METALS AND METAL MARTIX COMPOSITES |
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The Influence of Micro-arc Oxidation Time on the Surface Morphology andProperties of Ceramic Coating Developed on TA15 Alloy |
WANG Xian, YU Sirong, ZHAO Yan, ZHANG Peng, LIU Enyang, XIONG Wei
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College of Materials Science and Engineering, China University of Petroleum, Qingdao 266580 |
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Abstract Dense ceramic coatings were fabricated on TA15 by micro-arc oxidation for improving its hardness and corrosion resistance with NaAlO2, NaF and KOH as electrolyte. Surface morphology, chemical composition and phase composition of coatings were analyzed. Microhardness, surface roughness and corrosion resistance of coatings for different oxidation time were investigated. The results show that tiny honeycomb-like micro-nano pores could be seen on coatings. With the increase of oxidation time, the surface of coatings gradually became smooth. When the time was too long, pits, bulges and other defects were appeared. The surface roughness of the coatings firstly decreased and then increased. The coating was composed of TiO2, Al2O3 and Al2Ti3 phases. The surface microhardness of the coating always increased with the increase of oxidation time. The microhardness of the 50 min treated coating was 332.82HV, which increased by 59.2% compared to the matrix. The corrosion potential of the 40 min treated coating was +222.24 mV, which was 530 mV higher than that of the matrix. The corrosion current density of the 40 min treated coating was 1.73×10-9 A/cm2, which was reduced to 3% of the matrix. The 40 min treated coating exhibited the best corrosion resistance.
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Published: 31 May 2019
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Fund:This work was financially supported by the Natural Science Foundation of Shandong Province of China (ZR2017LEM004),the Open Fund of Key Laboratory of Oil & Gas Equipment, Ministry of Education (Southwest Petroleum University) (OGE201702-07), and the Fundamental Research Funds for the Central Universities (18CX02091A, 17CX06051). |
About author:: Xian Wang,Master of Materials Science and Enginee-ring from China University of Petroleum, from September 2016 to July 2019, is engaged in the research of titanium alloys and surface modification.Yan Zhao,Urgently-needed Talent of Qingdao, received his Ph.D. degree from materials processing engineering major of Northwest Polytechnic University in 2013 and then taught in China University of Petroleum as a lecturer. He focuses on the research of advanced metal materials and processing technology and has rich experience in titanium research. He has published 10 academic papers as the first author, including 4 indexed by SCI and 6 indexed by EI. |
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