Please wait a minute...
《材料导报》期刊社  2017, Vol. 31 Issue (2): 69-72    https://doi.org/10.11896/j.issn.1005-023X.2017.02.015
  材料研究 |
高体积比SiCp/6063Al复合材料的铝基钎料制备及钎焊工艺研究*
王鹏1, 高增1, 李锦竹1, 程东锋1, 徐冬霞1, 牛济泰1,2
1 河南理工大学材料科学与工程学院, 焦作 454003;
2 河南晶泰航空航天高新材料科技有限公司, 焦作 454003;
Preparation of Aluminum Base Filler Metals and Brazing Processes of 6063Al Matrix Composites with High SiC Content
WANG Peng1, GAO Zeng1, LI Jinzhu1, CHENG Dongfeng1, XU Dongxia1, NIU Jitai1,2
1 School of Material Science and Engineering, Henan Polytechnic University, Jiaozuo 454003;
2 Henan Jingtai High-Novel Materials Ltd. of Science and Technology, Jiaozuo 454003;
下载:  全 文 ( PDF ) ( 1697KB ) 
输出:  BibTeX | EndNote (RIS)      
摘要 采用快速甩带技术制备了(Al-10Si-20Cu-0.05Ce)-1Ti (质量分数/%)急冷箔状钎料,并对60%体积分数的SiCp/6063Al复合材料进行真空钎焊实验,然后对钎料及接头的显微组织与性能进行测定和分析。结果表明,急冷钎料的微观组织细小、成分均匀,厚80~90 μm,主要包含Al、CuAl2、Si和Al2Ti等相。当升高钎焊温度(T/℃)或延长保温时间(t/min),SiCp/钎料界面的润湿性改善,6063Al基体/钎料间互扩散和溶解作用增强,接头连接质量逐渐提高。当T=590 ℃、t=30 min时,接头抗剪强度达到112.6 MPa;当T=590 ℃、t=50 min时,少量小尺寸SiCp因液态钎料排挤而分散于钎缝,因加工硬化而使接头强度递增7.3%。然而,当T≥595 ℃、t≥60 min时,SiCp偏聚于钎缝,导致接头组织恶化,且剪切断裂以脆性断裂为主。综合考虑钎焊成本与接头强度使用要求,确定最佳钎焊工艺为590 ℃、30 min。
服务
把本文推荐给朋友
加入引用管理器
E-mail Alert
RSS
作者相关文章
王鹏
高增
李锦竹
程东锋
徐冬霞
牛济泰
关键词:  SiCp/Al复合材料  钎料  剪切强度  断口    
Abstract: Using (Al-10Si-20Cu-0.05Ce)-1Ti (wt%) filler metal foil prepared by rapidly melt-spun technique, compacted joints of SiCp/6063Al composites with 60% SiC content were obtained, and then their microstructure and properties were analyzed. Results indicated that the rapidly-cooled foils with thickness of 80-90 μm presented fine and uniform microstructure, and the foils mainly composed of Al, Cu2Al, Si and Al2Ti. With increasing brazing temperature or prolonging soaking time, the bonding quality of joints were gradually improved because of better wettability on the SiCp/filler interface and sufficient interdiffusion and dissolution between 6063Al/filler metal. The shear strength reached 112.6 MPa at 590 ℃ with soaking time of 30 min. When soaking time was prolonged to 50 min, the shear strength increased 7.3% due to work hardening of a composite seam, which was formed by small-size SiC particles migration and dispersion. However, when brazing temperature was higher than 595 ℃ and soaking time was longer than 60 min, the seam would be deteriorated seriously by segregation of SiC particles and which would lead to brittle fracture. Taking both the brazing cost and shearing strength of joint into consideration, the optimum brazing process is determined with temperature of 590 ℃ and soaking time of 30 min.
Key words:  SiCp/Al composites    filler metal    shear strength    fracture appearance
               出版日期:  2017-01-25      发布日期:  2018-05-02
ZTFLH:  TG454  
基金资助: *国家自然科学基金(51245008); 河南省高等学校重点科研项目计划(15A430007)
作者简介:  王鹏:男,1987年生,博士研究生,研究方向为复合材料先进连接技术 E-mail:wangpeng88626@163.com
引用本文:    
王鹏, 高增, 李锦竹, 程东锋, 徐冬霞, 牛济泰. 高体积比SiCp/6063Al复合材料的铝基钎料制备及钎焊工艺研究*[J]. 《材料导报》期刊社, 2017, 31(2): 69-72.
WANG Peng, GAO Zeng, LI Jinzhu, CHENG Dongfeng, XU Dongxia, NIU Jitai. Preparation of Aluminum Base Filler Metals and Brazing Processes of 6063Al Matrix Composites with High SiC Content. Materials Reports, 2017, 31(2): 69-72.
链接本文:  
http://www.mater-rep.com/CN/10.11896/j.issn.1005-023X.2017.02.015  或          http://www.mater-rep.com/CN/Y2017/V31/I2/69
1 Guo M, Liu J, Li Y. Microstructure and properties of SiCp/Al electronic packaging shell produced by liquid-solid separation[J]. Trans Nonferrous Metals Soc China,2014,24(4):1039.
2 Irving R R. Packaged for the road[J]. Mechan Eng,2001,123(7):56.
3 Liu J, Zhou G T, Chen C B, et al. Interface behavior and perfor-mance of laser induced brazing for SiCp/Al composite[J]. Trans China Weld Institut,2015(8):43(in Chinese).
刘骏,周广涛,陈聪彬,等.SiCp/Al激光诱导钎焊接头界面行为及性能[J].焊接学报,2015(8):43.
4 Zhang G, Chen B, Jin M, et al. Active-transient liquid phase (A-TLP) bonding of high volume fraction SiC particle reinforced A356 matrix composite[J]. Mater Trans,2015,56(2):212.
5 Niu J, Luo X, Tian H, et al. Vacuum brazing of aluminium metal matrix composite (55 vol% SiCp/A356) using aluminium-based fi-ller alloy[J]. Mater Sci Eng B,2012,177(19):1707.
6 Ahmed E M, Ebrahim M R. Microstructure and microhardness evolution of melt-spun Al-Si-Cu alloy[J]. Eur Phys J Plus,2014,129(4):1.
7 Von Ina Maja, Medved Jozef, Bon Ina Tonica, et al. Effect of Ce on morphology of α(Al)-Al2Cu eutectic in Al-Si-Cu alloy[J]. Trans Nonferrous Metals Soc China,2014,24(1):36.
8 Zhang G, Su W, Zhang J, et al. Development of Al-12Si-xTi system active ternary filler metals for Al metal matrix composites[J]. Trans Nonferrous Metals Soc China,2012,22(3):596.
9 Wang S, Zhou H, Kang Y. The influence of rare earth elements on microstructures and properties of 6061 aluminum alloy vacuum-brazed joints[J]. J Alloys Compd,2003,352(1-2):79.
10 Garbellini O, Palacio H. Correlation between fluidity and solidification-microstructures at the aluminum- rich corner of Al-Cu-Si system cast metals[J]. Weld J,1990,2:82.
11 Xu D X, Tian J F, Wang D B, et al. Effect of Al-20Cu-9.6Cu-xEr filler metal on microstructure and properties of brazed joints for SiCp/A356 composites by vacuum brazing [J]. J Mater Eng,2016(1):60(in Chinese).
徐冬霞,田金峰,王东斌,等.Al-20Cu-9.6Si-xEr钎料对SiCp/A356复合材料真空钎焊接头组织与性能的影响[J].材料工程,2016(1):60.
12 车荫昌.梁英教.无机热力学数据手册[M].沈阳:东北大学出版社,1993.
[1] 张冠星, 薛行雁, 龙伟民, 钟素娟, 孙华为, 董宏伟. BAg45CuZn钎料硫化处理组织和性能演变特性[J]. 材料导报, 2019, 33(z1): 425-427.
[2] 王刘珏,薛松柏,刘晗,林尧伟,陈宏能. 电子封装用Au-20Sn钎料研究进展[J]. 材料导报, 2019, 33(15): 2483-2489.
[3] 王剑豪,薛松柏,吕兆萍,王刘珏,刘晗. 纳米颗粒增强无铅钎料的研究进展[J]. 材料导报, 2019, 33(13): 2133-2145.
[4] 王星星,彭 进,崔大田,薛 鹏,李 红,胡安明,孙国元. 银基钎料在制造业中的研究进展[J]. 《材料导报》期刊社, 2018, 32(9): 1477-1485.
[5] 王星星, 彭进, 崔大田, 孙国元, 何鹏. 不锈钢表面电镀锡银钎料的润湿特性[J]. 《材料导报》期刊社, 2018, 32(8): 1263-1266.
[6] 袁战伟, 李付国, 王春伟, 王瑜, 郭亚杰, 周亮. 基于Murty准则的SiCp/Al复合材料热加工图研究[J]. 《材料导报》期刊社, 2018, 32(4): 657-661.
[7] 唐昌平, 李国栋, 李志云, 孙玹琪. 铸造Mg-Gd-Y-Nd-Zr合金在时效过程中的组织与性能演变[J]. 《材料导报》期刊社, 2018, 32(4): 574-578.
[8] 樊江磊, 刘占云, 李育文, 吴深, 王霄, 刘建秀. Sn-Cu系无铅钎料微合金化研究进展[J]. 材料导报, 2018, 32(21): 3774-3779.
[9] 侯斌, 刘凤美, 王宏芹, 李琪, 万娣, 张宇鹏. 不同温度下Sn-0.7Cu钎料在非晶Fe84.3Si10.3B5.4合金上的润湿行为及界面特征[J]. 材料导报, 2018, 32(18): 3208-3212.
[10] 唐昌平, 左国良, 刘文辉, 朱美韵, 李志云, 李权, 刘筱, 卢立伟. 挤压-T5态Mg-8Gd-4Y-Nd-Zr合金的动态冲击行为[J]. 《材料导报》期刊社, 2018, 32(14): 2437-2441.
[11] 万永强,胡小武,徐涛,李玉龙,江雄心. Cu/Sn37Pb/Cu钎焊接头界面微观结构及其剪切性能[J]. 《材料导报》期刊社, 2018, 32(12): 2003-2007.
[12] 王星星, 谭群燕, 薛鹏, 唐明奇, 龙伟民. 镀锡银钎料扩散过渡区的物相和形成机制*[J]. 《材料导报》期刊社, 2017, 31(8): 66-69.
[13] 刘发齐, 关志东, 边天涯. 三维编织复合材料紧固件剪切强度预报[J]. 《材料导报》期刊社, 2017, 31(7): 121-128.
[14] 王鹏,高增,程东锋,牛济泰,. 高体积比SiCp/A356复合材料真空扩散钎焊接头组织与性能研究*[J]. 材料导报编辑部, 2017, 31(22): 75-78.
[15] 张先炼, 何晓聪, 赵伦, 邢保英, 程强. TA1异质自冲铆接头力学性能及失效机理*[J]. 《材料导报》期刊社, 2017, 31(20): 92-95.
[1] Bingwei LUO,Dabo LIU,Fei LUO,Ye TIAN,Dongsheng CHEN,Haitao ZHOU. Research on the Two Typical Infrared Detection Materials Serving at Low Temperatures: a Review[J]. Materials Reports, 2018, 32(3): 398 -404 .
[2] Huimin PAN,Jun FU,Qingxin ZHAO. Sulfate Attack Resistance of Concrete Subjected to Disturbance in Hardening Stage[J]. Materials Reports, 2018, 32(2): 282 -287 .
[3] Siyuan ZHOU,Jianfeng JIN,Lu WANG,Jingyi CAO,Peijun YANG. Multiscale Simulation of Geometric Effect on Onset Plasticity of Nano-scale Asperities[J]. Materials Reports, 2018, 32(2): 316 -321 .
[4] Xu LI,Ziru WANG,Li YANG,Zhendong ZHANG,Youting ZHANG,Yifan DU. Synthesis and Performance of Magnetic Oil Absorption Material with Rice Chaff Support[J]. Materials Reports, 2018, 32(2): 219 -222 .
[5] Ninghui LIANG,Peng YANG,Xinrong LIU,Yang ZHONG,Zheqi GUO. A Study on Dynamic Compressive Mechanical Properties of Multi-size Polypropylene Fiber Concrete Under High Strain Rate[J]. Materials Reports, 2018, 32(2): 288 -294 .
[6] XU Zhichao, FENG Zhongxue, SHI Qingnan, YANG Yingxiang, WANG Xiaoqi, QI Huarong. Microstructure of the LPSO Phase in Mg98.5Zn0.5Y1 Alloy Prepared by Directional Solidification and Its Effect on Electromagnetic Shielding Performance[J]. Materials Reports, 2018, 32(6): 865 -869 .
[7] ZHOU Rui, LI Lulu, XIE Dong, ZHANG Jianguo, WU Mengli. A Determining Method of Constitutive Parameters for Metal Powder Compaction Based on Modified Drucker-Prager Cap Model[J]. Materials Reports, 2018, 32(6): 1020 -1025 .
[8] WANG Tong, BAO Yan. Advances on Functional Polyacrylate/Inorganic Nanocomposite Latex for Leather Finishing[J]. Materials Reports, 2017, 31(1): 64 -71 .
[9] HUANG Dajian, MA Zonghong, MA Chenyang, WANG Xinwei. Preparation and Properties of Gelatin/Chitosan Composite Films Enhanced by Chitin Nanofiber[J]. Materials Reports, 2017, 31(8): 21 -24 .
[10] YUAN Xinjian, LI Ci, WANG Haodong, LIANG Xuebo, ZENG Dingding, XIE Chaojie. Effects of Micro-alloying of Chromium and Vanadium on Microstructure and Mechanical Properties of High Carbon Steel[J]. Materials Reports, 2017, 31(8): 76 -81 .
Viewed
Full text


Abstract

Cited

  Shared   
  Discussed