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材料导报  2026, Vol. 40 Issue (8): 25040180-7    https://doi.org/10.11896/cldb.25040180
  无机非金属及其复合材料 |
玄武岩熔融出丝漏嘴长度对纤维成型的影响
刘春岳1, 张启帆2, 张建伟1,*, 张蕾2,3, 刘嘉麒1,3, 王淇芃2
1 青岛大学环境与地理科学学院,玄武岩纤维生态应用研究院,山东 青岛 266071
2 中科石源新材料科技(青岛)有限公司,山东 青岛 266237
3 中国科学院地质与地球物理研究所,北京 102213
Effect of Basalt Melt-out Nozzle Length on Fiber Forming
LIU Chunyue1, ZHANG Qifan2, ZHANG Jianwei1,*, ZHANG Lei2,3, LIU Jiaqi1,3, WANG Qipeng2
1 School of Environmental and Geographic Sciences, Institute of Basalt Fiber Ecological Applications, Qingdao University, Qingdao 266071, Shandong, China
2 Zhongke Shiyuan New Material Technology (Qingdao) Co., Ltd., Qingdao 266237, Shandong, China
3 Institute of Geology and Geophysics, Chinese Academy of Sciences, Beijing 102213, China
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摘要 玄武岩纤维制备中,出丝漏嘴长度直接关乎纤维能否成型以及拉丝过程稳定性。为探讨制备玄武岩纤维的熔融出丝漏嘴长度对纤维成型的影响,专门设计了漏嘴长度为2 mm、3 mm、4 mm、5 mm、6 mm的五孔坩埚,采用同一玄武岩熔体原料及实验环境条件。拉丝实验显示,所用样品在1 450 ℃成纤效果最好,3 mm长度的漏嘴最容易稳定成纤,2 mm和4 mm长度的漏嘴可成纤但不稳定,5 mm和6 mm长度的漏嘴成纤较难。基于熔融实验,利用COMSOL Multiphysics建立模型,选择1 450 ℃进行过程数据模拟分析,模拟结果与实验中呈现的不同漏嘴长度的成纤效果是吻合的;漏嘴长度与熔体流速负相关,3 mm漏嘴出口处熔体流动性好,而2 mm漏嘴的过高流速会降低拉丝稳定性;漏嘴长度与熔体温度负相关,3 mm的漏嘴熔体纵向温度变化较小,易成纤,而4 mm、5 mm、6 mm的漏嘴因散热增强末端温差达14.7~29.6 ℃,不利于成纤;漏嘴长度与熔体黏度正相关,3 mm漏嘴末端熔体黏度差为3.2 Pa·s,成纤稳定;随着漏嘴长度增加,黏度梯度逐渐增加,成纤稳定性降低;玄武岩熔体黏度与温度负相关。当漏嘴出口处熔体温度为1 379.9 ℃、流速为1.08×10-3 m/s、黏度为48.5 Pa·s时,漏嘴长度为3 mm条件下的成纤效果最优。所提出的方法对于玄武岩熔融出丝漏嘴长度参数的优化以及纤维产业化生产工艺参数的调整具有重要参考价值。
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刘春岳
张启帆
张建伟
张蕾
刘嘉麒
王淇芃
关键词:  玄武岩纤维  熔融  出丝漏嘴长度  纤维成型  模拟    
Abstract: The successful formation of basalt fibers and the stability of the fiber drawing process are directly governed by the length parameter of the spinneret nozzle. The influence of spinneret nozzle length on basalt fiber formation was systematically investigated through the design of a quintuple-orifice crucible with precisely controlled nozzle dimensions of 2 mm, 3 mm, 4 mm, 5 mm, and 6 mm. Under standardized experimental conditions with consistent basalt melt composition and thermal environment, optimal fiber formation was achieved at 1 450 ℃, wherein the 3 mm nozzle exhibited superior process stability. While continuous filaments were obtainable with 2 mm and 4 mm nozzles, notable process fluctuations were observed. The 5 mm and 6 mm configurations demonstrated compromised fiber-forming capability under equivalent process parameters. The quantitative correlation between spinneret nozzle geometries and fiber formation efficiency was systematically validated through COMSOL Multiphysics simulations conducted at 1 450 ℃ melt temperature. Computational results demonstrated precise consistency with experimental observations regarding filament continuity and process stability across varying nozzle lengths. The inverse correlation between nozzle length and melt flow velocity was quantitatively established, wherein optimal fluidity characteristics were attained at the 3 mm configuration, whereas excessive velocity gradients induced by the 2 mm nozzle were identified as detrimental to fiber drawing stability. Concurrently, longitudinal thermal gra-dients within the melt were demonstrated to be inversely governed by nozzle length, with the 3 mm variant exhibiting minimal temperature variation along the flow path, thus enabling continuous fiber formation. By contrast, terminal temperature differentials ranging from 14.7 ℃ to 29.6 ℃ were recorded in 4—6 mm nozzles due to intensified convective heat dissipation, resulting in compromised fiber-forming continuity. A positive correlation between spinneret nozzle length and melt viscosity was established through characterization, with the 3 mm configuration exhibiting an optimal terminal viscosity differential of 3.2 Pa·s that ensured stable fiber formation. Progressive destabilization of the fiberization process was observed as the nozzle length increased, attributable to amplified viscosity gradient magnitudes within the melt flow field. An inverse correlation between basaltic melt viscosity and temperature was established. Optimal fiber formation efficiency was demonstrated under standardized conditions of 1 379.9 ℃ melt temperature, 1.08×10-3 m/s flow velocity, and 48.5 Pa·s viscosity at the spinneret orifice, achieving superior process stability with the 3 mm nozzle configuration. The established methodology was validated as providing a critical optimization framework for spinneret nozzle length parameters and industrial fiber production process adjustments in basaltic melt fiberization systems.
Key words:  basalt fiber    melting    spinneret nozzle length    fiber formation    simulation
出版日期:  2026-04-25      发布日期:  2026-05-06
ZTFLH:  TQ343+.9  
基金资助: 省部共建生物多糖纤维成形与生态纺织国家重点实验室(青岛大学)课题(RZ2200002491);青岛大学学科建设人才项目(DC2100004477);玄纤工艺控制系统研发与制备(RH2500003392)
通讯作者:  * 张建伟,博士,青岛大学环境与地理科学学院玄武岩纤维生态应用研究院教授、硕士研究生导师。目前主要研究领域为地球化学、天然矿物材料。zhangjianwei1@qdu.edu.cn   
作者简介:  刘春岳,青岛大学环境与地理科学学院玄武岩纤维生态应用研究院硕士研究生,主要研究玄武岩纤维生产工艺。
引用本文:    
刘春岳, 张启帆, 张建伟, 张蕾, 刘嘉麒, 王淇芃. 玄武岩熔融出丝漏嘴长度对纤维成型的影响[J]. 材料导报, 2026, 40(8): 25040180-7.
LIU Chunyue, ZHANG Qifan, ZHANG Jianwei, ZHANG Lei, LIU Jiaqi, WANG Qipeng. Effect of Basalt Melt-out Nozzle Length on Fiber Forming. Materials Reports, 2026, 40(8): 25040180-7.
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https://www.mater-rep.com/CN/10.11896/cldb.25040180  或          https://www.mater-rep.com/CN/Y2026/V40/I8/25040180
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