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材料导报  2018, Vol. 32 Issue (22): 3931-3935    https://doi.org/10.11896/j.issn.1005-023X.2018.22.016
  金属与金属基复合材料 |
缓冲层Ta对退火Co/Cu/Co薄膜微观结构和界面互扩散的影响
彭晓文, 陈冷
北京科技大学材料科学与工程学院,北京 100083
Effect of Ta Buffer on Microstructure and Interdiffusion of Annealed Co/Cu/Co Film
PENG Xiaowen, CHEN Leng
School of Materials Science and Engineering, University of Science and Technology Beijing, Beijing 100083
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摘要 用直流磁控溅射法在Si/SiO2基底上制备了Co/Cu/Co薄膜和加入缓冲层的Ta/Co/Cu/Co薄膜,用扫描电子显微镜、原子力显微镜、X射线衍射和俄歇电子能谱研究了薄膜的微观结构、表面形貌、织构和界面互扩散现象。结果表明:退火后薄膜中均存在{111}和{002}衍射峰,加入缓冲层Ta后,Co/Cu/Co薄膜的衍射峰强度明显增强,并存在较强的{111}纤维织构,薄膜表面孔洞及粗糙度大幅减小。退火后薄膜界面处产生互扩散现象,层状结构被破坏。缓冲层Ta提高了薄膜与基底材料间的润湿性,可有效缓解界面互扩散现象。
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彭晓文
陈冷
关键词:  巨磁电阻(GMR)薄膜  缓冲层钽  退火  织构  互扩散    
Abstract: Co/Cu/Co film and Ta/Co/Cu/Co film with buffer layer was prepared on Si/SiO2 substrate by DC magnetron sputtering method. The microstructure, surface morphology, texture and interlayer interdiffusion phenomenon of the film were investigated by scanning electron microscope, atomic force microscope, X-ray diffraction and Auger electron energy spectrum. The experimental results indicated that {111} and {002} diffracation peaks were observed during annealing in both kinds of the Co/Cu/Co film. Stronger {111} diffracation peaks and {111} fibre texture exited in Ta/Co/Cu/Co multilayers than SiO2/Co/Cu/Co multilayers. Addition of Ta buffer decreased the hole density and the roughness of the film. Furthermore, interdiffusion of Co and Cu occured at the interface, as a result the film lamellar structure was destroyed. The addition of Ta buffer increased the wettability between Co/Cu/Co film and substrate, led to an improvement of microstructure and decreased the interface interdiffusion.
Key words:  giant magnetoresistance (GMR) multilayers    Ta buffer    annealing    texture    interdiffusion
               出版日期:  2018-11-25      发布日期:  2018-12-21
ZTFLH:  TB383  
基金资助: 国家自然科学基金(51171018)
通讯作者:  陈冷:通信作者,教授,博士研究生导师,主要从事材料织构与各向异性的研究 E-mail:lchen@ustb.edu.cn   
作者简介:  彭晓文:女,1988年生,博士研究生,主要从事薄膜材料的研究 E-mail:pengxiaowen@xs.ustb.edu.cn
引用本文:    
彭晓文, 陈冷. 缓冲层Ta对退火Co/Cu/Co薄膜微观结构和界面互扩散的影响[J]. 材料导报, 2018, 32(22): 3931-3935.
PENG Xiaowen, CHEN Leng. Effect of Ta Buffer on Microstructure and Interdiffusion of Annealed Co/Cu/Co Film. Materials Reports, 2018, 32(22): 3931-3935.
链接本文:  
http://www.mater-rep.com/CN/10.11896/j.issn.1005-023X.2018.22.016  或          http://www.mater-rep.com/CN/Y2018/V32/I22/3931
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