INORGANIC MATERIALS AND CERAMIC MATRIX COMPOSITES |
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Preparation of WS2-Cu Composites Under Different SPS Sintering Temperatures and Their Friction and Wear Properties |
JIANG Ye1, YAN Jianhui1,2,3, LI Maojian1
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1 College of Materials Science and Technology, Hunan University of Science and Technology, Xiangtan 411201, China 2 Hunan Provincial Key Defense Laboratory of High Temperature Wear Resisting Materials and Preparation Technology, Hunan University of Science and Technology, Xiangtan 411201, China 3 Hunan Provincial Key Laboratory of Advanced Materials for New Energy Storage and Conversion, Hunan University of Science and Technology, Xiangtan 411201, China |
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Abstract WS2 powder coated with copper was prepared using electroless plating technology. The WS2-Cu matrix composites were prepared by spark plasma sintering technique (SPS) using pure Cu and Cu coated WS2 powders as raw materials. The microstructure, mechanical properties and friction and wear properties of WS2-Cu matrix composites prepared at different sintering temperatures were studied. The results show that WS2 is distributed uniformly in the copper matrix and the interface between Cu and WS2 bond well. With an increase in the sintering temperature, the hardness of composites shows an increasing trend. WS2-Cu composites prepared at 500—750℃ have low friction coefficients (0.15—0.18). However, the composites prepared over 750℃ have high friction coefficients (0.42—0.54). The composites prepared at 700—750℃ has the lowest wear rate of (1.6—1.8)×10-5 mm3/(N·m). The surface treatment of WS2 powder coated with Cu improves the wear resistance of WS2-Cu composites. The suitable SPS sintering temperature for preparing WS2-Cu composites is 700—750℃. The plastic deformation, oxidative wear and adhesive wear were occurred during the friction and wear process in the WS2-Cu composites. There was a significant abrasive wear on the wear surface of the WS2-Cu composite when the WS2 was transformed into W.
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Published: 12 September 2020
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Fund:This work was jointly financially supported by the National Natural Science Foundation of China (51475161), Hunan Provincial Natural Science Foundation (2020JJ4025), Hunan Provincial Graduate Student Science and Technology Innovation Project (CX20190837). |
About author:: Ye Jiangreceived her bachelor's degree in June 2017 from Hunan University of Science and Technology. From September 2017 to the pre-sent, she is pursuing a master's degree at the School of Materials Science and Engineering of Hunan University of Science and Technology, focusing on the research of wear and friction pro-perties of composite materials. Jianhui Yanserved in School of Materials of Science and Engineering of Hunan University of Science and Technology. He is currently a professor and doctoral supervisor. He obtained Ph.D. degree in State Key Laboratory of Powder Metallurgy of Central South University. He has published more than 60 journal papers, applied 6 national invention patents and 4 of them were authorized. His major research interests are development of high temperature structural materials, protection of high temperature oxidation resistance for materials, wear resistance technology for materials surface, strengthening and toughening of materials. He presided National Natural Science Fund, Natural Science Fund of Hunan Province, and Science and Technology Project of Hunan Province, and so on |
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