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《材料导报》期刊社  2018, Vol. 32 Issue (4): 515-519    https://doi.org/10.11896/j.issn.1005-023X.2018.04.001
  材料研究 |
基于胶体晶体构筑银纳米薄膜及其抑制微放电性能研究
白园蕊1, 2, 马建中1, 2, 刘俊莉3, 鲍艳1, 2, 崔万照4, 胡天存4, 吴朵朵2, 5
1 陕西科技大学轻工科学与工程学院,西安 710021;
2 陕西农产品加工技术研究院,西安 710021;
3 陕西科技大学 材料科学与工程学院,西安 710021;
4 中国空间技术研究院西安分院,空间微波技术重点实验室,西安 710100;
5 陕西科技大学化学与化工学院,西安 710021
Construction of Silver Film by Colloidal Crystal Template and Its Micro-discharge Inhibition Performance
BAI Yuanrui1, 2, MA Jianzhong1, 2, LIU Junli3, BAO Yan1, 2, CUI Wanzhao4, HU Tiancun4, WU Duoduo2, 5
1 College of Bioresources Chemical and Materials Engineering, Shaanxi University of Science and Technology, Xi'an 710021;
2 Shaanxi Research Institute of Agricultural Products Processing Technology, Xi'an 710021;
3 School of Materials Science and Engineering, Shaanxi University of Science and Technology, Xi'an 710021;
4 National Laboratory of Science and Technology on Space Microwave, China Academy of Space Technology(Xi'an), Xi'an 710100;
5 College of Chemistry and Chemical Engineering, Shaanxi University of Science and Technology,Xi'an 710021;
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摘要 近年来,微放电效应的抑制研究在加速器、大功率微波器件等领域得到了广泛的关注。采用聚苯乙烯(PS)胶体晶体模板辅助磁控溅射法制备了类空心球结构的银薄膜,通过调节PS模板尺寸及溅射时间(镀银层厚度),得到具有抑制微放电效应的银薄膜。采用SEM表征银薄膜的形貌与结构,并用二次电子发射系数(SEY)测试平台表征银薄膜的SEY。结果表明,PS模板尺寸及溅射时间对银薄膜形貌及其二次电子抑制作用有显著的影响,当溅射时间为600 s,模板尺寸为1 000 nm时,银薄膜的SEY较小,即对二次电子的抑制作用较为显著,与初始镀银铝合金样品相比,其SEY值降低了48%。
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白园蕊
马建中
刘俊莉
鲍艳
崔万照
胡天存
吴朵朵
关键词:  PS胶体晶体  磁控溅射  银薄膜  二次电子发射系数  抑制    
Abstract: In recent years, multipactor suppression has been widely concerned in the accelerator, high-power microwave devices and other related fields. In this study, hollow sphere-like silver film was obtained via magnetron sputtering assisted by polystyrene (PS) colloidal crystal template. The second electron suppression effect of the silver film was adjusted by the size of PS template and the sputtering time (thickness of the silver layer). The morphology of silver films was characterized by SEM,and the SEY of silver films was characterized by secondary electron emission (SEY) test platform. The results show that size of PS template and sputtering time have significant effect on the morphology of silver film and its secondary electron suppression. When the sputtering time was 600 s and the template size was 1 000 nm, the maximum SEY of the silver film was relatively low, which meant the second electron suppression effect was more significant. Compared with the initial silver-plated aluminum alloy samples, the SEY value decreased by 48%.
Key words:  PS colloidal crystal    magnetron sputtering    silver film    secondary electron emission    suppression
出版日期:  2018-02-25      发布日期:  2018-02-25
ZTFLH:  TB34  
基金资助: 国家自然科学基金(21376145); 国家自然科学基金重点项目(U1537211); 陕西科技大学科研创新团队资助项目(TD12-03)
通讯作者:  马建中,男,1960年生,教授,主要研究方向为有机/无机纳米杂化材料的制备 E-mail:majz@sust.edu.cn;刘俊莉,女,1986年生,讲师,研究方向为有机-无机纳米复合材料的合成及应用 E-mail:liujunli042@163.com   
作者简介:  白园蕊:女,1992年生,硕士,主要研究方向为纳米涂层 E-mail:780656336@qq.com
引用本文:    
白园蕊, 马建中, 刘俊莉, 鲍艳, 崔万照, 胡天存, 吴朵朵. 基于胶体晶体构筑银纳米薄膜及其抑制微放电性能研究[J]. 《材料导报》期刊社, 2018, 32(4): 515-519.
BAI Yuanrui, MA Jianzhong, LIU Junli, BAO Yan, CUI Wanzhao, HU Tiancun, WU Duoduo. Construction of Silver Film by Colloidal Crystal Template and Its Micro-discharge Inhibition Performance. Materials Reports, 2018, 32(4): 515-519.
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https://www.mater-rep.com/CN/10.11896/j.issn.1005-023X.2018.04.001  或          https://www.mater-rep.com/CN/Y2018/V32/I4/515
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