INORGANIC MATERIALS AND CERAMIC MATRIX COMPOSITES |
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Research Progress in MAX Phase Ti3SiC2 Highly Conductive Coating |
ZHU Jie, ZHANG Fangzhou, XIE Youju, JIA Lintao, WANG Mengqian, LI Aijun
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Institute of Materials, School of Materials Science and Engineering, Shanghai University, Shanghai 200444, China |
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Abstract Ti3SiC2(TSC) is a new type of ternary compound MAX phase with excellent properties of both metallic and ceramic materials. Ti3SiC2 as a high conductive coating with great application potential has attracted more and more attention in recent years. The preparation technologies of Ti3SiC2 coating are constantly being reformed and optimized. There're mainly five common processes to prepare Ti3SiC2 coating, including chemical vapor deposition (CVD), physical vapor deposition (PVD), solid-state reaction, aerosol deposition method (ADM) and thermal sp-raying, respectively. The properties of Ti3SiC2 coatings are closely related to their purity to a large extent. Usually, a certain degree of impurities are contained in Ti3SiC2 coating, which has become an important factor restricting its wide application. It is found that the impurities in Ti3SiC2 coating are mainly TiC, Ti5Si3, SiC, TiSi2, etc. More over, the kinds of impurities produced by different methods are different. In order to improve the purity of Ti3SiC2 coating, it is necessary to explore and optimize the preparation process. At present, reactive chemical vapor deposition (RCVD) has realized the growth of pure Ti3SiC2 coating on graphite substrate by consuming silicon carbide (SiC) sublayer. Besides, ADM has also produced pure Ti3SiC2 coatings at room temperature, which reduces the synthesis temperature of conventional Ti3SiC2 coating. In addition, PVD technology not only provides the possibility of synthesizing Ti3SiC2 coating at low temperature, but also realizes the industrial production of Ti-Si-C composite coating. This paper comprehensively reviews the recent research on Ti3SiC2. The unique crystal structure and excellent properties of Ti3SiC2 coating are discussed. The different ways to prepare Ti3SiC2 coating were analyzed and current challenges in the synthesis of pure Ti3SiC2 coating were also introduced. Furthermore, the current and potential applications of Ti3SiC2 coating has been summarized. Overall, the analyses and discussions of various Ti3SiC2 coating synthesis technologies in this review will be contributed to synthesis of high purity Ti3SiC2 coating in the future.
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Published: 10 December 2021
Online: 2021-12-23
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Fund:National Natural Science Foundation of China (21676163, 51602189) |
Corresponding Authors:
zhangfzh@shu.edu.cn;aijun.li@shu.edu.cn
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About author: Jie Zhu received his B.E. degree in metal materials and engineering from Nanjing Institute of Technelogy in 2017. He is currently a postgraduate student in the School of Materials Science and Engineering, Shanghai University under the supervision of Prof. Aijun Li. His research has focused on depositing Ti3SiC2 coating by chemical vapor deposition. Fangzhou Zhang is an assistant researcher in School of Materials and Engineering of Shanghai University. In 2014, he graduated from the Ecole Normale Superieur de Cachan. After graduation, he worked in Aerospace Research Institute of Materials & Processing Technology and Shanghai University. In the past five years, he has successively obtained Technology Foundation for Selec-ted Overseas Chinese Scholar, National Natural Science Foundation of China, and Key Laboratory foundation of Equipment Development Department of the Central Military Commission. As the first author or the corresponding author, he published 6 SCI papers in academic journals including Nano Energy, Journal of Composite Material, etc. At present, he is mainly engaged in the research on the mechanical properties and behaviors of ceramic matrix composite materials. Aijun Li is currently a professor at the School of Mate-rials Science and Engineering at the Shanghai University (SHU). He received his Ph.D. degree in materials science from Northwestern Polytechnical University in 2004. He worked as a senior scientist and then a group leader for carbon materials at the Karlsruhe Institute of Technology (KIT), in Germany from 2010 to 2015, being involved with the research, development and application of composites. His main research interests are in the complex interactions of multi-physical and chemical phenomena involved in chemically reacting flows, mainly focusing on modeling, simulation and synthesis of composites by chemical vapor infiltration/deposition processes. |
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