烧结温度对石棉矿山废石制备微晶玻璃析晶性能的影响

doi:10.11896/cldb.21040122

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Abstract The glass-ceramics with forsterite as the main crystalline phase and enstatite as the secondary crystalline phase were prepared by direct sintering method using waste rock from Dahonggou asbestos mine as raw material. The effects of the sintering temperature (1 150—1 325 ℃) on the crystalline phase, microstructure and properties of crystallization of glass-ceramics were investigated by using various modern analytical testing methods. The results show that with the increase of sintering temperature, the type of crystalline phase is not affected, but the content changes. The content of enstatite gradually increases, and the content of forsterite slightly decreases; the grains in glass-ceramics grow up, and the interwoven occlusal structure is formed among the grains. The glass-ceramics prepared at the sintering temperature of 1 300 ℃ show the optimal physical and chemical properties, of which the linear shrinkage rate, the volume density and the flexural strength are the largest at 11.2%, 2.78 g/cm³ and 95 MPa, respectively,and the water absorption is the smallest at 0.03%.

Key words： mine waste rock glass-ceramic direct sintering forsterite enstatite

Published: 10 August 2022 Online: 2022-08-15

CLC number:

X754

Fund:National Key R & D Program of China(2018YFC1802902).

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	LIU Quan
	SUN Hongjuan
	PENG Tongjiang
	WANG Can

Cite this article:

LIU Quan,SUN Hongjuan,PENG Tongjiang, et al. Effect of Sintering Temperature on Crystallization Properties of Glass-ceramics Prepared from Asbestos Mine Waste Rock[J]. Materials Reports, 2022, 36(15): 21040122-5.

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http://www.mater-rep.com/EN/10.11896/cldb.21040122 OR http://www.mater-rep.com/EN/Y2022/V36/I15/21040122

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