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Effect of Semi-Solid Isothermal Heat Treatment on Non-dendritic Structure of Mg-7Zn-1Cu-0.3V Magnesium Alloy |
HUANG Xiaofeng1, 2, WEI Langlang1, YANG Jianqiao1, ZHANG Qiaoqiao1, SHANG Wentao1, LI Xujiao1
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1 State Key Laboratory of Advanced Processing and Recycling of Nonferrous Metals, Lanzhou University of Technology, Lanzhou 730050, China 2 Key Laboratory of Non-ferrous Metal Alloys and Processing, Ministry of Education, Lanzhou University of Technology, Lanzhou 730050, China |
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Abstract In this paper, the effects of holding temperature and holding time on the semi-solid non-dendritic microstructure evolution of Mg-7Zn-1Cu-0.3V magnesium alloy were studied by semi-solid isothermal heat treatment. The results show that the semi-solid isothermal heat treatment can transform the original dendritic structure of the Mg-7Zn-1Cu-0.3V alloy into semi-solid non-dendritic structure, and finally obtain small, round and evenly distributed spherical particles. Prolonging the isothermal time or increasing the holding temperature is beneficial to the separation and spheroidization of non-dendritic structures. However, when the holding temperature is too high or the time is too long, the semi-solid particles will merge and grow, and the main evolution mechanism is in accordance with the Ostwald ripening mechanism. During the whole isothermal heat treatment process, the semi-solid microstructure evolution mainly experienced three stages: initial coarsening, tissue separation and spheroidization, particle combination and ripening. The best isothermal heat treatment process of Mg-7Zn-1Cu-0.3V alloy is held for 35 min at the holding temperature of 580 ℃. The average size, solid phase rate and shape factor of non-dendritic particles are 33.25 μm, 45% and 1.33, respectively.
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Published: 14 July 2020
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Fund:This work was financially supported by the National Natural Science Foundation of China (51464032). |
About author:: Xiaofeng Huangreceived his Ph.D. degree from Harbin Institute of Technology (HIT) in January 2002 and obtained post-doctoral from Shanghai Jiao Tong University in May 2004, and entered Lanzhou University of Technology/State Key Laboratory of Advanced Proces-sing and Recycling of Nonferrous Metals, Lanzhou University of Technology in June 2004. He is currently an associate professor and master tutor. His research inte-rests focus on the advanced and high performance light metals, semi-solid forming of light alloy and precision plastic working. He hosted and participated in 3 provincial and ministerial level fund projects and two “863” programs. He has published more than 80 journal papers, applied 4 national invention patents, and is also a reviewer of several academic journals. |
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1 Guo J, Ye B, Wu Y J, et al. Special Casting & Nonferrous Alloys, 2019, 39(3), 254(in Chinese). 郭径, 叶兵, 吴玉娟, 等. 特种铸造及有色金属, 2019, 39(3), 254. 2 Xu J, Liu G, Zhang S, et al. Rare Metals, 2010, 29(5), 542. 3 Arruebarrena G, Hurtado I, Vinl J, et al. Advanced Engineering Materials, 2010, 9(9), 751. 4 Ye C L. Technology and Economic Guide, 2018, 26(19), 76(in Chinese). 叶成林. 科技经济导刊, 2018, 26(19), 76. 5 Buha J. Materials Science and Engineering A, 2008, 491(1/2), 70. 6 Feng K, Huang X F, Ma Y, et al. The Chinese Journal of Nonferrous Metals, 2013, 23(3), 635(in Chinese). 冯凯, 黄晓锋, 马颖, 等. 中国有色金属学报, 2013, 23(3), 635. 7 Spencer D B, Mehrabian R, Flemings M C. Metallurgical Transactions, 1972, 3(7), 1925. 8 Nishida M, Kawamura Y, Yamamuro T. Materials Science and Enginee-ring: A, 2004, 375-377, 1217. 9 Zhang D F, Qi F G, Zhao X B, et al. Journal of Chongqing University, 2010, 33(11), 53(in Chinese). 张丁非, 齐福刚, 赵霞兵, 等. 重庆大学学报, 2010, 33(11), 53. 10 Ye J, Lin X P, Dong Y, et al. Materials Science Forum, 2016, 4269(873), 33. 11 Buha J. Acta Materialia, 2008, 56(14), 3533. 12 Wang J H. Hot Working Technology, 2015, 44(19), 84(in Chinese). 王建华. 热加工工艺, 2015, 44(19), 84. 13 Zhang C, Liu J R, Huang W D. Rare Metal Materials and Engineering, 2011, 40(7), 1173(in Chinese). 张超, 刘建睿, 黄卫东. 稀有金属材料与工程, 2011, 40(7), 1173. 14 Zhong L X, Yang M B, Yuan S, et al. Journal of Chongqing University of Technology (Natural Science), 2019, 33(8), 90(in Chinese). 钟罗喜, 杨明波, 袁淑,等. 重庆理工大学学报(自然科学), 2019, 33(8), 90. 15 Li A W, Liu J W, Wu C L, et al. Chinese Journal of Nonferrous Metals, 2010, 20(8), 1487(in Chinese). 李爱文, 刘江文, 伍翠兰, 等. 中国有色金属学报, 2010, 20(8), 1487. 16 Huang X F, Zhang Y, Qin M L, et al. Transactions of Materials and Heat Treatment, 2016, 37(8), 53(in Chinese). 黄晓锋, 张玉, 秦牧岚, 等. 材料热处理学报, 2016, 37(8), 53. 17 Li Y D, Hao Y, Chen T J, et al. Chinese Journal of Nonferrous Metals, 2002, 12(6), 1143(in Chinese). 李元东, 郝远, 陈体军, 等, 中国有色金属学报, 2002, 12(6), 1143. 18 Hu Y, Rao L, Li Q P, et al. Rare Metal Materials and Engineering, 2016, 45(2), 493(in Chinese). 胡勇, 饶丽, 黎秋萍, 等. 稀有金属材料与工程, 2016, 45(2), 493. 19 Kang M K, Kim D Y, Hwang M H. Journal of the European Ceramic Society, 2002, 22(5), 603. 20 Wang S C, Li Y Y, Chen W P, et al. Acta Metallurgica Sinica, 2008, 44(8), 905(in Chinese). 王顺成, 李元元, 陈维平, 等. 金属学报, 2008, 44(8), 905. 21 Li C, Zhou C S, Liu Y F, et al. Foundry, 2014, 63(5), 495(in Chinese). 李春, 周春生, 刘彦峰, 等. 铸造, 2014, 63(5), 495. 22 Liu H Y, Wu K M, Lei Y H, et al. Physics Examination and Testing, 2007, 25(6), 1(in Chinese). 刘宏玉, 吴开明, 雷应华, 等. 物理测试, 2007, 25(6), 1. 23 Elgallad E M, Chen X G. Materials Science & Engineering A (Structural Materials: Properties, Microstructure and Processing), 2012, 556, 783. 24 Le Q C, Zhang X J, Cui J Z, et al. Acta Metallurgica Sinica, 2002, 38(12),1266(in Chinese). 乐启炽, 张新建, 崔建忠, 等. 金属学报, 2002, 38(12), 1266. 25 Zhang Y, Huang X F, Ma Y, et al. China Foundry, 2017, 14(2), 433. 26 Atkinson H V, Liu D. Materials Science and Engineering A, 2008, 496(1-2), 439. 27 Du L, Yan H. Chinese Journal of Materials Research, 2012, 26(2), 169(in Chinese). 杜磊, 闫洪. 材料研究学报, 2012, 26(2), 169. |
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