铁铝金属间化合物及其涂层制备的研究进展

doi:10.11896/cldb.20070273

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Abstract Fe-Al intermetallic compounds have been widely focused due to their high creep resistance, good wear resistance, and high-temperature anti-oxidation and vulcanization resistance. However, these compounds contain three grain structures, B2, DO₃ and A2, which are difficult to control them accurately. Also, high brittleness at room temperature of DO₃ brings difficulties in preparation and processing. These shortcomings greatly limit the application of Fe-Al intermetallic compounds.
This paper summarized several common preparation methods of Fe-Al intermetallic compound block materials including traditional casting me-thod and powder metallurgy method. As well as the additive manufacturing technology, some coatings' preparation methods, for example, cold spraying, hot spray and some other methods, which have been developed in recent years, were introduced as important points.
At the same time, referring to the key question of reaction control between Fe and Al in coatings, this paper focused on how to predict the sequence of the synthesis reaction of Fe-Al intermetallic compounds, which were generated in the original position of the interface reaction of Fe-Al coatings and proposed two prediction methods—phase diagram method and enthalpy change calculation method. Among them, the phase diagram can only represents the phase distribution in the heat balance state, and each phase region barely represents final products that are obtained under specific temperature and composition, thus the dynamic process of the occurrence of Fe-Al intermetallic compounds cannot be judged. Therefore, this paper calculated the enthalpy change value from the perspective of thermodynamics, combined with Kirchhoff formula, calculated, and plotted the enthalpy-temperature curve of common Fe-Al intermetallic compounds, and analyzed the reaction sequence of Fe-Al intermetallic compounds. The theoretical and experimental results of the enthalpy calculation method were highly compatible, thus could modify the phase diagram method, which is of great significance for the preparation of specific Fe-Al intermetallic compounds.

Key words： Fe-Al intermetallic compounds Fe-Al coating interface reaction enthalpy change calculating

Published: 30 November 2021

CLC number:

TG113.12

Fund:National Natural Science Foundation of China(U1967212), National Key Research and Development Program of China(2018YFE0306100).

About author:: You Wang received her B.E. degree in materials science from University of Science and Technology Beijing in 2019. She is currently pursuing her master degree at the School of Materials Science and Enginee-ring, University of Science and Technology Beijing under the supervision of prof. Zhangjian Zhou. Her research has focused on Fe-Al coatings preparation and interface reaction.
Zhangjian Zhou received his Ph.D. degree in School of Materials Science and Engineering, University of Science and Technology Beijing in 2007. After postdoctoral research at Forschungszentrum Jülich in German, he is currently a full professor in University of Sci. & Tech. Beijing. His major research projects are batch preparation technology and key service performance of ODS steel for fusion reactor in ITER project of ministry of science and technology, international atomic energy agency (IAEA) international cooperation program (CRP), etc.

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	WANG You
	DENG Nan
	TONG Zhenfeng
	ZHOU Zhangjian

Cite this article:

WANG You,DENG Nan,TONG Zhenfeng, et al. Research Progress on Preparation of Fe-Al Intermetallic Compounds and Coatings[J]. Materials Reports, 2021, 35(21): 21221-21227.

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http://www.mater-rep.com/EN/10.11896/cldb.20070273 OR http://www.mater-rep.com/EN/Y2021/V35/I21/21221

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