| METALS AND METAL MATRIX COMPOSITES |
|
|
|
|
|
| Study on Fatigue Cracking Mechanism and Temperature Sensitivity of 316H Austenitic Stainless Steel |
| DONG Hezhan1, YU Ting1, SONG Yuxuan1,2,*, WANG Zhiqiang1, CAI Zhihui4, JIN Weiya1,2,3, JIANG Yanyao1,2, GAO Zengliang1,2,3,*
|
1 Institute of Process Equipment and Control Engineering, Zhejiang University of Technology, Hangzhou 310023, China 2 Institute of Innovation Research of Shengzhou and Zhejiang University of Technology, Shengzhou 312400, Zhejiang, China 3 Engineering Research Center of Process Equipment and Re-manufacturing Ministry of Education, Zhejiang University of Technology, Hangzhou 310014, China 4 Special Equipment Testing Science Research Institute, Wenzhou 325038, Zhejiang, China |
|
|
|
|
Abstract 316H austenitic stainless steel is one of the candidate materials for the first circuit piping in the high temperature gas-cooled reactors of Gene-ration IV nuclear power plants by virtue of its excellent high temperature performance. However, unexpected fatigue cracking occurs inits structural components at high temperatures, and there is an urgent need to understand the fatigue failure mechanism. In the current research, tensile experiments of 316H stainless steel at different temperatures were carried out. It was found that the yield strength and the ultimate strength gradually decrease with the increase in temperature, while the elongation decreases with increasing temperature in the range from room temperature to 300 ℃. A plateau appears in the range of 300 ℃ to 550 ℃, and the elongation increases with the increase of the test temperature above 550 ℃. By carrying out low frequency fatigue experiments of the material at room temperature and at the gas-cooled reactor service temperature of 600 ℃, the cyclic stress-strain characteristics and the S-N curves at both temperatures were obtained. The microstructural evolution under static tension and low cycle fatigue and the fracture profiles of the tested specimens were analyzed by micro characterization techniques, and the fracture mechanism was studied. The results show that the structure of the grain boundary is stable below 300 ℃, and fatigue cracking is mainly due to transgranular fracture; while precipitates appear in the grain boundaries above 550 ℃ and the tensile fracture shows a characteristic of partial intergranular fracture. At both room and high temperatures, the material exhibits three distinct cyclic stages: cyclic hardening, cyclic softening, and rapid failure. Post-fatigue characterization reveals significant grain coarsening at high temperature, whereas at room temperature, the grain size remains stable while the geometrically necessary dislocation (GND) density increases markedly. Furthermore, the fatigue crack initiation mechanisms differ: at room temperature, cracks originate from the surface due to slip-band accumulation; in contrast, at high temperature, the initiation sites suffer from severe oxidation, manifesting a fatigue-oxidation synergistic initiation characteristic.
|
|
Published: 25 January 2026
Online: 2026-01-27
|
|
|
|
|
1 Zhao Y X, Xiong R, Liang B, et al. Nuclear Power Engineering, 2023, 44(5), 237(in Chinese). 赵宇翔, 熊茹, 梁波, 等. 核动力工程, 2023, 44(5), 237. 2 Bao F D. Research on high temperature and low cycle fatigue perfor-mance of nuclear grade 316H steel and its welded joints. Master’s Thesis, Tianjin University, China, 2021(in Chinese). 鲍方栋. 核级 316H 钢及其焊接接头的高温低周疲劳性能研究. 硕士学位论文, 天津大学, 2021. 3 Dong G S, Gao B, Wang Z B, et al. International Journal of Fatigue, 2023, 168, 107425. 4 Wang Q, Sun Q Y, Xiao L, et al. Materials Science and Engineering A-Structural Materials Properties Microstructure and Processing, 2016, 649, 359. 5 Lei Y B, Wang Z B, Zhang B, et al. Acta Materialia, 2021, 208, 116773. 6 Cheng Y, Lin Z, Xie S, et al. International Journal of Fatigue, 2024, 186, 108415. 7 Li X, Chang L, Liu C, et al. Corrosion Science, 2021, 191, 109784. 8 Yoon J H, Hong S, Koo G H, et al. Journal of the Korean Institute of Metals and Materials, 2015, 53(10), 681. 9 Zhao L, Qi X, Xu L, et al. Fatigue & Fracture of Engineering Materials & Structures, 2021, 44(2), 533. 10 Xu L Y, Bao F D, Zhao L, et al. Journal of Nuclear Materials, 2021, 546, 152758. 11 Yang J, Li B, Wang K, et al. International Journal of Fatigue, 2024, 188, 108523. 12 Gao Y F, Liang X B, Deng X L. Tensile testing of metallic materials-Part 1: Implementation guidelines for room temperature testing methods: GB-T228. 1-2021, China Quality and Standards Publishing House, China, 2014(in Chinese) 高怡斐, 梁新帮, 邓星临. 金属材料拉伸试验第 1 部分: 室温试验方法实施指南: GB-T228. 1-2021. 中国质检出版社, 2014, 13 Huang H W, Wang Z B, Lu J, et al. Acta Materialia, 2015, 87, 150. 14 Yin P, Zhang W, Zhang Y, et al. Materials Science and Engineering: A, 2023, 849, 143494. 15 Sourabh K, Singh J B. Journal of Materials Engineering and Perfor-mance, 2022, 31(5), 3821. 16 Zhang Z, Li A, Wang Y P, et al. Materials Science and Engineering: A, 2020, 794, 139928. 17 Long J, Pan Q, Tao N, et al. Materials Research Letters, 2018, 6, 456. 18 Pan Z X, Li Y B, Song Y X, et al. International Journal of Pressure Vessels and Piping, 2022, 200, 104774. 19 Mo Y F, Du R, Ma H S, et al. Mechanics and Practice, 2022, 44 (3), 564(in Chinese) 莫亚飞, 杜柔, 马寒松, 等. 力学与实践, 2022, 44(3), 564. 20 Geng D, Sun Q, Xin C, et al. Nanomaterials, 2021, 11, 3125. 21 Choudhury S S, Poddar P, Datta P. Materials & Design, 2021, 198, 109315. 22 Colin J, Fatemi A, Taheri S, et al. Journal of Materials Science, 2010, 45(6), 1599. 23 Wang Y, Zhang X, Li J, et al. Materials Science and Engineering: A, 2020, 779, 139135. 24 Ho H S, Lv C, Zhou W, et al. Fatigue and Fracture of Engineering Materials, 2022, 45, 1818. 25 Shiozawa K, Morii Y, Nishino S, et al. International Journal of Fatigue, 2006, 28, 1521. 26 Zhao Y, Gong B, Liu Y, et al. International Journal of Fatigue, 2024, 178, 107993. 27 Zhao X, Xue G, Liu Y, et al. Resultsin Physics, 2017, 7, 1845. 28 Xu C, Liang Y, Yang M, et al. Materials, 2021, 14, 2565. 29 Hyde J M, Sandiford R D. International Journal of Pressure Vessels and Piping, 2007, 84(3), 123. 30 Wang K, Tao N R, Liu G, et al. Acta Materialia, 2006, 54(19). 31 Chemkhi M, Retraint D, Roos A, et al. Surface and Coatings Technology, 2013, 221, 191. 32 Zhou J, Retraint D, Sun Z, et al. Surface and Coatings Technology, 2018, 349, 556. 33 Xu W, Liu X C, Lu K, et al. Acta Materialia, 2018, 152, 138. 34 Zhang S J, Xie J J, Jiang Q Q, et al. Materials Science & Engineering, 2017, 700, 66. 35 Wang Y, Yuan L C, Zhang S J, et al. Engineering Fracture Mechanics, 2019, 209, 369. 36 Ma Z W, Liu J B, Wang G, et al. Scientific Reports, 2016, 6, 1. 37 Chen W, You Z S, Tao N R, et al. Acta Materialia, 2017, 125, 255. 38 Sun R J, Keller S, Zhu Y, et al. International Journal of Fatigue, 2021, 145, 106081. 39 Zhang X, Zhao J F, Kang G Z, et al. International Journal of Plasticity, 2023, 163, 103553. 40 Gao X, Zhang L F, Yang M, et al. Oxidation of Metals, 2021, 96(3), 231. 41 Liu T, Wang Q, Zhang J, et al. International Journal of Fatigue, 2023, 167, 107321. 42 Xu J, Zhao Y H, Zhang M, et al. Materials Characterization, 2022, 185, 111750. 43 Long J, Pan Q, Tao N, et al. Acta Materialia, 2019, 166, 56. |
|
|
|