Please wait a minute...
材料导报  2019, Vol. 33 Issue (14): 2403-2407    https://doi.org/10.11896/cldb.18050079
  金属与金属基复合材料 |
预合金结合剂成分及烧结工艺对金刚石工具性能的影响
侯明1,2, 郭胜惠1,2,3,4, 高冀芸5, 杨黎1,2,4, 王梁1,2, 叶小磊1,2
1 昆明理工大学复杂有色金属资源清洁利用国家重点实验室,昆明 650093;
2 昆明理工大学冶金与能源工程学院,昆明 650093;
3 昆明理工大学国家超硬材料先进制备技术国际联合研究中心,昆明 650093;
4 昆明理工大学微波能工程应用和装备技术国家地方联合工程实验室,昆明 650093;
5 云南民族大学化学与环境学院,昆明 650500
Effect of Pre-alloyed Powder with Different Composition and Sintering Process on Performance of Diamond Tools
HOU Ming1,2, GUO Shenghui1,2,3,4, GAO Jiyun5, YANG Li1,2,4, WANG Liang1,2, YE Xiaolei1,2
1 State Key Laboratory of Complex Nonferrous Metal Resources Clean Utilization, Kunming University of Science and Technology, Kunming 650093;
2 Faculty of Metallurgical and Energy Engineering, Kunming University of Science and Technology, Kunming 650093;
3 State International Joint Research Center of Advanced Technology for Superhard Materials, Kunming University of Science and Technology, Kunming 650093;
4 National Local Joint Laboratory of Engineering Application of Microwave Energy and Equipment Technology, Kunming University of Science and Technology,Kunming 650093;
5 Faculty of Chemistry and Environment, Yunnan Minzu University, Kunming 650500
下载:  全 文 ( PDF ) ( 3033KB ) 
输出:  BibTeX | EndNote (RIS)      
摘要 以Fe40Cu40Co20预合金粉、Cu80Sn20预合金粉和WC粉为原料,通过真空无压烧结方法制得金刚石工具胎体样品,并采用扫描电子显微镜、洛氏硬度计、阿基米德排水法分析了预合金粉含量对样品微观形貌、硬度和相对致密度的影响。结果表明,Fe40Cu40Co20预合金粉、Cu80Sn20预合金粉和WC粉含量分别为50%、40%和10%时,样品具有最佳的综合力学性能,胎体的相对致密度和硬度分别达到94.6%和105HRB。在此基础上,探讨了最佳胎体配方条件下冷压压力及保温时间对样品力学性能的影响,研究发现冷压压力为45 MPa、烧结保温时间为30 min时,样品具有良好的综合力学性能。本工作可为建立金刚石工具的无压烧结方法提供前期实验探索。
服务
把本文推荐给朋友
加入引用管理器
E-mail Alert
RSS
作者相关文章
侯明
郭胜惠
高冀芸
杨黎
王梁
叶小磊
关键词:  预合金粉  真空无压烧结  烧结工艺  金刚石工具  力学性能    
Abstract: In this paper, Fe40Cu40Co20 pre-alloyed powders, Cu80Sn20 pre-alloyed powders and WC powders were used as raw materials. The matrix samples of diamond tools were prepared by vacuum pressureless sintering process. Scanning electron microscope, Rockwell hardness tester and Archimedes Drainage Act were used to check the microscope, hardness and relative density of samples. And the effects of different content of pre-alloyed powders on the micro-morphology, hardness and relative density of the carcass were studied. The results showed that when the content of Fe40Cu40Co20 pre-alloyed powder, Cu80Sn20 pre-alloyed powder and WC powder was 50%, 40% and 10% respectively, the overall performance of the matrix was the best. The density and hardness could reach 94.6% and 105HRB, respectively. On the basis of the best formula, the effects of different cold pressure and holding time on the mechanical properties of the matrix were studied. It was found that the matrix possessed superiority comprehensive mechanical properties when the cold pressing pressure was 45 MPa and the sintering holding time was 30 min. This work can provide preliminary experimental for the establishment of the pressureless sintering process for diamond tools.
Key words:  pre-alloyed powder    vacuum pressureless sintering    sintering process    diamond tools    mechanical properties
                    发布日期:  2019-06-19
ZTFLH:  TB34  
基金资助: 国家自然科学基金(51864028;51604134);云南省应用基础研究计划(2018FD053;2018FA029);云南省教育厅科学研究基金(2018JS306);国家国际科技合作项目(2015DFR50620)
通讯作者:  yanglikmust@163.com   
作者简介:  侯明,2016年6月毕业于辽宁科技学院,获得工程学士学位。现在是硕博连读在校学生,主要从事超硬材料制备领域的研究。杨黎,2013年11月毕业于华中科技大学,获得工程博士学位。目前是昆明理工大学副教授,主要从事金刚石工具烧结设备的制备及技术创新的研发,重点研究超硬材料,功能材料及纳米器件的制备。已经在著名期刊中发表论文20余篇。
引用本文:    
侯明, 郭胜惠, 高冀芸, 杨黎, 王梁, 叶小磊. 预合金结合剂成分及烧结工艺对金刚石工具性能的影响[J]. 材料导报, 2019, 33(14): 2403-2407.
HOU Ming, GUO Shenghui, GAO Jiyun, YANG Li, WANG Liang, YE Xiaolei. Effect of Pre-alloyed Powder with Different Composition and Sintering Process on Performance of Diamond Tools. Materials Reports, 2019, 33(14): 2403-2407.
链接本文:  
http://www.mater-rep.com/CN/10.11896/cldb.18050079  或          http://www.mater-rep.com/CN/Y2019/V33/I14/2403
1 Wang S X, Liu X J, Geng L, et al. Chinese Journal of Nonferrous Me-tals, 2008, 18(3),471(in Chinese).
王双喜, 刘雪敬, 耿林, 等. 中国有色金属学报, 2008, 18(3),471.
2 Wu Y H, Li G B, Lv J W. Diamond & Abrasives Engineering, 2006(2),23(in Chinese).
吴玉会, 李国彬, 吕建伟. 金刚石与磨料磨具工程, 2006(2),23.
3 Zhang G X, Ding T R, Long W M. Welding Technology, 2012, 41(12),38(in Chinese).
张冠星, 丁天然, 龙伟民. 焊接技术, 2012, 41(12),38.
4 Meng G H, Lei X X, Lu A J, et al. Powder Metallurgy Technology, 2015, 33(2),105(in Chinese).
蒙光海, 雷晓旭, 卢安军, 等. 粉末冶金技术, 2015, 33(2),105.
5 Lu X, He X B, Qu X H. Journal of Aeronautical Materials,2009, 29(1),16(in Chinese).
路新, 何新波, 曲选辉. 航空材料学报, 2009, 29(1),16.
6 Dong X L, Kong L. Superhard Material Engineering, 2009, 21(5),11(in Chinese).
董先龙, 孔辽. 超硬材料工程, 2009, 21(5),11.
7 Hou M, Guo S H, Gao J Y, et al. Diamond & Abrasives Engineering, 2017(5),35(in Chinese).
侯明, 郭胜惠, 高冀芸, 等. 金刚石与磨料磨具工程, 2017(5),35.
8 Xie D L. Study on preparation and application of FeCoCu pre-alloyed powders for deep prospecting diamond bits. Ph.D. Thesis, Hunan University, China, 2016(in Chinese).
谢德龙. 深孔钻探金刚石钻头用FeCoCu预合金粉的制备及性能研究. 博士学位论文, 湖南大学, 2016.
9 He J. Preparation and properties of Fe-Cu-Sn based diamond saw matrix. Master's Thesis, Zhongnan University, China, 2010(in Chinese).
何娟. Fe-Cu-Sn基金刚石锯片胎体材料制备及性能研究. 硕士学位论文, 中南大学, 2010.
10 Liang L X F. Metal binary phase diagram manual, Chemical Industry Press, China, 2009(in Chinese).
粱基谢夫,金属二元相图手册, 化学工业出版社,2009.
11 Huang W J, Meng F C. Journal of Chongqing University of Technology (Natural Science),2010, 24(10),28(in Chinese).
黄伟九, 孟范成. 重庆理工大学学报(自然科学), 2010, 24(10),28.
12 Yan J, Jiang K Y. Journal of Chongqing University of Technology (Natural Science), 2012, 26(9),42(in Chinese).
闫洁, 江开勇.重庆理工大学学报(自然科学), 2012, 26(9),42.
13 Yang L Q, Luo Y, Luo W L. Superhard Material Engineering, 2016, 28(6),10(in Chinese).
杨理清, 骆颖, 罗文来. 超硬材料工程, 2016, 28(6),10.
14 Chen Z W. Development of special impregnated diamond drill bits sui-table for Jin chuan mining area. Master's Thesis, Zhongnan University, China, 2008(in Chinese).
陈章文. 适合金川矿区的特种孕镶金刚石钻头研制. 硕士学位论文, 中南大学, 2008.
[1] 刘印, 王昌, 于振涛, 盖晋阳, 曾德鹏. 医用镁合金的力学性能研究进展[J]. 材料导报, 2019, 33(z1): 288-292.
[2] 岳慧芳, 冯可芹, 庞华, 张瑞谦, 李垣明, 吕亮亮, 赵艳丽, 袁攀. 粉末冶金法烧结制备SiC/Zr耐事故复合材料的研究[J]. 材料导报, 2019, 33(z1): 321-325.
[3] 张长亮, 卢一平. 氮元素对Ti2ZrHfV0.5Mo0.2高熵合金组织及力学性能的影响[J]. 材料导报, 2019, 33(z1): 329-331.
[4] 晁代义, 徐仁根, 孙有政, 赵巍, 吕正风, 程仁策, 邵文柱. 850 ℃时效处理对2205双相不锈钢组织与力学性能的影响[J]. 材料导报, 2019, 33(z1): 369-372.
[5] 任秀秀, 朱一举, 赵省向, 韩仲熙, 姚李娜. 四种含能晶体微观力学性能与摩擦性能的关系[J]. 材料导报, 2019, 33(z1): 448-452.
[6] 薛晓武, 王新闻, 刘红波, 卿宁. 水性聚碳酸酯型聚氨酯的制备及性能[J]. 材料导报, 2019, 33(z1): 488-490.
[7] 杨康, 赵为平, 赵立杰, 梁宇, 薛继佳, 梅莉. 固化湿度对复合材料层合板力学性能的影响与分析[J]. 材料导报, 2019, 33(z1): 223-224.
[8] 平学龙, 符寒光, 孙淑婷. 激光熔覆制备硬质颗粒增强镍基合金复合涂层的研究进展[J]. 材料导报, 2019, 33(9): 1535-1540.
[9] 薛翠真, 申爱琴, 郭寅川. 基于孔结构参数的掺CWCPM混凝土抗压强度预测模型的建立[J]. 材料导报, 2019, 33(8): 1348-1353.
[10] 孙娅, 吴长军, 刘亚, 彭浩平, 苏旭平. 合金元素对CoCrFeNi基高熵合金相组成和力学性能影响的研究现状[J]. 材料导报, 2019, 33(7): 1169-1173.
[11] 李响, 毛萍莉, 王峰, 王志, 刘正, 周乐. 长周期有序堆垛相(LPSO)的研究现状及在镁合金中的作用[J]. 材料导报, 2019, 33(7): 1182-1189.
[12] 郭丽萍, 谌正凯, 陈波, 杨亚男. 生态型高延性水泥基复合材料的可适性设计理论与可靠性验证Ⅰ:可适性设计理论[J]. 材料导报, 2019, 33(5): 744-749.
[13] 赵立臣, 谢宇, 张喆, 王铁宝, 王新, 崔春翔. ZnO纳米棒/多孔锌泡沫的制备及其压缩和抗菌性能[J]. 材料导报, 2019, 33(4): 577-581.
[14] 何秀兰, 杜闫, 巩庆东, 郑威, 柳军旺. 凝胶-发泡法制备多孔Al2O3陶瓷及其力学性能[J]. 材料导报, 2019, 33(4): 607-610.
[15] 董天顺, 郑晓东, 李国禄, 王海斗, 周秀锴, 李亚龙. 大气等离子喷涂Fe基涂层及其氩弧重熔层的组织与力学性能[J]. 材料导报, 2019, 33(4): 678-683.
No Suggested Reading articles found!
Viewed
Full text


Abstract

Cited

  Shared   
  Discussed