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《材料导报》期刊社  2017, Vol. 31 Issue (16): 26-30    https://doi.org/10.11896/j.issn.1005-023X.2017.016.006
  材料研究 |
通过改进的制备工艺提高FINEMET纳米晶磁粉芯的磁性能及其机理*
李庆达1, 郭建永1, 胡军1, 王宏立1, 连法增2, 陆曹卫3
1 黑龙江八一农垦大学工程学院, 大庆 163319;
2 东北大学材料各向异性与织构教育部重点实验室, 沈阳 110004;
3 安泰科技股份有限公司,北京 100081
Improving the Performance of FINEMET Nanocrystalline Magnetic Powder Core by a Revamped Process and the Corresponding Mechanism
LI Qingda1, GUO Jianyong1, HU Jun1, WANG Hongli1, LIAN Fazeng2, LU Caowei3
1 College of Engineering,Heilongjiang August First Land Reclamation University, Daqing 163319;
2 Key Laboratory for Anisotropy and Texture of Materials of Ministry of Education, Northeastern University, Shenyang 110004;
3 Advance Technology and Materials Co., Ltd., Beijing 100081
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摘要 通过对比实验研究了改进的制备工艺下FINEMET纳米晶磁粉芯的磁性能,并探讨了其相应的物理机制。采用扫描电镜、透射电镜和X射线衍射仪检测磁粉的表面形貌、内部结构和晶格畸变,采用B-H分析仪检测磁粉芯的动态磁性能。结果表明,改进的制备工艺能够有效降低磁粉芯的损耗,提高磁导率和频率应用范围。延长非晶粉末的球磨时间能够降低磁粉芯的磁滞损耗和涡流损耗,最佳的球磨时间为8 h。通过对比磁粉的晶格畸变,发现通过改进工艺制备的磁粉的晶格畸变相对较小,该工艺提高磁性能的原因在于磁粉残余内应力的有效释放。
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李庆达
郭建永
胡军
王宏立
连法增
陆曹卫
关键词:  FINEMET  磁粉芯  退火  损耗  磁导率  改进的制备工艺    
Abstract: The magnetic property of FINEMET nanocrystalline magnetic powder core prepared by a revamped process was studied through comparative experiments, and the corresponding physical mechanism was observed. Scanning electron microscopy, transmission electron microscopy and X-ray diffraction were used to characterize the morphology, internal structure and lattice deformation of magnetic powders, B-H analyzer was used to characterize magnetic properties of magnetic powder core. The results showed that the revamped process could effectively reduce the loss of the magnetic powder core, and promote magnetic permeability and frequency range. The hysteresis loss and eddy current loss could be decreased by increasing milling time, and the optimum mil-ling time was 8 h. Our experiments found that the magnetic powders produced by the revamped process possess a relatively low lattice deformation, which means that the effective release of the remnant internal stress leads to the improve of magnetic powder core′s performance.
Key words:  FINEMET    magnetic powder core    annealing    loss    permeability    revamped process
出版日期:  2017-08-25      发布日期:  2018-05-07
ZTFLH:  TM271.2  
  TM272  
基金资助: 黑龙江省自然科学基金(QC2014C058); 黑龙江省普通高等学校青年学术骨干支持计划(1252G042); 黑龙江八一农垦大学引进人才科研启动基金(2010)
作者简介:  李庆达:男,1982年生, 博士, 副教授, 主要研究方向为金属软磁材料及器件 E-mail:liqingda23@126.com
引用本文:    
李庆达, 郭建永, 胡军, 王宏立, 连法增, 陆曹卫. 通过改进的制备工艺提高FINEMET纳米晶磁粉芯的磁性能及其机理*[J]. 《材料导报》期刊社, 2017, 31(16): 26-30.
LI Qingda, GUO Jianyong, HU Jun, WANG Hongli, LIAN Fazeng, LU Caowei. Improving the Performance of FINEMET Nanocrystalline Magnetic Powder Core by a Revamped Process and the Corresponding Mechanism. Materials Reports, 2017, 31(16): 26-30.
链接本文:  
https://www.mater-rep.com/CN/10.11896/j.issn.1005-023X.2017.016.006  或          https://www.mater-rep.com/CN/Y2017/V31/I16/26
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