Materials Reports  2021, Vol. 35 Issue (Z1): 100-103 |
| INORGANIC MATERIALS AND CERAMIC MATRIX COMPOSITES |
|
|
|
|
|
| Research on Gel Injection Molding of Dental Braces with ZTA Ceramic Materials |
| WU Zinuo1,2, JIA Hongyu1,2, ZHANG Yuqing1,2, CHEN Yang1,2
|
1 College of Materials Science and Engineering, North China University of Technology, Tangshan 063000, China
2 Hebei Provincial Laboratory of Inorganic Nonmetallic Materials, Tangshan 063000, China |
|
|
|
|
Abstract In order to improve the performance of ZTA ceramics in oral clinical application, dental braces with ZTA ceramic materials were prepared by gel injection molding, polymer as adhesive, carboxymethyl cellulose as skeleton. We explored the influence of powder solid content, carboxymethyl cellulose (CMC), acrylic acid (AA) and ammonium persulfate (APS) on the bending strength, fracture toughness of ZTA ceramic materials. ZTA ceramics at the optimal process level were prepared and their properties were tested. The results showed as follows: the addition amount of CMC was 0.85 g, the addition amount of APS was 0.8 g, the addition amount of AA was 7.5 mL, the addition amount of Al2O3 was 110 g, and the addition amount of ZrO2 was 33 g. The flexural strength of the ZTA ceramic material was 222.3 MPa, the fracture toughness was 8.67 MPa·m 1/2, the relative density was 0.977, and the shear strength was between 6.06—6.93 MPa, meeting the clinical requirements.
|
|
Published: 16 July 2021
|
|
|
| Fund:Natural Science Foundation of Hebei Province (E2016209327), College Students Innovation and Entrepreneurship Training Program of North China University of Science and Technology (R2020083, X2020067), and Research and Practice Project of Education and Teaching Reform of North China University of Science and Technology (Q1864-01), Basic Research Expenses Project for Provincial Colleges and Universities (JYG2021001). |
| About author:: Zinuo Wu is a student from the School of Materials Science and Engineering, North China University of Science and Technology. During the period of school, he won the second prize of the national “Internet +” competition, the title of Outstanding College Student and the title of Outstanding Student Leader. At present, he has presided over and participated in two university innovation and entrepreneurship project, and two papers have been published. His main research interests are the modification of dental ceramic support and the preparation of carbon-based absorbing materials by polymer conversion.Yang Chen obtained her PhD from the Shandong University and served in School of Materials of Science and Engineering, North China University of Science and Technology, till now. She is currently an associate professor and master supervisor. She has published more than 20 journal papers, applied 2 national invention patents and all were authorized. Her team's research inte-rests are oral bracket material, carbon fiber and its composites, ceramic-based absorbing materials, carbon-based absorbing materials and so on. She participated in or presided over more than 10 scientific research projects, and has trained a number of master's degree, more than 100 undergraduates. |
|
|
1 侯晓蓓, 肖建中, 夏风.材料导报, 2007(专辑Ⅷ), 373.
2 侯晓蓓.陶瓷托槽材料及其成型工艺的研究.硕士学位论文,华中科技大学, 2007.
3 何柏林, 孙佳.粉末冶金工业, 2009, 19(4), 48.
4 Magdalena Szutkowska, Marek Boniecki. Journal of Materials Processing Technology, 2006,175, 416.
5 Wang J, Stevens R.Journal of Materials Science, 1988,23, 804.
6 卓蓉晖, 张建.江苏陶瓷, 2003(2),24.
7 李承亮, 赵兴宇, 郭文利,等.材料导报, 2007(5),36.
8 高华.热压铸氧化铝陶瓷工艺过程研究. 硕士学位论文,辽宁科技大学, 2014.
9 缪大梅.氧化铝凝胶注模成型工艺的研究.硕士学位论文, 苏州大学, 2006.
10 Anonymous. Research and Development, 1995, 37(9), 29.
11 王小锋, 王日初, 彭超群,等.中国有色金属学报, 2010, 20(3), 496.
12 Omatete O, Janney M A, Strehlow R A.American Ceramic Society Bulletin, 1991, 70(10), 1641.
13 Yuan B, Wu H, Sun X, et al.Materials Letters, 2012, 81(3), 151.
14 窦建鹏, 马景陶, 林旭平,等.稀有金属材料与工程, 2011, 40(3), 641.
15 李承亮, 赵兴宇, 郭文利,等.材料导报, 2007(5), 36.
16 郭瑞松, 杨正方, 袁启明, 等.硅酸盐学报, 1999(2), 141.
17 王丽梅,陈旸,孟菲,等.材料导报:研究篇,2016,30(2),85.
18 乜玉强, 王丽梅, 许佳欣,等.中国陶瓷, 2016, 52(9),69.
19 George Odian. Principles of polymerization,John Wiley & Sons, USA, 2004.
20 潘祖仁. 高分子化学,化学工业出版社, 2001. |
|
|
|
渝公网安备50019002502923号 © Editorial Office of Materials Reports.
