氧化锆受控影响因素及合成方法研究进展

doi:10.11896/cldb.25040096

材料导报

2026, Vol. 40

Issue (8): 25040096-15 https://doi.org/10.11896/cldb.25040096

无机非金属及其复合材料

氧化锆受控影响因素及合成方法研究进展

董正文¹, 常心如¹, 王锴², 周点翔¹, 陈帅¹, 郭耸^1,*

1 南京理工大学安全科学与工程学院,南京 210094
2 中国舰船研究设计中心,武汉 430064

Research Progress on Controlled Influencing Factors and Synthesis Methods of Zirconia

DONG Zhengwen¹, CHANG Xinru¹, WANG Kai², ZHOU Dianxiang¹, CHEN Shuai¹, GUO Song^1,*

1 School of Safety Science and Engineering, Nanjing University of Science and Technology, Nanjing 210094, China
2 China Ship Development and Design Center, Wuhan 430064, China

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摘要氧化锆(ZrO₂)纳米材料因优异的生物相容性、光电性能和力学性能以及较强的热稳定性和化学稳定性被应用于医学、航空航天、检测装置和先进陶瓷等领域。目前多种合成方法被应用于制备ZrO₂纳米材料,通过精细调控形成多元化结构以提升其使用性能。通过对近年来ZrO₂影响因素以及合成方法的相关文献进行整理,本文旨在为合成高性能ZrO₂提供参考。合成过程中ZrO₂性能受多方面因素的影响,如颗粒形貌、团聚程度以及结晶度等。通过调节合成参数(如反应时间、反应和煅烧温度、溶液pH值、前驱液种类等)论述影响ZrO₂性能的主要因素。此外,ZrO₂可通过多种方法进行合成,包括水热法、溶剂热法、溶胶凝胶法、化学气相沉积法以及微乳法,重点阐述不同方法合成ZrO₂的基本原理以及优势,最后与本文采用的预混滞止火焰合成法进行对比,从而进一步分析选择方法的不同对最终产物的影响。ZrO₂的合成技术将朝着更加高效、环保和精准的方向推进。一方面,新兴技术的不断涌现和交叉融合将催生出更多创新性的合成方法;另一方面,对ZrO₂性能的深入研究将推动其在新兴领域的应用拓展。同时,如何降低合成成本、提高生产效率、实现大规模工业化生产也将是未来需要解决的关键问题。

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	董正文
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	陈帅
	郭耸

关键词: 氧化锆合成方法纳米材料形貌控制

Abstract: Zirconia (ZrO₂) nanomaterials are utilized across diverse fields, including medicine, aerospace, detection devices, and advanced ceramics, owing to their outstanding biocompatibility, optoelectronic properties, and mechanical performance, as well as excellent thermal stability and chemical stability. Currently, multiple synthesis techniques are employed to prepare ZrO₂ nanomaterials, with precise control to form diverse structures for enhancing their service performance. This paper compiles relevant recent literature on the influencing factors and synthesis methods of ZrO₂ in recent years, aiming to provide a reference for synthesizing high-performance ZrO₂. During synthesis, the properties of ZrO₂ are in-fluenced by multiple factors, such as particle morphology, degree of agglomeration, and crystallinity. The main influencing factors of ZrO₂ performance are discussed by adjusting synthesis parameters (including reaction time, reaction and calcination temperatures, solution pH value, and types of precursor solution). Furthermore, ZrO₂ can be synthesized through various methods, including hydrothermal method, solvothermal method, sol-gel method, chemical vapor deposition method, and microemulsion method. This paper focuses on elucidating the basic principles and respective advantages of synthesizing ZrO₂ using these different methods. Finally, a comparison with the premixed stagnation flame synthesis method adopted in this paper is conducted to further analyze the impact of different synthetic method selection on the final product. The synthesis technology of ZrO₂ will advance towards a more efficient, environmentally friendly and precise direction. On the one hand, with the conti-nuous emergence and cross-integration of emerging technologies, more innovative synthesis methods will be fostered. On the other hand, in-depth research on the properties of ZrO₂ will drive the expansion of its applications in emerging fields. Meanwhile, how to reduce synthesis costs, improve production efficiency and realize large-scale industrial production will also be the key issues to be solved in the future.

Key words: zirconia synthesis method nanomaterial topography control

出版日期: 2026-04-25 发布日期: 2026-05-06

ZTFLH:

X932

基金资助: 国家自然科学基金(52474234);江苏省研究生科研与实践创新计划项目(SJCX24_0157;KYCX25_0682)

通讯作者: * 郭耸,南京理工大学安全科学与工程学院博士研究生导师。目前主要研究领域为危险物质热行为应用及燃爆危险性防控技术。guosong@njust.edu.cn

作者简介: 董正文,南京理工大学安全科学与工程学院研究生,在郭耸教授的指导下研究气溶胶颗粒火焰合成。

引用本文:

董正文, 常心如, 王锴, 周点翔, 陈帅, 郭耸. 氧化锆受控影响因素及合成方法研究进展[J]. 材料导报, 2026, 40(8): 25040096-15.
DONG Zhengwen, CHANG Xinru, WANG Kai, ZHOU Dianxiang, CHEN Shuai, GUO Song. Research Progress on Controlled Influencing Factors and Synthesis Methods of Zirconia. Materials Reports, 2026, 40(8): 25040096-15.

链接本文:

https://www.mater-rep.com/CN/10.11896/cldb.25040096 或 https://www.mater-rep.com/CN/Y2026/V40/I8/25040096

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