氧化锆多孔陶瓷制备方法研究进展

doi:10.11896/cldb.21080217

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Abstract Porous zirconia materials are equipped with many advanced properties, such as the high specific surface area and extremely low thermal conductivity that is derived from their porous structures, as well as the good biocompatibility and chemical stability coming from the intrinsic pro-perties of zirconia. According to reported literature, the porosity and pore size greatly affect the thermodynamic performance of porous zirconia materials, while the morphology of the pores governs their permeability and capability in thermal shock resistance. Generally, the applications of porous zirconia materials substantially rely on their pore structures, therefore it is of great significance to review the recent fabrication methods that can achieve different types of pores in zirconia.
The prevailing fabrication methods for porous zirconia can be classified into three types:physical, chemical and phase separation (combination of the first two methods) methods. In recent years, the different methods to control pore structures have attracted worldwide attention. Basically, each pore-forming approach has its unique controlling mechanics to realize the goal structure of the pores. Typically, the products formed using physical methods are equipped with high mechanical performances, whereas their maximum porosity is quite limited. On the other hand, the chemical pore formation methods can offer high controllability over the micro-structure, but the preparation processes are inclined to generate toxic liquids or gases. Compared with the former two kinds of methods, phase separation can systematically adjust the porosity and micro-structure by designing the precursor reagents, nevertheless, this approach has strict requirement on the solution composition as well as the preparation environment. Although each pore forming method has its own pros and cons, phase separation is gaining more and more research interest for its great advantages in designing and achieving desirable porosity and pore structure. The technical key to conducting this approach is to properly formulate the precursor solution and to match the degrees of phase separation and gelation, in order to freeze the desirable two-phase condition with the gelling process and further acquire the suitable porous ceramic material.
In this review, we have concluded diverse fabrication methods for porous zirconia materials, and also have discussed and compared the typical features of the as-produced samples. Based on the reported data, we try to define the current challenges and the corresponding potential solutions in the research field of porous ceramics, which may pave the way for designing and preparing future porous zirconia with more advanced properties.

Key words： zirconia porous ceramics pore structure pore forming method phase separation

Published: Online: 2023-07-10

CLC number:

TQ174

Fund:National Natural Science Foundation of China(51905033),National Science and Technology Major Projects(2017-Ⅶ-0013-0110, J2019-Ⅶ-0015-0155), and Fundamental Research Funds for the Central Universities(FRF-GF-20-12B).

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	YU Haibo
	LIANG Shuaishuai
	LI Jiang
	QI Bin

Cite this article:

YU Haibo,LIANG Shuaishuai,LI Jiang, et al. Review:Preparation Methods of Porous Zirconia Ceramics[J]. Materials Reports, 2023, 37(13): 21080217-10.

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http://www.mater-rep.com/EN/10.11896/cldb.21080217 OR http://www.mater-rep.com/EN/Y2023/V37/I13/21080217

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