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材料导报  2021, Vol. 35 Issue (24): 24062-24067    https://doi.org/10.11896/cldb.20090364
  无机非金属及其复合材料 |
低温玻璃钎料钎焊高体积分数SiCp/Al复合材料与电子玻璃的工艺及性能研究
楚军龙1, 高增1, 王振江1, 牛济泰1,2, 陶星空3
1 河南理工大学材料科学与工程学院,焦作 454003
2 河南晶泰航空航天高新材料科技有限公司,焦作 454003
3 大连理工大学材料科学与工程学院,大连 116024
Process and Properties of Brazing of High Volume SiCp/6063Al Composites and Electronic Glass with Low Temperature Glass Solder
CHU Junlong1, GAO Zeng1, WANG Zhenjiang1, NIU Jitai1,2, TAO Xingkong3
1 School of Materials Science and Engineering, Henan Polytechnic University, Jiaozuo 454003, China
2 Henan Jingtai High-Novel Materials Ltd. of Science and Technology, Jiaozuo 454003, China
3 School of Materials Science and Engineering, Dalian University of Technology, Dalian 116024, China
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摘要 本研究在大气环境下将PbO-ZnO-SiO2系非晶玻璃粉末和PbTiO3晶体粉末等比例混合均匀制得了复合玻璃钎料,实现了高体积分数SiCp/6063Al复合材料和DM305玻璃之间的连接。结果表明:当封接温度为480 ℃,保温30 min,复合玻璃钎料完成了预氧化后的复合材料与DM305玻璃之间的连接,接头无裂纹、气孔等缺陷,剪切强度为7.55 MPa,气密性为1×10-8 Pa·cm3/s,符合使用要求。在封接过程中,复合玻璃钎料与母材的氧化膜相溶,在复合材料一侧出现了Al元素的扩散现象。
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楚军龙
高增
王振江
牛济泰
陶星空
关键词:  SiCp/6063Al复合材料  DM305电子玻璃  复合玻璃钎料  力学性能    
Abstract: The composite glass brazing material prepared by mixing PbO-ZnO-SiO2 amorphous glass powder and PbTiO3 crystal powder uniformly in an atmospheric environment realizes the connection between high volume fraction SiCp/6063Al composite material and DM305 glass. The results show that when the sealing temperature is 480 ℃ and the holding time is 30 minutes, the composite glass brazing filler metal completes the connection between the pre-oxidized composite material and DM305 glass, the joint has no defects such as cracks and pores, and the shear strength is 7.55 MPa. The air tightness of 1×10-8 Pa·cm3/s meets the requirements of use. During the sealing process, the composite glass brazing filler metal is compatible with the oxide film of the base material, and Al element diffusion occurs on the side of the composite material.
Key words:  SiCp/6063Al    DM305 electronic glass    glass solder    mechanical properties
出版日期:  2021-12-25      发布日期:  2021-12-27
ZTFLH:  TG454  
基金资助: 河南省科技攻关项目(202102210036);中国博士后科学基金资助项目(2021M692891)
通讯作者:  mrgaozeng@163.com   
作者简介:  楚军龙,2018年6月毕业于河南理工大学,获得工学学士学位。现为河南理工大学材料科学与工程学院硕士研究生,在牛济泰教授的指导下从事铝基复合材料在电子封装材料领域的研究。高增,河南理工大学材料科学与工程学院讲师、硕士研究生导师。长期从事新型材料特种连接技术的基础理论与实际应用研究,尤其致力于复合材料的焊接、各类轻合金的绿色连接技术与数值仿真研究;参与国家自然科学基金1项,焦作市委托科研项目1项。近年来在国内外知名刊物上发表学术论文10余篇。
引用本文:    
楚军龙, 高增, 王振江, 牛济泰, 陶星空. 低温玻璃钎料钎焊高体积分数SiCp/Al复合材料与电子玻璃的工艺及性能研究[J]. 材料导报, 2021, 35(24): 24062-24067.
CHU Junlong, GAO Zeng, WANG Zhenjiang, NIU Jitai, TAO Xingkong. Process and Properties of Brazing of High Volume SiCp/6063Al Composites and Electronic Glass with Low Temperature Glass Solder. Materials Reports, 2021, 35(24): 24062-24067.
链接本文:  
http://www.mater-rep.com/CN/10.11896/cldb.20090364  或          http://www.mater-rep.com/CN/Y2021/V35/I24/24062
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