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材料导报  2024, Vol. 38 Issue (17): 23060075-10    https://doi.org/10.11896/cldb.23060075
  无机非金属及其复合材料 |
粉体特性对光固化3D打印陶瓷浆料性质影响的研究进展
郝舒琪1, 苏海军1,2,*, 赵迪1, 李翔1, 董栋1, 于佳俊3
1 西北工业大学凝固技术国家重点实验室,西安 710072
2 西北工业大学深圳研究院,广东 深圳 518057
3 南昌大学物理与材料学院,南昌 330031
Research Progress on the Effect of Powder Characteristics on the Properties of Ceramic Slurry Based Stereolithography 3D Printing
HAO Shuqi1, SU Haijun1,2,*, ZHAO Di1, LI Xiang1, DONG Dong1, YU Jiajun3
1 State Key Laboratory of Solidification Processing, Northwestern Polytechnical University, Xi'an 710072, China
2 Research & Development Institute of Northwestern Polytechnical University in Shenzhen, Shenzhen 518057, Guangdong, China
3 School of Physics and Materials Science, Nanchang University, Nanchang 330031, China
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摘要 陶瓷材料因力学性能优异、化学稳定性好而被广泛应用,但其硬度高,脆性大,使陶瓷构件的成型与加工存在挑战。传统陶瓷成型技术已无法满足复杂精密陶瓷的生产需求。近年来陶瓷增材制造技术发展迅猛,光固化3D打印凭借打印速度快、成型精度高、生坯表面光滑等独特优势脱颖而出。作为光固化技术的原料,陶瓷浆料的性质严重影响成型质量。高质量光固化浆料应具有高固含量、低粘度、抗沉降的特点。由于光固化浆料的组成成分多样,影响陶瓷浆料性质的因素众多,如何获取最佳光固化浆料配方一直是一个难点。针对上述问题,本文在简述光固化3D打印技术原理及陶瓷浆料制备原则的基础上,从陶瓷粉体的性质出发,重点介绍了陶瓷粉体性质、粒径分布及级配设计对浆料流变性、稳定性以及光聚合性能影响的研究进展,并对光固化3D打印浆料制备中的陶瓷原料优化方法进行了总结与展望,为研究者从陶瓷原料选择与设计角度改善光固化浆料性质提供参考。
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郝舒琪
苏海军
赵迪
李翔
董栋
于佳俊
关键词:  光固化3D打印  陶瓷粉体特性  浆料制备  浆料流变性  固含量    
Abstract: Ceramic materials are widely used because of their excellent mechanical properties and chemical stability. However, due to their high hardness and brittleness, there are challenges in the forming and processing of ceramic components. Traditional ceramic molding technologies have been unable to meet requirements of the production of complex precise ceramics. Recently, ceramic additive manufacturing technology has developed rapidly. Stereolithography 3D printing technology stands out with its unique advantages such as fast printing speed, high molding accuracy and smooth surface of green bodies. As the raw material of stereolithography, the properties of ceramic slurry affect the printing process and molding quality of ceramic products seriously. High quality stereolithography ceramic slurry has the characteristics of high solid content, low viscosity, and anti-settling. Due to the variety of components, many factors affect the properties of ceramic slurry. How to obtain the best formulation of ceramic slurry has always been a difficult problem. For this problem, based on a brief introduction to the theory of stereolithography 3D printing technology and the preparation principle of ceramic slurry, starting from the properties of ceramic powder, this paper focuses on the research progress of the effects of ceramic powder properties, particle size distribution and grading design on the rheology, stability and photopolymerization performance of the slurry. Finally, we summarize and prospect optimization methods of ceramic raw materials in the preparation of ceramic slurry based by stereolithography 3D printing. This paper is aiming to provide a reference for researchers to improve slurry properties by selecting and designing raw ceramic materials.
Key words:  stereolithography 3D printing    ceramic powder characteristics    slurry preparation    rheology of slurry    solid content
出版日期:  2024-09-10      发布日期:  2024-09-30
ZTFLH:  TQ174  
基金资助: 国家自然科学基金(52130204; 52174376; 52202070);创新特区项目(23-TQ09-02-ZT-01-005);航空科学基金(20220042053001); 陕西省科技计划(2024GX-YBXM-220; 2024GX-YBXM-400; 2024GX-ZDCYL-03-03);广东省基础研究基金(2021B1515120028)
通讯作者:  *苏海军,西北工业大学材料学院教授、博士研究生导师。2003年西北工业大学材料科学与工程系本科毕业,同年9月在本校继续攻读硕士学位,2009年6月获西北工业大学材料加工工程专业博士学位,随后留校任教至今。长期从事先进定向凝固技术与理论及新材料研究工作,涉及高温合金、高熵合金、超高温复合陶瓷、生物陶瓷、钙钛矿太阳能电池、结构功能一体化复合材料以及定向凝固与增材制造技术等。国家优秀青年科学基金获得者、中国有色金属学会创新争先计划获得者,入选国家首批“香江学者”计划。发表 SCI论文 160余篇,授权中国发明专利 50 余项、美国发明专利1项,参编专著3部。获陕西高校科学技术研究优秀成果特等奖、陕西省科学技术一等奖、陕西省冶金科学技术一等奖、全国有色金属优秀青年科技奖和陕西省青年科技奖各1项。shjnpu@nwpu.edu.cn   
作者简介:  郝舒琪,2021年6月于南昌大学获得工学学士学位。现为西北工业大学材料学院硕士研究生,在苏海军教授的指导下进行研究。目前主要研究领域为共晶结构氧化物陶瓷的复杂结构成型。
引用本文:    
郝舒琪, 苏海军, 赵迪, 李翔, 董栋, 于佳俊. 粉体特性对光固化3D打印陶瓷浆料性质影响的研究进展[J]. 材料导报, 2024, 38(17): 23060075-10.
HAO Shuqi, SU Haijun, ZHAO Di, LI Xiang, DONG Dong, YU Jiajun. Research Progress on the Effect of Powder Characteristics on the Properties of Ceramic Slurry Based Stereolithography 3D Printing. Materials Reports, 2024, 38(17): 23060075-10.
链接本文:  
http://www.mater-rep.com/CN/10.11896/cldb.23060075  或          http://www.mater-rep.com/CN/Y2024/V38/I17/23060075
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