Ti3AlC2陶瓷粉末的研究现状及进展

doi:10.11896/cldb.20090196

材料导报

2022, Vol. 36

Issue (20): 20090196-11 https://doi.org/10.11896/cldb.20090196

无机非金属及其复合材料

Ti₃AlC₂陶瓷粉末的研究现状及进展

高丽娜¹, 陈文革^1,2, 李树丰^1,2,*

1 西安理工大学材料科学与工程学院,西安 710048
2 西安市先进粉末冶金材料和新技术重点实验室,西安 710048

Research Status and Progress of Ti₃AlC₂ Ceramic Powder

GAO Lina¹, CHEN Wenge^1,2, LI Shufeng^1,2,*

1 School of Materials Science and Engineering, Xi’an University of Technology, Xi’an 710048, China
2 Xi’an Key Laboratory of Advanced Powder Metallurgy Materials and New Technology, Xi’an 710048, China

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摘要层状三元钛铝化碳Ti₃AlC₂是MAX相家族中重要的一员,其因兼具金属与陶瓷的双重性能优点,引起了广泛关注。它是一种潜在的功能材料和结构材料,可作为高温结构材料、热交换器材料、耐腐蚀构件、低摩擦系数材料、电接触材料、核燃料包壳材料、损伤敏感部件等,具有广泛的应用前景。
但是合成Ti₃AlC₂的窗口非常窄,目前制备高纯Ti₃AlC₂块体材料大多采用原位反应法,不仅合成物中Ti₃AlC₂的纯度难以控制,制品外形简单,尺寸小,而且很难实现工业化生产。而常规陶瓷材料的制造大多是先合成相应的高纯陶瓷粉末,然后再通过粉体的不同设计,制备出所需要的陶瓷材料。因此,合成高纯Ti₃AlC₂陶瓷粉末对于实现Ti₃AlC₂陶瓷材料的工业化生产至关重要。
学者们针对制备高纯Ti₃AlC₂陶瓷粉末展开了深入、系统的研究。目前主要的制备方法有自蔓延高温合成法、无压烧结法、机械合金化法、机械合金化-热处理法、熔盐法、微波烧结法等,这些方法均可制备出微米或纳米级的高纯Ti₃AlC₂粉末。其中,无压烧结法工艺简单,适用范围广。众多研究表明,添加Sn、Si、Ni、B₂O₃等各种助剂可显著降低其合成温度,并提高产物中Ti₃AlC₂相的纯度。熔盐法可在较低的温度下合成分散性较好且纯度较高的纳米级Ti₃AlC₂粉体,合成产物的形貌及尺寸可控。这两种制备技术具有一定的优异性。
本文综述了国内外学者针对高纯Ti₃AlC₂陶瓷粉末的研究所取得的最新进展,分别对Ti₃AlC₂陶瓷粉末的各种制备技术、合成机理、性能对比及应用前景进行了梳理,最后对Ti₃AlC₂陶瓷粉末研究领域内亟待解决的问题进行了分析与讨论。

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关键词: MAX相 Ti₃AlC₂粉末制备技术合成机理

Abstract: Ternary layered Ti₃AlC₂, an important member of the MAX phases, attracted extensive attention due to its advantages of both metal and ceramic concurrently. As a potential functional and structural material, Ti₃AlC₂ has wide application prospects as high temperature structural materials, heat exchanger materials, corrosion-resistant components, low-friction-coefficient materials, electrical contact materials, nuclear fuel cladding materials, damage-sensitive parts and so on.
However, the synthesis window for Ti₃AlC₂ is quite narrow. At present, the in-situ reaction method is mostly used to prepare high-purity Ti₃AlC₂ bulk materials. The purity of the product prepared by this method is difficult to control, the appearance is simple, the size is small, and it is difficult to industrialize. In general, to manufacture the conventional ceramic materials, the corresponding high-purity ceramic powder is synthesized first, and then to prepare the required ceramic materials through different designs of the powder. So, the synthesis of high-purity Ti₃AlC₂ powder is vital for the manufacture of Ti₃AlC₂ ceramic materials.
In-depth and systematic research has been carried out on the synthesis of high-purity Ti₃AlC₂ ceramic powder. Currently, the main preparation methods include self-propagation high-temperature synthesis, pressureless sintering, mechanical alloying, mechanical alloying-heat treatment, molten salt, microwave sintering, etc., all of which can prepare micron or nano high-purity Ti₃AlC₂ powder. Among them, the pressureless sintering method has a simple process and a wide range of applications. Numerous studies have shown that adding additives such as Sn, Si, Ni and B₂O₃ can significantly reduce the synthesis temperature and increase the purity of the Ti₃AlC₂ phase in the product. Nano Ti₃AlC₂ powder with good dispersibility and high purity can be synthesized by molten salt method at a lower temperature, and its morphology and size are controllable. These two preparation methods are superior to others.
This paper reviewed the latest research progress of high-purity Ti₃AlC₂ powder. The preparation technology, synthesis mechanism, property comparison and future application of the Ti₃AlC₂ powder were summarized. Finally, the urgent problems in the Ti₃AlC₂ powder research were analyzed and discussed.

Key words: MAX phase Ti₃AlC₂ powder preparation technology synthesis mechanism

发布日期: 2022-10-26

ZTFLH:

TF12

基金资助: 国家自然科学基金(51871180); 国家重点研发计划(2021YFB3701203);浙江省自然科学基金(LGG20E010004); 台州市科技计划项目(1902gy16)

通讯作者: ^*shufengli@xaut.edu.cn

作者简介: 高丽娜,2009年6月毕业于西安理工大学,获得工学硕士学位。现为西安理工大学博士研究生,在李树丰教授和陈文革教授的共同指导下进行研究。目前主要研究领域为MAX/金属基复合材料。
李树丰,西安理工大学材料科学与工程学院教授、博士研究生导师。2009年于日本大学获得机械工学博士学位。2009年7月至2013年7月,在日本大阪大学结合研究所进行博士后研究工作。目前主要从事粉末冶金、陶瓷及金属基复合材料的基础研究。近年来,在Carbon、Acta Materialia、MSEA、Composites Part A、《材料研究学报》等国内外著名期刊上共发表SCI/EI学术论文100余篇,被引超1 600余次。

引用本文:

高丽娜, 陈文革, 李树丰. Ti₃AlC₂陶瓷粉末的研究现状及进展[J]. 材料导报, 2022, 36(20): 20090196-11.
GAO Lina, CHEN Wenge, LI Shufeng. Research Status and Progress of Ti₃AlC₂ Ceramic Powder. Materials Reports, 2022, 36(20): 20090196-11.

链接本文:

http://www.mater-rep.com/CN/10.11896/cldb.20090196 或 http://www.mater-rep.com/CN/Y2022/V36/I20/20090196

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