Materials Reports  2020, Vol. 34 Issue (Z1): 148-152 |
| INORGANIC MATERIALS AND CERAMIC MATRIX COMPOSITES |
|
|
|
|
|
| Hydrothermal Synthesis of Dice-like and Hex-pod-like Cuprous Oxide withMulti-cavities |
| MO Ruofei
|
| Guangxi University of Chinese Medicine, Nanning 530200, China |
|
|
|
|
Abstract In this work, hydrothermal method was adopted to prepare dice-like and hex-pod-like cuprous oxide(Cu2O) microncrystals with multi-cavities via reduction of copper(II) acetate with glucose in water-ethanol alkaline solution, using oleic acid as capping agent and EDTA as chelating agent. Through controlling the dosage of NaOH, oleic acid and NaOH, Cu(OAc)2 and glucose, water/ethanol volume ratio, the morphology of Cu2O can be controlled respectively. Thus, cuprous oxide with dice or hexapod shape can be obtained.
|
|
Published: 01 July 2020
|
|
|
| Fund:This work was financially supported by Doctoral Research Start-up Fund of Guangxi University of Chinese Medicine(2018BS027). |
| About author:: Ruofei Mo, associate professor of Guangxi University of Chinese Medicine. From 2004 to 2007, he obtained his Ph.D. in physical chemistry from Shanxi Institute of Coal Chemistry, Chinese Academy of Sciences. He has published 5 SCI papers and obtained 2 Chinese invention patents. The research party is inorganic nano materials and their applications. In recent years, he has participated in 2 National Natural Science Foundation projects, direct 1 Guangxi science and technology development project and participated in 3 Guangxi science and technology plan projects. |
|
|
1 Caruso F, Caruso R A, Mohwald H. Science,1998,282,1111.
2 Sun Y G, Xia Y N. Science,2002,298,2176.
3 Yin Y D, Rioux R M, Erdonmez C K, et al. Science,2004,304,711.
4 Yang H G, Zeng H C. Angewandte Chemie International Edition,2004,43,5930.
5 Yang J H, Qi L M, Lu C H, et al. Angewandte Chemie International Edition,2005,44,598.
6 Chen J, Saeki F, Wiley B J, et al. Nano Letters,2005,5(3),473.
7 Sawant S S, Bhagwat A D, Mahajan C M. Journal of Nano- and Electro-nic Physics,2016,8(1),01035-1.
8 Tolstova Y, Omelchenko S T, Blackwell R E, et al. Solar Energy Mate-rials and Solar Cells,2017,160,340.
9 Masudy-Panah S, Radhakrishnan K., Tan H R, et al. Solar Energy Materials and Solar Cells,2015,140,266.
10 Toe C Y, Zheng Z K, Wu H, et al. Angewandte Chemie International Edition,2018,130(41),13801.
11 Lei B, Zheng D. RSC Advances,2015,5(14),10089.
12 Choi Y H, Kim D H, Han H S, et al. Langmuir,2014,30,700.
13 Zhang L Z, Jing D W, Guo L J, et al. ACS Sustainable Chemistry & Engineering,2014,2,1446.
14 Lu C H, Qi L M, Yang J H, et al. Advanced Materials,2005,17(21),2562.
15 Kuo C H, Huang M H. Journal of the American Chemical Society,2008,130,12815.
16 Xu H L, Wang W Z. Angewandte Chemie International Edition,2007,46(9),1489.
17 Xu J, Tang Y B, Zhang W X, et al. Crystal Growth & Design,2009,9,4524.
18 Li G L, Ma P, Zhang Y F, et al. Journal of Materials Science,2016,51,3979.
19 Xu H L, Wang W Z, Zhou L. Crystal Growth & Design,2008,8(10),3486.
20 Siegfried M J, Choi K S. Advanced Materials,2004,16(19),1743. |
|
|
|
渝公网安备50019002502923号 © Editorial Office of Materials Reports.
