Effect of Cryogenic Deformation Treatment Before Solid Solution on Microstructure and Properties of 7050 Aluminum Alloy
WANG Lei1,2, YI Youping1,2, HUANG Shiquan1,2, DONG Fei1,2
1 College of Mechanical and Electrical Engineering, Central South University, Changsha 410083 2 State Key Laboratory of High Performance Complex Manufacturing, Central South University, Changsha 410083
Abstract: This study proposes a new cryogenic deformation process for 7050 aluminum alloy free forgings.That is, the alloy is placed in liquid nitrogen before heat treatment,after the alloy is lowered to the liquid nitrogen temperature, a single pass compression deformation is performed along the high direction. After heat treatment, hardness, room temperature tensile, electrical conductivity, intergranular corrosion, exfoliation corrosion test and metallographic microscope, scanning electron microscopy and transmission electron microscopy were used to study the effect of different cryogenic deformation on microstructure, mechanical properties and corrosion resistance of 7050 aluminum alloy.The results show that as the degree of cryogenic deformation increases, the recrystallization ratio of the alloy increases, the grains gradually refine, the spacing of the precipita-tion phase at the grain boundary decreases, and the discontinuous distribution changes to a continuous distribution, and the width of the precipitation zone is narrow. The tensile strength, yield strength and hardness of the alloy are obviously increased. The maximum lifting ranges are 33 MPa, 35 MPa and 10.5HV, respectively. The maximum elongation is 1.5%. The electrical conductivity shows a downward trend. The alloy resists intergranular corrosion and anti-flaking. Corrosion performance is reduced, the maximum depth of intergranular corrosion corresponding to 30% cryogenic deformation is 167 μm, and the peeling corrosion grade is EC.
Heinz A, Haszler A, Keidel C E, et al. Materials Science and Enginee-ring A, 2000, 280(1), 102.2 Oliveira A F, Barros M C, Cardoso K R, et al. Materials Science and Engineering A, 2004, 379(2),321.3 Mukhopadhyay A K. Metals Materials and Processes,2007,119(1), 1.4 Williams J C,Starke J E. Acta Materialia,2003,51, 5775.5 Chakrabarti D J,Liu J,Sawtell R R. Materials Science Forum,2004,28, 969.6 Furukawa M, Horita Z, Nemoto M, et al. Acta Materialia, 1996, 44(44), 4619.7 Gan W P, Wang Y R,Chen T P,et al. Materials Review, 2006, 20(5), 111(in Chinese).甘卫平,王义仁,陈铁平,等. 材料导报, 2006, 20(5), 111.8 Rangaraju N,Raghuram T,Krishina B V,et al.Materials Science and Engineering: A, 2005,398(1), 246.9 Zahid G H, Huang Y, Prangnell P B. Acta Materialia, 2009, 57(12), 3509.10 Zhao Y H, Liao X Z, Cheng S, et al. Advanced Materials, 2010, 18(17), 2280.11 Yang L J,Wu H Y,Gao G J,et al.Light Alloy Fabrication Technology, 2018(1), 14(in Chinese).杨丽娟, 吴红艳, 高冠军,等. 轻合金加工技术, 2018(1), 14.12 Shanmugasundaram T, Murty B S, Sarma V S. Scripta Materialia, 2006, 54(12), 2013.13 Peng G S, Chen K H, Chen S Y, et al. Materials & Corrosion, 2015, 63(3), 254.14 Mondolfo L F. Aliminumalloys: structure and propertys, Metallurgical Industry Press, US, 1998.15 Wang Z Q,Liu X F,Bian X F. Foundry,2001,50(6), 316(in Chinese).王振卿,刘相法,边秀房.铸造,2001,50(6), 316.16 Zhang X M,Song F X,Liu S D,et al. Journal of Central South University(Science and Technology), 2011, 42(8), 2252(in Chinese).张新明,宋丰轩,刘胜胆,等.中南大学学报(自然科学版), 2011, 42(8), 2252.17 Wang S.Optimized deformation processes and related mechanisms for improving the strength, toughness and formability of AA7050 aluminum alloy. Ph.D. Thesis, University of Science & Technology Beijing,China, 2017(in Chinese).王铄. AA7050铝合金强韧性和成形性改善的轧制工艺优化及机理研究. 博士学位论文, 北京科技大学, 2017.18 Li P C. Heavy Castings and Forgings, 2011(2), 39(in Chinese).李蓬川. 大型铸锻件, 2011(2), 39.