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材料导报  2018, Vol. 32 Issue (18): 3208-3212    https://doi.org/10.11896/j.issn.1005-023X.2018.18.019
  金属与金属基复合材料 |
不同温度下Sn-0.7Cu钎料在非晶Fe84.3Si10.3B5.4合金上的润湿行为及界面特征
侯斌1, 刘凤美1, 王宏芹2, 李琪1, 万娣1, 张宇鹏1
1 广东省焊接技术研究所(广东省中乌研究院),广东省现代焊接技术重点实验室,广州 510650;
2 工业和信息化部电子第五研究所可靠性研究分析中心,广州 510610
Wetting Behavior and Interfacial Characteristics of Sn-0.7Cu Solder on Amorphous Fe84.3Si10.3B5.4 Alloy at Different Temperatures
HOU Bin1, LIU Fengmei1, WANG Hongqin2, LI Qi1, WAN Di1, ZHANG Yupeng1
1 Guangdong Provincial Key Laboratory of Advanced Welding Technology, Guangdong Welding Institute (China-Ukraine E.O.Paton Institute of Welding), Guangzhou 510650;
2 Reliability Research and Analysis Center, The Fifth Research Institute of MITT, P. R, Guangzhou 510610
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摘要 采用座滴法及利用SEM-EDS分别对Sn、Sn-37Pb、Sn-58Bi和Sn-0.7Cu四种钎料在非晶Fe84.3Si10.3B5.4合金上的静态润湿及界面特征进行了对比研究,优选出Sn-0.7Cu钎料作为适用于非晶Fe84.3Si10.3B5.4合金的焊接钎料。进而采用座滴法研究了不同温度下Sn-0.7Cu钎料在非晶Fe84.3Si10.3B5.4合金上的动态润湿行为,并利用SEM-EDS观察分析了其在非晶Fe84.3Si10.3B5.4合金表面润湿后的界面微观组织形貌及成分。结果表明,Sn-0.7Cu钎料在非晶Fe84.3Si10.3B5.4合金上的最终平衡润湿角随着温度的升高而变小,润湿性越来越好;同时Sn-0.7Cu与非晶Fe84.3Si10.3B5.4合金界面上形成的FeSn2金属间化合物由间断分布变为连续分布,且其厚度逐渐增加,界面反应逐渐增强。
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侯斌
刘凤美
王宏芹
李琪
万娣
张宇鹏
关键词:  Sn-Cu钎料  非晶Fe84.3Si10.3B5.4合金  润湿行为  界面反应    
Abstract: The sessile drop method and scanning electron microscopy (SEM) and energy dispersive spectrometer (EDS) was used to study the static wetting and interfacial microstructure morphology of Sn, Sn-37Pb, Sn-58Bi and Sn-0.7Cu on amorphous Fe84.3Si10.3B5.4substrate. The research results showed that Sn-0.7Cu alloy was selected as better solder for amorphous Fe84.3Si10.3B5.4alloy. The wetting behavior of Sn-0.7Cu solder on amorphous Fe84.3Si10.3B5.4alloy at different temperatures was investigated by sessile drop method. The microstructure morphology and composition of Sn-0.7Cu solder/amorphous alloy substrate interface was analyzed by SEM and EDS. With increasement of soldering temperature, the final equilibrium wetting angle of Sn-0.7Cu solder on amorphous Fe84.3Si10.3B5.4 alloy substrate was getting smaller and smaller, and the wettability was better. At the same time, the thickness of intermetallic compound (FeSn2) forming at the interface between Sn-0.7Cu solder and amorphous Fe84.3Si10.3B5.4 alloy substrate gradually increased which was from discontinuous to continuous distribution, and the interfacial reaction increased gradually.
Key words:  Sn-Cu solder    amorphous Fe84.3Si10.3B5.4 alloy    wetting behavior    interfacial reaction
                    发布日期:  2018-10-18
ZTFLH:  TG425+.1  
基金资助: 国家重点研发计划(2017YFB0305700);国家自然科学基金青年基金项目(51304176;51405092);广州市科技计划项目(对外科技合作)(201807010028);广东省焊接产业技术创新联盟示范建设产学研合作项目(2014B090907007)
作者简介:  侯斌:男,1989年生,硕士,工程师,主要从事钎焊扩散焊方面的研究 E-mail:houb@gwi.gd.cn
引用本文:    
侯斌, 刘凤美, 王宏芹, 李琪, 万娣, 张宇鹏. 不同温度下Sn-0.7Cu钎料在非晶Fe84.3Si10.3B5.4合金上的润湿行为及界面特征[J]. 材料导报, 2018, 32(18): 3208-3212.
HOU Bin, LIU Fengmei, WANG Hongqin, LI Qi, WAN Di, ZHANG Yupeng. Wetting Behavior and Interfacial Characteristics of Sn-0.7Cu Solder on Amorphous Fe84.3Si10.3B5.4 Alloy at Different Temperatures. Materials Reports, 2018, 32(18): 3208-3212.
链接本文:  
http://www.mater-rep.com/CN/10.11896/j.issn.1005-023X.2018.18.019  或          http://www.mater-rep.com/CN/Y2018/V32/I18/3208
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