高能球磨法制备微米银片的工艺研究

材料导报

2021, Vol. 35

Issue (z2): 428-432

金属与金属基复合材料

高能球磨法制备微米银片的工艺研究

唐卫岗¹, 胡岭¹, 黄世盛¹, 陈融¹, 郭冰², 沈杭燕²

1 杭州华光焊接新材料股份有限公司,杭州 311112
2 中国计量大学材料与化学学院,杭州 310018

Study on the Process of Preparing Micron Silver Flakes by High Energy Ball Mill

TANG Weigang¹, HU Ling¹, HUANG Shisheng¹, CHEN Rong¹, GUO Bing², SHEN Hangyan²

1 Hangzhou Huaguang Advanced Welding Materials Co., Ltd, Hangzhou 311112, China
2 College of Materials and Chemistry, China Jiliang University, Hangzhou 310018, China

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摘要采用高能球磨法将微细银粉制备成微米级的片状银粉,并探究了不同的球磨参数对于银粉形貌和粒径的影响。实验发现,球磨时间越长,银粉的成片性较好,粒径越大。且球磨转速、球料比以及球磨介质无水乙醇量的选择至关重要,过低或过高都会影响球磨效率,使得银粉的成片性变差。当球料比为10∶1,转速250 r·min^-1,无水乙醇添加量为3 mL时,球磨制备的银粉团聚少,成片性好,银粉粒径为2~6 μm。

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	唐卫岗
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关键词: 高能球磨球磨参数微米银粉片状银粉

Abstract: Micron-sized flake silver powders were successfully prepared by high-energy ball milling method using 1 μm silver particles as raw material. The effects of ball milling parameters on the morphology and particle size of silver powders were investigated. The results show that the longer the ball milling time is used, the better the flake-forming property and the larger the particle size of the silver powder are obtained. The ball milling efficiency and the flake-forming property of the silver powders are also affected by the ball milling speed, the ball-to-material ratio and the concentration of the ball milling medium. When the ball-to-material ratio is 10∶1, the ball milling speed is 250 r·min^-1, the ball milling time is 24 h, and the amount of anhydrous ethanol is 3 mL, the silver powders prepared by ball milling have less agglomeration and better flake-forming property. The particle size of the silver powder is 2—6 μm.

Key words: high-energy ball milling ball milling parameters micron-sized silver flake silver

发布日期: 2021-12-09

ZTFLH:

TB383.1

基金资助: 浙江省科技计划项目(2018C01123)

通讯作者: shenhangyan@cjlu.edu.cn

作者简介: 唐卫岗,入职杭州华光焊接新材料股份有限公司近20年,参与了华光新材多项重大装备的设计开发,为公司钎料产业化水平提升做出重要贡献,作为公司研究院执行院长,带领团队开展了一系列钎料新产品和钎料装备的开发。重视钎焊整体解决方案的研究,在开发钎料新产品的同时,开展产业化装备和钎焊设备的设计开发,是公司多项发明和实用新型专利的主要发明人,2020年获得中国机械工业科学技术特等奖。
沈杭燕,2005年博士毕业于日本东北大学金属冶金学专业。2006年至今在中国计量大学材料与化学学院工作,现为中国计量大学教授,期间曾于2012年赴墨尔本大学做高级访问学者。在国内外学术期刊上发表论文50余篇,申请国家发明专利20余项,其中授权10项。研究领域为金属焊接材料,电子封装材料和纳米材料等。

引用本文:

唐卫岗, 胡岭, 黄世盛, 陈融, 郭冰, 沈杭燕. 高能球磨法制备微米银片的工艺研究[J]. 材料导报, 2021, 35(z2): 428-432.
TANG Weigang, HU Ling, HUANG Shisheng, CHEN Rong, GUO Bing, SHEN Hangyan. Study on the Process of Preparing Micron Silver Flakes by High Energy Ball Mill. Materials Reports, 2021, 35(z2): 428-432.

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http://www.mater-rep.com/CN/ 或 http://www.mater-rep.com/CN/Y2021/V35/Iz2/428

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