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《材料导报》期刊社  2017, Vol. 31 Issue (14): 1-3    https://doi.org/10.11896/j.issn.1005-023X.2017.014.001
  研究快报 |
用LiAlH4一步还原白炭黑制取多孔硅的研究*
汪徐春, 张雪梅, 叶祥桔, 陈俊明, 过家好, 张婷, 毛杰, 陈忠平
安徽科技学院化学与材料工程学院, 蚌埠 233000;
Preparation of Porous Silicon by One-step Reduction of Silica with LiAlH4
WANG Xuchun, ZHANG Xuemei, YE Xiangjie, CHEN Junming, GUO Jiahao, ZHANG Ting, MAO Jie, CHEN Zhongping
College of Chemistry and Material Engineering, University of Science and Technology of Anhui, Bengbu 233000;
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摘要 多孔硅因其独特高效的光电效应而日益成为国内外研究的热点。在温度为450 ℃和500 ℃的条件下,采用LiAlH4热还原白炭黑(微米或纳米级二氧化硅)一步制得多孔硅,并利用XRD、红外光谱、扫描电镜、固体发射光谱等对实验产物进行了表征和分析。所提出的方法既绿色环保,又经济实惠,具有潜在的应用和推广价值。
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汪徐春
张雪梅
叶祥桔
陈俊明
过家好
张婷
毛杰
陈忠平
关键词:  氢化锂铝  一步还原  多孔硅    
Abstract: Porous silicon is becoming a hot research topic both at home and abroad because of its unique and efficient photoelectric effect.The porous silicon was prepared by thermal reduction of silica (micro- or nano-silica) at a temperature of 450 ℃ and 500 ℃ by one-step reacting with LiAlH4.The products were characterized and analyzed by XRD, IR, SEM and SPEF. This experimental method is green and environmentally friendly which has potential value of application.
Key words:  lithium aluminum hydride    one-step reduction    porous silicon
出版日期:  2017-07-25      发布日期:  2018-05-04
ZTFLH:  TB321  
  O649.4  
基金资助: *国家自然科学基金(21603002);安徽省人才基金(gxfxZD2016176);安徽省教育厅自然科学重点基金(KJ2016A171;KJ2016A184);材料科学与工程重点学科(AKZDXK2015A01)
作者简介:  汪徐春:男,1970年生,博士,教授,研究方向为功能材料 E-mail:xuchun.wang@163.com;wangxc@ahstu.edu.cn
引用本文:    
汪徐春, 张雪梅, 叶祥桔, 陈俊明, 过家好, 张婷, 毛杰, 陈忠平. 用LiAlH4一步还原白炭黑制取多孔硅的研究*[J]. 《材料导报》期刊社, 2017, 31(14): 1-3.
WANG Xuchun, ZHANG Xuemei, YE Xiangjie, CHEN Junming, GUO Jiahao, ZHANG Ting, MAO Jie, CHEN Zhongping. Preparation of Porous Silicon by One-step Reduction of Silica with LiAlH4. Materials Reports, 2017, 31(14): 1-3.
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https://www.mater-rep.com/CN/10.11896/j.issn.1005-023X.2017.014.001  或          https://www.mater-rep.com/CN/Y2017/V31/I14/1
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