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材料导报  2026, Vol. 40 Issue (4): 25020087-6    https://doi.org/10.11896/cldb.25020087
  金属与金属基复合材料 |
QBe2弹簧管表面黄斑成因分析及调控可行性研究
朱亮1, 葛声宏2,3, 沈琪峰3, 吴恒3, 陶海军1,*
1 南京航空航天大学材料科学与技术学院,南京 211106
2 南京航空航天大学机电学院,南京 210016
3 中航工业南京伺服控制系统有限公司,南京 211100
Cause Analysis and Regulation Feasibility of the Yellow Spots on the Surface of QBe2 Spring Tubes
ZHU Liang1, GE Shenghong2,3, SHEN Qifeng3, WU Heng3, TAO Haijun1,*
1 College of Materials Science and Technology, Nanjing University of Aeronautics and Astronautics, Nanjing 211106, China
2 College of Mechanical and Electrical Engineering, Nanjing University of Aeronautics and Astronautics, Nanjing 210016, China
3 AVIC Nanjing Servo Control System Co., Ltd., Nanjing 211100, China
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摘要 某公司采用国产QBe2棒材生产伺服弹簧管,在最终检验中发现其薄壁处存在黄斑,严重影响弹簧管的外观质量及使用性能。针对此问题,本工作采用扫描电子显微镜(SEM)、电子探针显微分析仪(EPMA)及透射电子显微镜(TEM)等表征、分析了黄斑的形成原因,并探究均匀化退火工艺对其调控的可行性。研究发现:零件表面黄斑为β相,其存在形态不受制造过程中的机加工、热处理工艺的影响,测试表明其在硬态(固溶+拉拔态)原材料棒材中已存在。后期采用605 ℃下6 h的预退火+860 ℃下100 h的均匀化退火,可以促进原材料中β相的Be元素扩散,从而达到消除β相的目的。
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朱亮
葛声宏
沈琪峰
吴恒
陶海军
关键词:  弹簧管  QBe2  β相  原位表征  均匀化退火    
Abstract: The domestic QBe2 bar was used to produce servo spring tube by a company. In the final inspection, it was found that there was macula in the thin wall, which seriously affected the appearance quality and performance of the spring tube. To explore the above problems, scanning electron microscope (SEM), electron probe microanalyzer (EPMA) and transmission electron microscope (TEM) were used to characterize and analyze the causes of macular formation, and explore the feasibility of homogenization annealing process on its regulation. It is found that the macula on the surface of the part is β phase, and its existing form is not affected by the machining and heat treatment process in the manufactu-ring process. The test results show that it already exists in the hard (solid solution+drawing) raw material bar. In the later stage, pre-annealing at 605 ℃ for 6 h+homogenization annealing at 860 ℃ for 100 h can promote the diffusion of be element in β phase in raw materials, so as to achieve the purpose of eliminating β phase.
Key words:  spring tube    QBe2    β phase    in-situ characterization    homogenization annealing
出版日期:  2026-02-25      发布日期:  2026-02-13
ZTFLH:  TG164.1  
  TG166.2  
通讯作者:  * 陶海军,博士,南京航空航天大学材料科学与技术学院副教授、硕士研究生导师,主要研究领域为纳米光电材料、材料微观缺陷、材料缺陷钝化技术。taohaijun@nuaa.edu.cn   
作者简介:  朱亮,南京航空航天大学材料科学与技术学院硕士研究生,主要研究领域为有色金属材料。
引用本文:    
朱亮, 葛声宏, 沈琪峰, 吴恒, 陶海军. QBe2弹簧管表面黄斑成因分析及调控可行性研究[J]. 材料导报, 2026, 40(4): 25020087-6.
ZHU Liang, GE Shenghong, SHEN Qifeng, WU Heng, TAO Haijun. Cause Analysis and Regulation Feasibility of the Yellow Spots on the Surface of QBe2 Spring Tubes. Materials Reports, 2026, 40(4): 25020087-6.
链接本文:  
https://www.mater-rep.com/CN/10.11896/cldb.25020087  或          https://www.mater-rep.com/CN/Y2026/V40/I4/25020087
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