interrupted extraction samples. The results show that when the holding time of high temperature annealing reached 5h, some grains had secondary recrystallization. With the extension of thetime of secondary recrystallization, the number of secondary recrystallization grains significantly increased. Goss texture increased with the extended of holding time, while the texture contents of {111}〈112〉 and {411}〈148〉 significantly decreased. The Goss texture content reached 91.1% and its strength reached 284.771 at the time of annealing for 25 h. The inhibitor gradually coarsens with the extension of the high-temperature annealing time, and its pinning of the grain boundary gradually weakens until the inhibitory effect is completely lost.
Key words:  Nb-containing low temperature grain-oriented electrical steel    high temperature annealing    secondary recrystallization    texture
               出版日期:  2021-06-25      发布日期:  2021-07-01
ZTFLH:  TG142.1  
基金资助: 国家自然科学基金(51674123);河北省自然科学基金重点项目(E2017209237)
通讯作者:  tsfengyl@163.com   
作者简介:  梁锦钰,华北理工大学硕士研究生,2014年9月至2018年6月在华北理工大学获得金属材料工程学士学位,主要研究方向为新型金属材料。
冯运莉, 华北理工大学教授,博士研究生导师。主要从事新型金属材料、材料加工新技术与组织性能控制、金属基复合材料以及钢铁材料表面处理等方面的研究。
引用本文:    
梁锦钰, 冯运莉, 段阳会, 李杰. 高温退火时间对含铌低温取向电工钢二次再结晶行为的影响[J]. 材料导报, 2021, 35(12): 12141-12146.
LIANG Jinyu, FENG Yunli, DUAN Yanghui, LI Jie. Effect of High Temperature Annealing Time on Secondary Recrystallization Behavior of Nb-containing Low Temperature Grain-oriented Electrical Steel. Materials Reports, 2021, 35(12): 12141-12146.
链接本文:  
http://www.mater-rep.com/CN/10.11896/cldb.20040050  或          http://www.mater-rep.com/CN/Y2021/V35/I12/12141
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