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材料导报  2020, Vol. 34 Issue (2): 2077-2082    https://doi.org/10.11896/cldb.18110100
  金属与金属基复合材料 |
选区激光熔化制备Ni-Cr-B-Si合金粉末的微观组织与性能
王文权, 李雅倩, 李欣, 刘亮, 陈飞
吉林大学材料科学与工程学院,长春 130025
Microstructures and Properties of Ni-Cr-B-Si Alloy Powders Prepared by Selective Laser Melting
WANG Wenquan, LI Yaqian, LI Xin, LIU Liang, CHEN Fei
School of Materials Science and Engineering,Jilin University,Changchun 130025,China
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摘要 由于模具在使用过程中极易出现镶块磨损和失效的情况,而一些进口模具镶块成本较高,本研究提出了一种新型的制备模具镶块的方法,为修复模具提供了一种新思路。本试验利用选区激光熔化工艺,选取不同工艺参数对粒度为21~60 μm 的Ni-Cr-B-Si合金粉末进行打印,最终分别得到表面粗糙度Ra≤3.5 μm和致密度为98.6%的立体试样。通过对合金试样表面形貌、微观组织和力学性能的研究与分析,得到激光能量密度对三者的影响规律。随激光能量密度的增大,试样的表面粗糙度先减小后增大,并在激光能量密度为78 J/mm3时获得表面质量最佳的试样。试样的耐磨性能与致密度呈现同样的变化趋势,二者均随激光能量密度的增大而增大,但过高的能量密度会导致试样边角产生开裂和翘曲,故80 J/mm3的激光能量密度最为适宜。选区激光熔化工艺具有快速冷却的特点,该特点使合金试样具有细小的微观组织,并且随能量密度的增大,试样的晶体生长形态从胞状树枝晶向等轴树枝晶转变。试样中基体相为FeNi3、γ-Ni和Ni3Si,主要强化相为M7C3、M23C6和Cr2B,在晶粒细化和强化相二者的共同作用下,试样具有较高的硬度和良好的耐磨性,显微硬度平均值达到848.1HV0.5。同等试验条件下,本试验制得的合金试样的耐磨性能显著优于常用的H13热作性模具钢。
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王文权
李雅倩
李欣
刘亮
陈飞
关键词:  Ni-Cr-B-Si合金粉末  选区激光熔化  表面形貌  微观组织  力学性能    
Abstract: Since the mold inserts are prone to failure in service processes, this study proposed a new method for preparing mold inserts. Ni-Cr-B-Si alloy powders specially manufactured were processed by selective laser melting (SLM) with different parameters in this research to obtain metal parts for mould repairing. It has been found that both the surface quality and relative density of the metal parts were improved with the increase of laser energy input. The metal part samples with fine surface roughness (Ra≤3.5 μm) and high relative density (98.6%) were obtained. Rapid melting and solidification in the SLM process resulted in fine gains and microstructures of the metal parts. The main phases of the microstructures included FeNi3, γ-Ni and Ni3Si, etc. and the strengthening phases such as M7C3, M23C6 and Cr2B in the SLM samples. The combination of fine grains with strengthening phases contributes to the excellent mechanical properties of the metal parts. The average microhardness of the SLM prepared metal parts could reach 848.1HV0.5. Correspondingly, the wear resistance of the metal parts was much better than that of the common hot-work die steel H13 under the same test conditions.
Key words:  Ni-Cr-B-Si alloy powders    selective laser melting    surface morphology    microstructures    mechanical properties
               出版日期:  2020-01-25      发布日期:  2020-01-03
ZTFLH:  TB36  
基金资助: 吉林省省校共建项目(440050316A14);温州市重大科技专项(ZG2017032);吉林省科技发展计划项目(20150520024JH)
通讯作者:  wwq@jlu.edu.cn   
作者简介:  王文权,吉林大学材料科学与工程学院教授,博士研究生导师。长期从事材料连接和材料表面改性领域的教学和科研工作。2010—2012年在长春轨道客车股份有限公司博士后工作站工作,2009年在德国亚琛大学表面工程研究所任访问学者,2007年在韩国釜山国立大学材料连接实验室任访问学者,2001年在日本JICA进行“钢材特性与应用”的专业项目研修。负责完成的“不锈钢车体结构激光焊接工艺研究”和“不锈钢车体CMT焊接工艺研究”项目成果在长春轨道客车股份有限公司得到了产业化应用。课题“等离子喷焊模具修复新材料开发与应用研究”在一汽集团锻造公司也得到了应用。发表了SCI与EI检索论文20余篇,负责完成科研项目17项,授权发明专利5项。
引用本文:    
王文权, 李雅倩, 李欣, 刘亮, 陈飞. 选区激光熔化制备Ni-Cr-B-Si合金粉末的微观组织与性能[J]. 材料导报, 2020, 34(2): 2077-2082.
WANG Wenquan, LI Yaqian, LI Xin, LIU Liang, CHEN Fei. Microstructures and Properties of Ni-Cr-B-Si Alloy Powders Prepared by Selective Laser Melting. Materials Reports, 2020, 34(2): 2077-2082.
链接本文:  
http://www.mater-rep.com/CN/10.11896/cldb.18110100  或          http://www.mater-rep.com/CN/Y2020/V34/I2/2077
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