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材料导报  2021, Vol. 35 Issue (18): 18131-18135    https://doi.org/10.11896/cldb.20070291
  金属与金属基复合材料 |
爆炸焊接Nb/Q345R层状复合材料的热震性能研究
宋晓毓1, 王德志1, 吴壮志1, 段柏华1, 毕海莲2, 刘新利1
1 中南大学材料科学与工程学院,长沙 410083
2 黄山学院化学化工学院, 黄山 245041
Research on Thermal Shock Performance of Nb/Q345R Laminated Composite Fabricated by Explosive Welding
SONG Xiaoyu1, WANG Dezhi1, WU Zhuangzhi1, DUAN Bohua1, BI Hailian2, LIU Xinli1
1 Materials Science and Engineering, Central South University, Changsha 410083, China
2 School of Chemistry and Chemical Engineering, Huangshan University, Huangshan 245041, China
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摘要 铌作为一种难熔金属,具有熔点高、塑性好、抗酸和抗液态金属腐蚀能力强等特性,被广泛应用于电子、机械、航空航天等领域。本工作研究了爆炸焊接Nb/Q345R层状复合材料的热震性能,通过将Nb/Q345R试样在氢气中分别加热到800 ℃和1 000 ℃后迅速冷却完成一次热震,研究材料在进行10次、30次、50次热震循环后,试样的界面组织形貌及其结合强度的变化,进而评价其热震性能。采用X射线衍射(XRD)、扫描电子显微镜(SEM)等表征手段分析材料成分和界面组织形貌的变化,并通过压缩剪切试验测量层状复合材料的界面结合强度。研究结果表明,在800 ℃热震10次时,层状材料界面处开始产生微裂纹,而在1 000 ℃热震50次时,材料界面处裂纹沿界面扩展、延伸,导致界面结合强度显著降低,降低至材料本身结合强度的13.22%。
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宋晓毓
王德志
吴壮志
段柏华
毕海莲
刘新利
关键词:  爆炸焊接Nb/Q345R  层状复合材料  热震性能  压缩剪切试验  界面组织与性能    
Abstract: As a refractory metal, niobium has the characteristics of high melting point, good plasticity, strong acid resistance and liquid metal corrosion resistance, and is widely used in electronics, machinery, aerospace and other fields. This paper studies the thermal shock performance of the Nb/Q345R laminated composite fabricated by explosive welding material. The Nb/Q345R sample is heated to 800 ℃ and 1 000 ℃ in hydrogen and then rapidly cooled to complete a thermal shock. After 10, 30, 50 thermal shock cycles, the interface structure and bonding strength of the sample changed, and then the thermal shock performance was evaluated. X-ray diffraction (XRD), scanning electron microscopy (SEM) and other characterization methods are used to analyze the changes in material composition and interface structure morphology, and the interfacial bonding strength of layered composites is measured through compression shear tests. The research results show that at 800°C for 10 thermal shock cycles, microcracks begin to occur at the interface of the layered material, and at 1 000 ℃ for 50 cycles, the cracks at the material interface expand and extend along the interface, resulting in a significant reduction in the interface bonding strength. Reduced to 13.22% of the bonding strength of the material itself.
Key words:  explosive welding Nb/Q345R    laminated composite material    thermal shock performance    compression shear test    interface structure and property
               出版日期:  2021-09-25      发布日期:  2021-09-30
ZTFLH:  TB331  
基金资助: 国家重点研发计划资助(2018YFC1901700)
作者简介:  宋晓毓,中南大学硕士研究生,2018年毕业于中南大学,获工学学士学位。主要从事难熔金属回收利用方面的研究。
刘新利,中南大学副教授,硕士研究生导师,2015年毕业于中南大学材料学专业,获博士学位。主要从事难熔金属相关材料的开发及回收,粉末冶金多孔材料等方面的基础与应用研究。已在国内外科技刊物上发表论文50余篇,申请专利12项,获授权专利3项。
引用本文:    
宋晓毓, 王德志, 吴壮志, 段柏华, 毕海莲, 刘新利. 爆炸焊接Nb/Q345R层状复合材料的热震性能研究[J]. 材料导报, 2021, 35(18): 18131-18135.
SONG Xiaoyu, WANG Dezhi, WU Zhuangzhi, DUAN Bohua, BI Hailian, LIU Xinli. Research on Thermal Shock Performance of Nb/Q345R Laminated Composite Fabricated by Explosive Welding. Materials Reports, 2021, 35(18): 18131-18135.
链接本文:  
http://www.mater-rep.com/CN/10.11896/cldb.20070291  或          http://www.mater-rep.com/CN/Y2021/V35/I18/18131
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