超声功率对多场耦合作用下脉冲电沉积Ni-ZrO<sub>2</sub>纳米复合镀层性能的影响

doi:10.11896/cldb.19020070

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Abstract As one of effective means to alleviate the nanoparticles agglomeration, ultrasonic horn was applied to the magnetic field-pulse electrodeposition apparatus, and Ni-ZrO₂ nanocomposite coatings were successfully produced under magnetic-ultrasonic fields coupling action. The aim of this study was to investigate the effects of ultrasonic power on the surface morphology, ZrO₂ content, microstructure, microhardness, wear resistance and corrosion resistance of Ni-ZrO₂ nanocomposite coating. Results showed that ZrO₂ content and microhardness in the composite prepared by no-ultrasonic magnetic field-pulse electrodeposition were 6.43wt% and 384HV, respectively. After applying ultrasonic power from 0 W up to 320 W, ZrO₂ content and microhardness increased firstly and then decreased. Under ultrasonic power of 240 W, SEM and EDS results indicated that the Ni-ZrO₂ composite coating displayed a fine and compact surface structure whereas the ZrO₂ content in composite coating was 15.2wt%, and the composite coating displayed the highest microhardness of 494HV than the other coatings. The worn surface morphology was smooth with only a few of grains worn and the Ni-ZrO₂ nanocomposite coating showed the best corrosion resistance according to the results of surface morphology and Tafel curves in 4% NaCl solution.

Key words： electrodeposition magnetic-ultrasonic fields coupling action ultrasonic Ni-ZrO₂ nanocomposite coating performance

Published: 03 January 2020

CLC number:

TQ153.1

About author:: Weiping Jia, is educated and learned at the Dalian University of Technology, and at the same time worked as a teacher in Dalian University, focusing on the research of electroplating for surface modification and electroforming micro 3D parts;Menghua Wu, Ph.D., professor, the head of the key laboratory of “Special Processing and Functional Material Preparation” in Liaoning, focusing on special processing. His research interests are the electrochemical micro machining and material modification process.

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	JIA Weiping
	WU Menghua
	JIA Zhenyuan
	DONG Guifu
	LI Xiaopeng
	ZHOU Shao’an

Cite this article:

JIA Weiping,WU Menghua,JIA Zhenyuan, et al. Effects of Ultrasonic Power on the Performance of Pulse-electrodeposited Ni-ZrO₂ Nanocomposite Coating Under Magnetic-Ultrasonic Fields Coupling Action[J]. Materials Reports, 2020, 34(2): 2017-2022.

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http://www.mater-rep.com/EN/10.11896/cldb.19020070 OR http://www.mater-rep.com/EN/Y2020/V34/I2/2017

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