Please wait a minute...
材料导报  2020, Vol. 34 Issue (10): 10093-10097    https://doi.org/10.11896/cldb.19070220
  金属与金属基复合材料 |
低塑性加工对定向凝固镍基合金DZ125高温氧化性能的影响
马文彬1,2, 郭京京2, 骆红云2, 唐君2, 杨晓光1
1 北京航空航天大学能源与动力工程学院,北京 100191
2 北京航空航天大学材料科学与工程学院,北京 100191
Effect of Low Plastic Processing on High Temperature Oxidation Property of Directionally Solidified Nickel-based Superalloy DZ125
MA Wenbin1,2, GUO Jingjing2, LUO Hongyun2, TANG Jun2, YANG Xiaoguang1
1 School of Energy and Power Engineering, Beihang University, Beijing 100191, China
2 School of Materials Science and Engineering, Beihang University, Beijing 100191, China
下载:  全 文 ( PDF ) ( 5666KB )     补充信息
输出:  BibTeX | EndNote (RIS)      
摘要 本工作在常温下对定向凝固镍基高温合金DZ125进行表面低塑性加工(熨压),并研究其高温抗氧化性能。通过微观组织分析发现,DZ125经过低塑性加工后,表面层微观组织由原始柱状晶转变为纳米晶,平均晶粒尺寸约10 nm。研究DZ125在950 ℃时的恒温氧化性能发现,低塑性加工样品表面氧化物主要为氧化铝(Al2O3)。高温下Al2O3稳定性优于氧化铬(Cr2O3),对材料的高温抗氧化性能产生正面效应,获得的氧化膜相对致密且均匀,氧化动力学曲线呈现抛物线规律。通过EDS分析试样横截面,固溶态及低塑性加工态的DZ125出现了不同程度的内氧化,低塑性加工状态下,氧化层较厚且明显。
服务
把本文推荐给朋友
加入引用管理器
E-mail Alert
RSS
作者相关文章
马文彬
郭京京
骆红云
唐君
杨晓光
关键词:  定向凝固  镍基合金  DZ125  低塑性加工  高温氧化    
Abstract: In this work, the low-plasticity burnishing (LPB) was employed to study the high temperature oxidation properties of the directionally solidified nickel-based superalloy DZ125. Microstructure analysis revealed that after the LPB process the microstructure of the surface layer changed from pristine columnar crystal to nanocrystalline, with an average grain size of about 10 nm. The surface oxide of LPB samples after high-tempe-rature oxidation at 950 ℃ was mainly alumina (Al2O3), which has better oxidation resistance than chromium oxide (Cr2O3). The oxide film obtained by LPB is relatively dense and uniform. Furthermore, analysis of the cross section of the specimen by EDS reveals that the LPB sample shows obvious internal-oxidation, with thicker oxide layer.
Key words:  directionally solidification    nickel-based superalloy    DZ125    low-plasticity burnishing (LPB)    high-temperature oxidation
               出版日期:  2020-05-25      发布日期:  2020-04-26
ZTFLH:  TG172.3  
基金资助: 国家重点研发计划(2016YFF0203301)
通讯作者:  骆红云,北京航空航天大学教授,博士研究生导师。主要研究方向:(1)(超细及纳米)材料的制备及损伤机理、表征、监测;(2)低塑性加工纳米梯度材料表面完整性;(3)生物材料及仿生材料。luo7128@163.com   
作者简介:  马文彬,2016年9月至今在北京航空航天大学攻读博士学位,主要从事镍基高温合金环境腐蚀及疲劳性能研究。
引用本文:    
马文彬, 郭京京, 骆红云, 唐君, 杨晓光. 低塑性加工对定向凝固镍基合金DZ125高温氧化性能的影响[J]. 材料导报, 2020, 34(10): 10093-10097.
MA Wenbin, GUO Jingjing, LUO Hongyun, TANG Jun, YANG Xiaoguang. Effect of Low Plastic Processing on High Temperature Oxidation Property of Directionally Solidified Nickel-based Superalloy DZ125. Materials Reports, 2020, 34(10): 10093-10097.
链接本文:  
http://www.mater-rep.com/CN/10.11896/cldb.19070220  或          http://www.mater-rep.com/CN/Y2020/V34/I10/10093
1 Hu Y B, Zhang L, Cheng C Q, et al. Acta Metallurgica Sinica (Engish Letters), 2017, 30(9), 857.
2 She L, Chen R Z, Wang T. Transactions of Materials and Heat Treatment, 2002, 23(4), 13(in Chinese).
佘力, 陈荣章, 王涛. 材料热处理学报, 2002, 23(4), 13.
3 Zhu R Z, Lu Y X. Heat resistant steel and superalloy, Chemical Industry Press, China,1996(in Chinese).
朱日彰, 卢亚轩.耐热钢和高温合金, 化学工业出版社, 1996.
4 Guo J T. Superalloy material science, China Science Publishing, China,2010(in Chinese).
郭建亭. 高温合金材料学, 科学出版社, 2010.
5 Tian N. Creep behavior and influencing factors of DZ125 alloy under long-life service conditions. Ph.D. Thesis, Shenyang University of Technology, China,2014(in Chinese).
田宁. 长寿命服役条件下DZ125合金的蠕变行为及影响因素. 博士学位论文, 沈阳工业大学, 2014.
6 Ge B M, Zhang J, Li Y F, et al. China Foundry, 2013, 10(1), 24.
7 Han C H. Investigation on the deformation processing and relationship between microstructure and property of TC4 alloy ring part. Master's Thesis, Harbin Institute of Technology, China, 2015(in Chinese).
韩春辉. TC4环形件锻造与轧制工艺及组织性能研究. 硕士学位论文,哈尔滨工业大学, 2015.
8 Zhao Z. Study on constant temperature oxidation behavior of DZ792 alloy. Master's Thesis, Northeastern University, China, 2009(in Chinese).
赵卓. DZ792合金的恒温氧化行为研究. 硕士学位论文, 东北大学, 2009.
9 Bensch M, Sato A, Warnken N, et al. Acta Materialia, 2012, 60(15), 5468.
10 Li W Y, Liu H F, Zhao S Q. Transactions of Materials and Heat Treatment, 2008, 29(3), 26(in Chinese).
李维银, 刘红飞, 赵双群. 材料热处理学报, 2008, 29(3), 26.
11 Liang Y J. Inorganic thermodynamic data sheet, Northeastern University Press, China, 1993(in Chinese).
梁英教. 无机物热力学数据手册, 东北大学出版社, 1993.
12 Eaborn C. Landolt B. Journal of Organometallic Chemistry, 1978, 149(2), C47.
13 Wenderoth M, Völkl R, Vorberg S, et al. Intermetallics, 2007, 15(4), 539.
14 Wenderoth M, Glatzel U, Völkl R. Metallurgical and Materials Transactions A, 2005, 36(3), 567.
15 Bensch M, Preuβner J, Hüttner R, et al. Acta Materialia, 2010, 58(5), 1607.
[1] 蒋健博, 黄以平, 李少林, 刘海浪, 彭治国, 谭毅. 电子束诱导定向凝固对硅中Fe杂质分凝的影响[J]. 材料导报, 2020, 34(Z2): 173-176.
[2] 李鑫, 谢辉, 杨宾, 李双明. Mg2(Si,Sn)基热电材料研究进展[J]. 材料导报, 2020, 34(Z1): 43-47.
[3] 林启权, 周行, 董文正, 钦椿凯. CoO和Cr2O3复合掺杂对金属陶瓷的致密化及抗高温氧化性的影响[J]. 材料导报, 2020, 34(6): 6044-6048.
[4] 刘浩东, 喻辉, 戴京涛, 崔爱永, 魏华凯, 赵培仲, 卢长亮. 非真空激光定向凝固参数对DZ22合金熔覆层组织的影响[J]. 材料导报, 2020, 34(20): 20091-20095.
[5] 李鑫, 谢辉, 魏鑫, 张亚龙. Mg2Si1-xSnx合金热电性能的第一性原理计算预测[J]. 材料导报, 2020, 34(18): 18098-18103.
[6] 孙彬, 郝明欣, 尤宏广, 王皓, 曹光明. Fe-1Cr-0.2Si钢的高温氧化行为[J]. 材料导报, 2020, 34(16): 16131-16135.
[7] 杨金祥, 石爽, 姜大川, 李旭, 李鹏廷, 谭毅, 姚玉杰, 池明, 张润德, 张建帅. 多晶硅定向凝固过程中温度对凝固速率的影响[J]. 材料导报, 2019, 33(z1): 28-32.
[8] 范舟, 黄泰愚, 刘建仪. 硫对镍基合金825(100)电子结构影响的密度泛函研究[J]. 材料导报, 2019, 33(z1): 332-336.
[9] 平学龙, 符寒光, 孙淑婷. 激光熔覆制备硬质颗粒增强镍基合金复合涂层的研究进展[J]. 材料导报, 2019, 33(9): 1535-1540.
[10] 卢百平, 崔春娟, 田露露, 问亚岗, 王佩. 布里奇曼定向凝固Ni-12%Si过共晶的弹性模量与断裂韧性[J]. 材料导报, 2019, 33(8): 1383-1388.
[11] 陈文龙, 刘敏, 张吉阜, 邓子谦, 肖晓玲, 唐维学. 等离子喷涂-物理气相沉积7YSZ热障涂层高温氧化过程中的阻抗谱分析[J]. 材料导报, 2019, 33(4): 605-606.
[12] 王晓娟, 刘林, 赵新宝, 黄太文, 杨文超, 张军, 傅恒志. 添加碳和硼改善第三代镍基定向凝固高温合金的显微组织和偏析行为[J]. 材料导报, 2019, 33(20): 3452-3459.
[13] 朱靖, 李勇, 王莹, 李焕, 赵亚茹. 不同定向凝固速率下Cu-2.5%Cr合金中带状组织的形成机理[J]. 材料导报, 2019, 33(2): 309-313.
[14] 魏岑,李向明. 一种不稳定的共晶生长方式:倾斜共晶生长的研究进展[J]. 材料导报, 2019, 33(15): 2532-2537.
[15] 蒋智秋, 陈泉志, 董婉冰, 童庆, 李伟洲. Al对激光熔覆镍基合金涂层组织与性能的影响[J]. 材料导报, 2019, 33(12): 2035-2039.
[1] Bingwei LUO,Dabo LIU,Fei LUO,Ye TIAN,Dongsheng CHEN,Haitao ZHOU. Research on the Two Typical Infrared Detection Materials Serving at Low Temperatures: a Review[J]. Materials Reports, 2018, 32(3): 398 -404 .
[2] Huimin PAN,Jun FU,Qingxin ZHAO. Sulfate Attack Resistance of Concrete Subjected to Disturbance in Hardening Stage[J]. Materials Reports, 2018, 32(2): 282 -287 .
[3] Xu LI,Ziru WANG,Li YANG,Zhendong ZHANG,Youting ZHANG,Yifan DU. Synthesis and Performance of Magnetic Oil Absorption Material with Rice Chaff Support[J]. Materials Reports, 2018, 32(2): 219 -222 .
[4] XU Zhichao, FENG Zhongxue, SHI Qingnan, YANG Yingxiang, WANG Xiaoqi, QI Huarong. Microstructure of the LPSO Phase in Mg98.5Zn0.5Y1 Alloy Prepared by Directional Solidification and Its Effect on Electromagnetic Shielding Performance[J]. Materials Reports, 2018, 32(6): 865 -869 .
[5] WANG Tong, BAO Yan. Advances on Functional Polyacrylate/Inorganic Nanocomposite Latex for Leather Finishing[J]. Materials Reports, 2017, 31(1): 64 -71 .
[6] HUANG Dajian, MA Zonghong, MA Chenyang, WANG Xinwei. Preparation and Properties of Gelatin/Chitosan Composite Films Enhanced by Chitin Nanofiber[J]. Materials Reports, 2017, 31(8): 21 -24 .
[7] DU Wenbo, YAO Zhengjun, TAO Xuewei, LUO Xixi. High-temperature Anti-oxidation Property of Al2O3 Gradient Composite Coatings on TC11 Alloys[J]. Materials Reports, 2017, 31(14): 57 -60 .
[8] ZHANG Le, ZHOU Tianyuan, CHEN Hao, YANG Hao, ZHANG Qitu, SONG Bo, WONG Chingping. Advances in Transparent Nd∶YAG Laser Ceramics[J]. Materials Reports, 2017, 31(13): 41 -50 .
[9] ZHANG Yating, REN Shaozhao, DANG Yongqiang, LIU Guoyang, LI Keke, ZHOU Anning, QIU Jieshan. Electrochemical Capacitive Properties of Coal-based Three-dimensional Graphene Electrode in Different Electrolytes[J]. Materials Reports, 2017, 31(16): 1 -5 .
[10] CHEN Bida, GAN Guisheng, WU Yiping, OU Yanjie. Advances in Persistence Phosphors Activated by Blue-light[J]. Materials Reports, 2017, 31(21): 37 -45 .
Viewed
Full text


Abstract

Cited
  Shared   
  Discussed