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材料导报  2021, Vol. 35 Issue (10): 10023-10028    https://doi.org/10.11896/cldb.20040062
  无机非金属及其复合材料 |
羰基铁粉/FeSiBCCr复合非晶磁粉芯的性能
池强1,2, 谢磊1, 常良2, 李强1, 董亚强2
1 新疆大学物理科学与技术学院,乌鲁木齐 830046
2 中国科学院磁性材料与器件重点实验室,浙江省磁性材料及其应用技术重点实验室,中国科学院宁波材料技术与工程研究所,宁波 315201
Study on the Properties of Carbonyl Iron Powder/FeSiBCCr Composite Amorphous Magnetic Powder Core
CHI Qiang1,2, XIE Lei1, CHANG Liang2, LI Qiang1, DONG Yaqiang2
1 School of Physics Science and Technology, Xinjiang University, Urumqi 830046, China
2 Key Laboratory of Magnetic Materials and Devices, Zhejiang Province Key Laboratory of Magnetic Materials and Application Technology, Ningbo Institute of Materials Technology and Engineering, Chinese Academy of Sciences, Ningbo 315201, China
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摘要 随着5G时代的到来,数量庞大的基站建设对低损耗、高频特性、大功率软磁复合磁粉芯的需求不断增长,同时,宽禁带半导体技术的迅速发展对电子器件的小型化、高频化、高功率密度提出了更高的要求。然而,几乎没有软磁材料能够满足第三代宽禁带半导体的外源环境要求,这进一步制约了下一代电子器件的发展。为了满足发展需求,本工作通过将具有高饱和磁化强度(Ms)的羰基铁粉(Carbonyl iron powder, CIP)与水雾化FeSiBCCr微细非晶粉末复合,成功制备了综合软磁性能优异的FeSiBCCr复合非晶磁粉芯。研究结果表明,与没有复合CIP的FeSiBCCr非晶磁粉芯相比,当CIP含量为20%(质量分数,下同)时,FeSiBCCr复合非晶磁粉芯的Ms提高到160 emu/g左右,整体提高约6.7%;在100 Oe外加直流场下,FeSiBCCr复合非晶磁粉芯的直流偏置性能达到72%,提高了10.8%;在0.05 T@100 kHz条件下,FeSiBCCr复合非晶磁粉芯的损耗降低至296 mW/cm3,整体降低11.6%;FeSiBCCr复合非晶磁粉芯的有效磁导率和品质因数分别提高到47.0和174,提高了14.6%和9.4%。通过复合不同含量的CIP制备的新型FeSiBCCr复合非晶磁粉芯具有高的饱和磁化强度、低的损耗和良好的直流偏置特性,有望满足高频大电流器件的需要,在高频电磁系统中具有良好的应用前景。
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池强
谢磊
常良
李强
董亚强
关键词:  复合非晶磁粉芯  羰基铁粉  饱和磁化强度  损耗  直流偏置性能    
Abstract: With the advent of the 5G era, the construction of a large number of base stations has an increasing demand for low loss, high frequency characteristics and high-power soft magnetic composite magnetic powder core. Meanwhile, the rapid development of wide band-gap semiconductor technology has put forward higher requirements for the miniaturization, high-frequency and high power density of electronic devices. However, few soft magnetic materials can meet the external environment requirements of third-generation wide band-gap semiconductors, which further restricts the development of next-generation electronic devices. In order to meet the development requirements, FeSiBCCr composite amorphous magnetic powder cores with excellent comprehensive soft magnetic properties were successfully prepared by compounding water-atomized FeSiBCCr fine amorphous powder with carbonyl iron powder (CIP) with high saturation magnetization (Ms). The results show that, compared with FeSiBCCr amorphous magnetic powder cores without composite CIP, Ms of FeSiBCCr composite amorphous magnetic powder cores increase to about 160 emu/g when the CIP content is 20% (mass fraction, the same below), and the overall improvement is about 6.7%. Under 100 Oe external DC field, the DC-bias performance of FeSiBCCr composite amorphous magnetic cores reaches 72%, which is improved by 10.8%. Under the condition of 0.05 T@100 kHz, the coer loss of FeSiBCCr composite amorphous magnetic powder core is reduced to 296 mW/cm3, and the overall decrease is 11.6%. The effective permeability and quality factor of FeSiBCCr composite amorphous magnetic powder cores are increased to 47.0 and 174, respectively, by 14.6% and 9.4%. The new FeSiBCCr composite amorphous magnetic powder cores with the different filling contents of CIP exhibit high Ms, low core loss and good DC-bias characteristics, which are expected to meet the needs of high-frequency and high-current devices, and thus have a good application prospect in high-frequency electromagnetic systems.
Key words:  composite amorphous magnetic powder cores    carbonyl iron powder    saturation magnetization    core loss    DC-bias performance
               出版日期:  2021-05-25      发布日期:  2021-06-04
ZTFLH:  TB331  
  TB31  
基金资助: 国家自然科学基金(51601205;51771161);宁波市“科技创新2025”重大专项(2018B10031);宁波市奉化区重大科技专项(20194FHQ010015)
通讯作者:  qli@xju.edu.cn;dongyq@nimte.ac.cn   
作者简介:  池强,2017年6月毕业于太原科技大学,获得工学学士学位。现为新疆大学物理科学与技术学院硕士研究生,并在中国科学院宁波材料技术与工程研究所作课题生,在李强教授和董亚强高级工程师的指导下进行研究。目前主要研究领域为非晶纳米晶软磁粉芯。
李强,新疆大学教授,博士研究生导师。2002年香港中文大学博士毕业,2005年在新疆大学任教至今,其中2011—2012年在韩国庆北国立大学作博士后。在国内外学术期刊上发表学术论文50余篇,其团队主要研究方向包括:过渡族金属基块体金属玻璃磁热效应的研究;制备冷速对Fe基块体非晶态合金性能的影响;不添加玻璃化形成元素块体非晶合金的制备及性能表征;通过亚稳液相分离机制制备块体磁性纳米合金;铁基磁性块体非晶态合金的制备及性能表征。主持国家自然科学基金科研项目5项。获2017年度自治区科技进步二等奖一项,排名第一。已培养博士1名、硕士40余名、本科生百余名。
董亚强,中国科学院宁波材料技术与工程研究所高级工程师,硕士研究生导师。在国际知名学术期刊上发表SCI论文50余篇,申报国家发明专利24项,其中6项已授权。主要研究方向包括:微细金属粉末制备技术;非晶纳米晶软磁复合材料的制备及应用;非晶纳米晶软磁材料的开发及应用。作为项目负责人,主持国家自然科学基金青年基金、中科院科技网络服务计划项目(STS项目)、宁波市科技创新2025重大专项和宁波市自然科学基金等项目。已共同培养硕士研究生10余名。
引用本文:    
池强, 谢磊, 常良, 李强, 董亚强. 羰基铁粉/FeSiBCCr复合非晶磁粉芯的性能[J]. 材料导报, 2021, 35(10): 10023-10028.
CHI Qiang, XIE Lei, CHANG Liang, LI Qiang, DONG Yaqiang. Study on the Properties of Carbonyl Iron Powder/FeSiBCCr Composite Amorphous Magnetic Powder Core. Materials Reports, 2021, 35(10): 10023-10028.
链接本文:  
http://www.mater-rep.com/CN/10.11896/cldb.20040062  或          http://www.mater-rep.com/CN/Y2021/V35/I10/10023
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