静电纺β-环糊精/石墨烯载银抗菌纤维膜的制备与表征

doi:10.11896/j.issn.1005-023X.2018.04.007

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Abstract The one pot method was used to load nano Ag particle on graphene oxide nanosheets(AGCN). β-cyclodextrin/Ag-graphene composite nanosheets-based fiber membranes were synthesized by electrospinning and in situ thermal cross-linking. Scanning electron microscopy, energy spectrum, Fourier transform infrared spectra, differential scanning calorimetry and the detection of inhibition zone were used to characterize the morphology, structure and antibacterial property of fiber membranes. The results showed that thermal cross-linking did not influence cyclic structure of β-cyclodextrin. The surface of fibers with AGCN was rough, and AGCN did not participate in thermal cross-linking. Fiber membranes had good antibacterial property after the addition of AGCN. Meanwhile, the antibacterial property was improved with the increasing amount of AGCN.

Key words： electrospinining β-cyclodextrin; Ag-graphene antisepsis

Published: 25 February 2018

CLC number:

TB324

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	Articles by authors
	ZHANG Xuerong
	HU Yinchun
	XI Shaohui
	WANG Zhaowei
	ZHAN Yan
	HUANG Di
	HU Chaofan
	WEI Yan

Cite this article:

ZHANG Xuerong,HU Yinchun,XI Shaohui, et al. Synthesis and Characterization of β-Cyclodextrin/Ag-graphene-based Electrospun Fiber Membranes for Antibiosis[J]. Materials Reports, 2018, 32(4): 545-548.

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http://www.mater-rep.com/EN/10.11896/j.issn.1005-023X.2018.04.007 OR http://www.mater-rep.com/EN/Y2018/V32/I4/545

1 Stephen M, Catherine N, Brenda M, et al. Oxolane-2,5-dione modified electrospun cellulose nanofibers for heavy metals adsorption[J].Journal of Hazardous Materials,2011,192(2):922.
2 Pirzada T, Arvidson S A, Saquing C D, et al. Hybrid silica-PVA nanofibers via sol-gel electrospinning[J].Langmuir,2012,28(13):5834.
3 Huang Z M, Zhang Y Z, Kotaki M, et al. A review on polymer nanofibers by electrospinning and their applications in nanocompo-sites[J].Composites Science & Technology,2003,63(15):2223.
4 Meng Depeng, Wu Juntao. Adsorption and seperation materials produced by electrospinning[J].Progress in Chemistry,2015,28(5):657(in Chinese).
孟德芃,吴俊涛.静电纺丝法制备新型吸附分离材料[J].化学进展,2015,28(5):657.
5 Agarwal S, Greiner A, Wendorff J H. Electrospinning of manmade and biopolymer nanofibers-progress in techniques, materials, and applications[J].Advanced Functional Materials,2010,19(19):2863.
6 Yuan W, Zhang K Q. Structural evolution of electrospun composite fibers from the blend of polyvinyl alcohol and polymer nanoparticles[J].Langmuir,2012,28(43):15418.
7 Wen Qian. Preparation and characterization of β-cyclodextrin nanocomposite materials[D].Changchun: Jilin University,2014(in Chinese).
文茜.β-环糊精纳米复合材料的制备及其性能研究[D].长春:吉林大学,2014.
8 Szejtli J, Szente L. Elimination of bitter, disgusting tastes of drugs and foods by cyclodextrins[J].European Journal of Pharmaceutics & Biopharmaceutics Official Journal of Arbeitsgemeinschaft Fur Pharmazeutische Verfahrenstechnik E V,2005,61(3):115.
9 Bae J R. Ultrasonic relaxation for complexation reaction between β-cyclodextrin and butanoic acid in aqueous solution[J].Journal of the Acoustical Society of Korea,2012,31(2):100.
10 Prabaharan M, Mano J F. Chitosan derivatives bearing cyclodextrin cavitiesas novel adsorbent matrices[J].Carbohydrate Polymers,2006,63(2):153.
11 Zhao R, Wang Y, Li X, et al. Synthesis of beta-cyclodextrin-based electrospun nanofiber membranes for highly efficient adsorption and separation of methylene blue[J].ACS Applied Materials & Interfaces,2015,7(48):26649.
12 Liu Chuochuo. Preparation and antibacterial property of polyethersulfone hybrid ultrafiltration membranes containing immobolized lyzosyme[D].Zhengzhou:Zhengzhou University,2014(in Chinese).
刘绰绰.负载溶菌酶的聚醚砜杂化超滤膜制备及其抗菌性能研究[D].郑州:郑州大学,2014.
13 Kang G D, Cao Y M. Development of antifouling reverse osmosis membranes for water treatment:A review[J].Water Research,2012,46(3):584.
14 Texter J. Graphene oxide and graphene flakes as stabilizers and dispersing aids[J].Current Opinion in Colloid & Interface Science,2015,20(5-6):454.
15 Tang C, Saquing D, Harding J R, et al. In situ cross-linking of electrospun poly(vinyl alcohol) nanofibers[J].Macromolecules,2010,43(2):630.
16 Zhang Z, Xu F, Yang W, et al. A facile one-pot method to high-quality Ag-graphene composite nanosheets for efficient surface-enhanced Raman scattering[J].Chemical Communications,2011,47(22):6440.
17 GBT 20944.1-2007纺织品抗菌性能的评价第1部分:琼脂扩散法[S].北京:中国标准出版社,2007.
18 Li L, Hsieh YL. Ultra-fine polyelectrolyte fibers from electrospinning of poly(acrylic acid)[J].Polymer,2005,46(14):5133.
19 Qin Jing. Preparation of graphene oxide nano-composite membrane and study on its anti-biofouling property[D].Jinan:Shandong University,2015(in Chinese).
秦静.氧化石墨烯纳米复合膜的制备及抗污染性能研究[D].济南:山东大学,2015.
20 Liu S, Hu M, Zeng T H, et al. Lateral dimension-dependent antibacterial activity of graphene oxide sheets[J].Langmuir,2012,28(33):12364.
21 Marambio-Jones C, Hoek E M V. A review of the antibacterial effects of silver nanomaterials and potential implications for human health and the environment[J].Journal of Nanoparticle Research,2010,12(5):1531.