先驱体转化陶瓷涂层的裂解方法研究进展

doi:10.11896/cldb.20040261

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Abstract As the service environment of metal parts become more and more demanding, according to the different environment and failure characteristics of metal parts, different ceramic material systems and appropriate technologies are selected to prepare high-performance ceramic protective coating on the surface of metal parts and giving it special functions. The preparation of ceramic protective coatings on metal parts has become an effective way to solve the problem of reliable service of metal parts under harsh working conditions. As a new method of in-situ preparation of ceramic coating, polymer derived ceramic method takes advantage of the good fluidity, formability and designability of molecular structure of the precursor polymer, the polymer coating transformed into ceramic coating by pyrolysis, and dense protective coating is formed on the surface of the substrate material.
Pyrolysis is an important way for precursors to transform from organic to ceramic coating. Traditional furnace pyrolysis uses setting heating program to achieve continuous and batch preparation of ceramic coatings on the surface of metals, porous materials, fibers or fiber-reinforced composite materials. The furnace pyrolysis simple and easy to control, but it has a great thermal effect on the substrate, then it is impossible to prepare ceramic coating on substrate with low melting point or complex structure. Laser pyrolysis can selectively control the heat input, with uniform heating rate and fast pyrolysis, and laser pyrolysis has little thermal effect on the substrate. Ceramic coatings with special compositions can be prepared by laser pyrolysis, while the precursor must be able to absorb laser, and the efficiency of laser pyrolysis is low. Ion beam irradiation is a non-thermal cracking method, which the pyrolysis speed is high, but has low efficiency and high cost.
In this paper, the research progress in pyrolysis method of polymer derived ceramic coatings is summarized. The advantages and disadvantages of pyrolysis methods including furnace pyrolysis, laser pyrolysis and ion irradiation for polymer derived ceramic coatings are compared. In the future, it is necessary to explore new methods and technologies for controllable preparation of polymer derived ceramic coatings, reveal the evolution law microstructure from polymers to ceramic coatings, realize the accurate control of the preparation of the densification ceramic coatings which the crack defects can be precisely controlled.

Key words： polymer-derived ceramics organosilicon polymers pyrolysis method ceramic coatings

Published: 30 November 2021

CLC number:

TB33

Fund:National Natural Science Foundation of China (51805540), Beijing Natural Science Foundation (3192040), National Key Research and Development Project (2017YFF0207905).

About author:: Enzhong Li, associate professor of National Key Laboratory for Remanufacturing, Army Academy of Armored Forces. In recnet years, he has taken charge of a great variety of scientific projects such as National Natural Science Foundation of China, Beijing Natural Science Foundation and Weapon Equipment Basic Research, has also participated National Key Research and Deve-lopment Project, Major Consulting Project of Chinese Academy of Engineering and so forth. He has published more than 40 academic papers, has been authorized to have 5 invention patents in China and more than 10 monographs, and has won three awards at the provincial or ministerial level. His research interest is synthesis of advanced ceramics, nanomaterials and the application in surface engineering and remanufacturing.

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	LI Enzhong
	GUO Weiling
	LIU Jun
	YU Helong
	XU Binshi

Cite this article:

LI Enzhong,GUO Weiling,LIU Jun, et al. Research Progress in Pyrolysis Method of Polymer Derived Ceramic Coatings[J]. Materials Reports, 2021, 35(21): 21151-21158.

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http://www.mater-rep.com/EN/10.11896/cldb.20040261 OR http://www.mater-rep.com/EN/Y2021/V35/I21/21151

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