Fe3O4@CuO磁流体的制备和边界润滑性能

doi:10.11896/cldb.22060132

材料导报

2024, Vol. 38

Issue (8): 22060132-7 https://doi.org/10.11896/cldb.22060132

无机非金属及其复合材料

Fe₃O₄@CuO磁流体的制备和边界润滑性能

何彦¹, 王优强^1,2,*, 莫君¹, 赵涛¹, 朱玉玲¹, 李梦杰¹

1 青岛理工大学机械与汽车工程学院,山东青岛 266520
2 工业流体节能与污染控制教育部重点实验室,山东青岛 266520

Preparation and Boundary Lubrication Performance of Fe₃O₄@CuO Magnetic Fluid

HE Yan¹, WANG Youqiang^1,2,*, MO Jun¹, ZHAO Tao¹, ZHU Yuling¹, LI Mengjie¹

1 School of Mechanical and Automotive Engineering, Qingdao University of Technology, Qingdao 266520, Shandong, China
2 Key Laboratory of Energy Conservation and Pollution Control of Industrial Fluids, Ministry of Education, Qingdao 266520, Shandong, China

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摘要采用化学共沉淀法合成了纳米Fe₃O₄和纳米Fe₃O₄@CuO粒子。采用场发射透射电镜(FETEM)、X射线衍射仪(XRD)、振动样品磁强计(VSM)和傅里叶变换红外光谱仪(FTIR)对纳米粒子进行表征。采用表面活性剂法制备了不同粒子含量的PAO3磁流体。利用磁流体对外加磁场的响应特性和紫外分光光度计对磁流体分散性进行了表征。采用摩擦副为12CrNi4A和Si₃N₄的UMT-3往复摩擦磨损试验机对磁流体的摩擦学性能进行了评估。摩擦实验结果表明,含纳米Fe₃O₄粒子的PAO3基磁流体的润滑效果比较差。而质量分数为1%的纳米PAO3基Fe₃O₄@CuO粒子磁流体润滑时的摩擦系数相比于PAO3油润滑降低了29.6%,磨痕宽度降低了49.6%。从磨痕表面分析来看,这得益于CuO的摩擦烧结作用,在摩擦表面形成了有效的摩擦膜并修复磨损表面。

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	何彦
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	李梦杰

关键词: 航空润滑油纳米粒子磁流体减摩抗磨

Abstract: Nano Fe₃O₄ particles and nano Fe₃O₄@CuO particles were synthesized by chemical coprecipitation. The nanoparticles were characterized by field emission transmission electron microscopy (FETEM), X-ray diffraction (XRD), vibrating sample magnetometer (VSM) and fourier transform infrared spectrometer (FTIR). Polyalphaolefin (PAO) 3 magnetic fluids with different particle contents were prepared by surfactant method. The magnetic fluid was characterized by some changes of magnetic field and ultraviolet spectrophotometer. The friction and wear tester is UMT-3. The friction pairs are 12CrNi4A and Si₃N₄. The experimental results show that the addition of nano Fe₃O₄ increases the friction and wear. Compared with PAO3 oil, the friction coefficient of PAO3 based magnetic fluid lubricated with nano Fe₃O₄ and CuO composite nanoparticles is reduced by 29.6% and the wear scar width is reduced by 49.6%. From the analysis of wear mark surface, this is due to the friction sintering effect of CuO, and an effective friction film is formed on the friction surface to repair the wear surface.

Key words: aviation lubrication nanoparticle magnetic fluid antifriction and antiwear

出版日期: 2024-04-25 发布日期: 2024-04-28

ZTFLH:

TH117.1

基金资助: 国家自然科学基金(51575289);山东省自然科学基金(ZR2021ME063)

通讯作者: *王优强,青岛理工大学机械与汽车工程学院教授、博士研究生导师。1992年7月青岛理工大学冶金机械专业本科毕业,1995年3月东北大学机械学专业硕士毕业,1999年6月北京石油大学机械工程专业博士毕业。目前主要从事摩擦学与表界面工程及铝镁金属材料处理与加工。在Tribology International、Lubrication Science、STLE Tribology Transactions、Industrial Lubrication and Tribology、《机械工程学报》等国内外重要学术期刊上发表学术论文200余篇,其中SCI收录30余篇,EI收录30余篇,中文核心期刊收录100余篇。wyq1970301@126.com

作者简介: 何彦,2020年7月西华大学交通运输专业本科毕业,2020年9月于青岛理工大学攻读硕士学位。在王优强教授的指导下进行研究,目前主要研究领域为摩擦学与表界面工程。

引用本文:

何彦, 王优强, 莫君, 赵涛, 朱玉玲, 李梦杰. Fe₃O₄@CuO磁流体的制备和边界润滑性能[J]. 材料导报, 2024, 38(8): 22060132-7.
HE Yan, WANG Youqiang, MO Jun, ZHAO Tao, ZHU Yuling, LI Mengjie. Preparation and Boundary Lubrication Performance of Fe₃O₄@CuO Magnetic Fluid. Materials Reports, 2024, 38(8): 22060132-7.

链接本文:

https://www.mater-rep.com/CN/10.11896/cldb.22060132 或 https://www.mater-rep.com/CN/Y2024/V38/I8/22060132

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