高温处理对玄武岩纤维抗拉强度和结构的影响

doi:10.11896/cldb.22090168

材料导报

2024, Vol. 38

Issue (11): 22090168-6 https://doi.org/10.11896/cldb.22090168

无机非金属及其复合材料

高温处理对玄武岩纤维抗拉强度和结构的影响

苗世坦¹, 刘嘉麒^1,2,*, 郭玲¹, 刘忠¹, 丁宝明³, 张蕾²

1 河北地质大学宝石与材料学院,河北省岩石矿物材料绿色开发重点实验室,玄武岩纤维研究所,石家庄 050031
2 中国科学院地质与地球物理研究所,北京 100029
3 中国地质大学(北京)地球科学与资源学院,北京 100083

Effect of High Temperature Treatment on Tensile Strength and Structure of Basalt Fiber

MIAO Shitan¹, LIU Jiaqi^1,2,*, GUO Ling¹, LIU Zhong¹, DING Baoming³, ZHANG Lei²

1 Institute of Basalt Fiber Materials, Hebei Key Laboratory of Green Development of Rock and Mineral Materials, School of Gem and Materials, Hebei GEO University, Shijiazhuang 050031, China
2 Institute of Geology and Geophysics, Chinese Academy of Sciences, Beijing 100029, China
3 School of Earth Sciences and Resources, China University of Geosciences (Beijing), Beijing 100083, China

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摘要本工作选取山东某地的玄武岩矿石为原料,制备了连续玄武岩纤维,并在空气气氛条件下,对玄武岩纤维进行200～900 ℃的高温热处理。采用多种现代分析测试手段,研究了热处理温度对玄武岩纤维的抗拉强度、表面形貌、微观结构及析晶行为的影响。结果表明:随着热处理温度的升高,纤维的抗拉强度呈近线性下降趋势;纤维表面出现沿轴向裂纹分布的缺陷且数量增多,损伤程度增大;纤维内部单元无序化程度增加,结构逐渐解聚;800 ℃热处理后,主要析晶相为辉石相与磁铁矿相,900 ℃热处理后出现赤铁矿相。

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关键词: 玄武岩纤维高温处理抗拉强度结构

Abstract: In this work, continuous basalt fibers were prepared from basalt in Shandong Province. Basalt fibers were heat treated at 200—900 ℃ under air atmosphere. The effects of heat treatment temperature on tensile strength, surface morphology, microstructure and crystallization beha-vior of basalt fibers were studied by various modern analysis and testing methods. The results showed that the tensile strength of the fibers decreased linearly with the increase of heat treatment temperature. Defects on the surface that distribute along the axial cracks increased in number and severity. The fiber structure gradually decomposed and the degree of disorder of internal units increased. After heat treatment at 800 ℃, the main crystallization phases were augite phase and magnetite phase. Hematite phase occurs after heat treatment at 900 ℃.

Key words: basalt fiber high temperature treatment tensile strength structure

发布日期: 2024-06-25

ZTFLH:

TB321

基金资助: 河北省科技厅指导地方科技发展资金项目(206Z1501G)

通讯作者: *刘嘉麒,中国科学院院士,中国科学院地质与地球物理研究所研究员,河北地质大学特聘教授。主要从事火山学、第四纪地质学、玄武岩新材料等研究。共发表论文300余篇,代表专著有《中国火山》《玄武岩纤维材料》。liujq@mail.iggcas.ac.cn

作者简介: 苗世坦,现为河北地质大学宝石与材料学院硕士研究生,在刘嘉麒研究员的指导下进行研究。目前主要研究领域为天然矿物材料。

引用本文:

苗世坦, 刘嘉麒, 郭玲, 刘忠, 丁宝明, 张蕾. 高温处理对玄武岩纤维抗拉强度和结构的影响[J]. 材料导报, 2024, 38(11): 22090168-6.
MIAO Shitan, LIU Jiaqi, GUO Ling, LIU Zhong, DING Baoming, ZHANG Lei. Effect of High Temperature Treatment on Tensile Strength and Structure of Basalt Fiber. Materials Reports, 2024, 38(11): 22090168-6.

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http://www.mater-rep.com/CN/10.11896/cldb.22090168 或 http://www.mater-rep.com/CN/Y2024/V38/I11/22090168

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