POLYMERS AND POLYMER MATRIX COMPOSITES |
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Effect of Waste Oil Residue Regenerators on Dynamic Mechanical Properties and Component Migration of Aged Asphalt |
KUANG Dongliang1, MA Xiaojun1,2, MA Xiaoyan1,*, YUAN Bin3, HOU Junpeng1, CAI Jun4
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1 School of Materials Science and Engineering, Chang’an University, Xi’an 710064, China 2 Qinghai Transportation Planning and Design Institute Co., Ltd., Xining 810000, China 3 Gansu Road and Bridge Construction Group Maintenance Technology Co., Ltd., Lanzhou 730050, China 4 Qinghai Xihu Highway Management Co., Ltd., Xining 810000, China |
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Abstract The study of recycled asphalt is currently primarily focused on the recovery of aging asphalt properties, with little attention paid to the aging of recycled asphalt. In this study, two types of recycled engine oil bottom (REOB1 and REOB2) were used to regenerate the aged matrix asphalt, and short-term (TFOT) and long-term (PAV) aging were performed on the recycled asphalt. The dynamic mechanical properties and chemical component changes of recycled asphalt and its aged condition were evaluated using the dynamic shear rheometer (DSR) and the thin layer chromatography-flame ionization detector (TLC-FID). The results show that both REOB regenerants can restore the performance of aging matrix asphalt to that of the original asphalt, and that REOB2 regenerant is more compatible with aging matrix asphalt than REOB1 regenerant;the complex modulus and phase angle of the aging matrix asphalt could be retrieved by both REOB regenerants, according to master curve fitting with the CAM model and normalization of the fitting data. During the secondary aging process, the normalized complex modulus index (NCMI) of RA+REOB reclaimed asphalt gradually increases in the low and medium frequency range, and even after long-term aging, its complex modulus is still lower than that of long-term aging matrix asphalt. The normalized phase angle index (NPAI) in the middle frequency range is significantly higher than in the low and high frequency ranges, and the NPAI of the RA+REOB1 recycled asphalt after PAV aging is lower than the matrix asphalt after long-term aging. The chemical components of the RA+REOB recycled asphalt migrate from the aromatic components to the resins as the aging degree increases, and the REOB1 reclaimed asphalt loses the most light components after PAV aging.
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Published: 25 January 2024
Online: 2024-01-26
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Fund:Key R & D and Transformation Plan of Qinghai Province(2021-SF-165), the China Postdoctoral Science Foundation (2020M683401), the Natural Science Foundation of Shaanxi Province (2021JQ-262), the Fundamental Research Funds for the Central Universities (300102311402), and the National Natural Science Foundation of China(52208417). |
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