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《材料导报》期刊社  2017, Vol. 31 Issue (2): 46-50    https://doi.org/10.11896/j.issn.1005-023X.2017.02.010
  材料研究 |
Fe+注入增强Ti6Al4V表面喷丸强化层的生物摩擦学性能*
郑宇1, 王远1, 于晓华2
1 西南林业大学机械与交通学院, 昆明 650224;
2 昆明理工大学固体废弃物资源化国家工程研究中心, 昆明 650093;
Bio-tribological Properties of Shot-peened Layers on Ti6Al4V Improved by Fe+ Implantation
ZHENG Yu1, WANG Yuan1, YU Xiaohua2
1 Faculty of Machinery and Transaction, Southwest Forestry University, Kunming 650224;
2 School of Materials Science and Engineering, Kunming University of Science and Technology, Kunming 650093;
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摘要 为改善Ti6Al4V表面喷丸强化层的生物摩擦学性能,把不同参数Fe+注入到直径4 mm喷丸的强化层中。用Nano Indenter Ⅱ型纳米显微力学探针测定试样改性层的纳米硬度,在MRTR多功能摩擦磨损试验机上以ZrO2球/改性层为摩擦副进行人工唾液和透明质酸钠溶液润滑下的生物摩擦学试验,使用S-3000N扫描电子显微镜分析改性层组织形貌和生物摩擦学试验后的磨痕形貌。结果表明:Fe+注入Ti6Al4V表面喷丸强化层的形成相为Fe2Ti。随着注入能量和剂量增加,Fe2Ti含量从3.7%增至4.7%;Fe+注入改性层的纳米硬度从8.46 GPa增至10.29 GPa,都远高于单一喷丸强化层的5.59 GPa;在人工唾液和透明质酸钠溶液润滑下的摩擦因数分别从0.53降至0.38和从0.49降至0.28,都低于单一喷丸强化层的0.62和0.59,磨损呈现不同程度的减轻。Fe+注入能显著提高Ti6Al4V表面单一喷丸强化层的减摩抗磨性能。
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郑宇
王远
于晓华
关键词:  Ti6Al4V  Fe+注入  喷丸强化  生物摩擦学  人工唾液  透明质酸钠溶液    
Abstract: Fe+ with different energies and doses were implanted into shot-peened layers (the diameter of shot peen was 4 mm) on Ti6Al4V to improve the bio-tribological properties. The nano-hardness of modified layers was measured by Nano Indenter Ⅱ and bio-tribological tests were performed on MRTR multifunctional machine with artificial saliva and sodium hyaluronate as lubricants. The friction pairs used in the bio-tribological test were ZrO2 ball/modified layers on Ti6Al4V. S-3000N SEM was used to observe the surface microstructures and grinding cracks. The results demonstrated that the formed phases in the shot-peened layers on Ti6Al4V by Fe+ implantation were Fe2Ti. With the increase of ion energies and doses, the content of Fe2Ti increased from 3.7% to 4.7%; the nano-hardness of modified layers on Ti6Al4V by Fe+ implantation increased from 8.46 GPa to 10.29 GPa, which were much higher than the ones with value 5.59 GPa of the single shot-peened layer; the friction coefficient of modified layers with Fe+ implantation decreased from 0.53 to 0.38 and from 0.49 to 0.28 under artificial saliva and sodium hyaluronate, which were lower than ones with value 0.62 and 0.59 of the single shot-peened layer, respectively, and the wear loss of Fe+ implantation layers reduced to varying degrees. We can inferred that Fe+ implantation obviously improves friction and wear resistance of the single shot-peened layer on Ti6Al4V surface.
Key words:  Ti6Al4V    Fe+ implantation    shot-peening    bio-tribology    artificial saliva    sodium hyaluronate
               出版日期:  2017-01-25      发布日期:  2018-05-02
ZTFLH:  TG178.1  
基金资助: *国家自然科学基金(51301144);云南省教育厅卓越青年教师特殊培养项目(51400672)
作者简介:  郑宇:男,1990年生,硕士研究生,主要从事钛合金表面改性研究 E-mail:zhengyu9097@163.com 王远:通讯作者,男,1978年生,博士,副教授,主要从事金属材料表面改性及非晶合金材料的研究 E-mail:wyuan88@126.com 于晓华:通讯作者,男,1986年生,博士,讲师,主要从事材料热力学及纳米材料尺寸效应的研究 E-mail:xiaohua_y@163.com
引用本文:    
郑宇, 王远, 于晓华. Fe+注入增强Ti6Al4V表面喷丸强化层的生物摩擦学性能*[J]. 《材料导报》期刊社, 2017, 31(2): 46-50.
ZHENG Yu, WANG Yuan, YU Xiaohua. Bio-tribological Properties of Shot-peened Layers on Ti6Al4V Improved by Fe+ Implantation. Materials Reports, 2017, 31(2): 46-50.
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http://www.mater-rep.com/CN/10.11896/j.issn.1005-023X.2017.02.010  或          http://www.mater-rep.com/CN/Y2017/V31/I2/46
1 Tessier P Y, Pichon L, Villechaise P, et al. Carbon nitride thin films as protective coatings for biomaterials: Synthesis, mechanical and biocompatibility characterizations[J]. Diamond Related Mater,2003,12(3-7):1066.
2 Habibovic P, Li J P. Biological performance of uncoated and octacalcium phosphate-coated Ti6A14V[J]. Biomaterials,2005,26(1):23.
3 Wang Changxiang, Zheng Changqiong, Ran Junguo. Materials for joint replacement and friction and wear[J]. J Biomed Eng,1997,14(1):64(in Chinese).
王昌祥,郑昌琼,冉均国. 关节置换材料及摩擦磨损[J]. 生物医学工程学杂志,1997,14(1):64.
4 Chakpavarty S, Dyer J P, Conway J C. Influence of surface treatments on fretting of Ti6242 at elevated temperature [R]. ASTM STP1367. West Conshohochen: American Society for Testing and Materials,2000:491.
5 Xue L, Koul A K, Bibby M. A survey of surface treatments to improve the fretting fatigue resistance of Ti6Al4V [C]//Proc of Conf on Computer Methods and Experimental Measurement for Surface Treatment Effect. Milan:Computational Mechanics Pub,1995:265.
6 Yang H C, Zhang S R, Yu D B, et al. Corrosion resistance and magnetostrictive properties of (Tb0.3Dy0.7)Fe2 alloy modified by nitrogen ion implantation[J]. J Rare Earths,2015,33:629.
7 Mohamed Abdel, Hady Gepreel, Mitsuo Niinomi. Biocompatibility of Ti alloys for long-term implantation[J]. J Mech Behav Biomed Mater,2013,20:407.
8 Gao Yukui. Effect of shot-Peening on microstructure of TC4 tita-nium alloy[J].Rare Met Mater Eng,2010,39(9):1536(in Chinese).
高玉魁. 喷丸强化对TC4钛合金组织结构的影响[J].稀有金属材料与工程,2010,39(9):1536.
9 Wang Min, Lin Chengxiao, Ma Caixia. Mechanism of surface nano-crystallization of Ti6Al4V Alloy[J].Chin J Rare Met,2011,35(5):633(in Chinese).
王敏,蔺成效,马彩霞.Ti6A14V钛合金表面纳米化机制研究[J].稀有金属,2011,35(5):633.
10 Sokol D W, Clauer A H. Applications of laser peening to titanium alloys[C ]//ASME/JSME 2004 Pressure Vessels and Piping Division Conference.San Diego,CA,2004:25.
11 Lin Wanming, Wei Yinghui, Du Huayun, et al. Influence of surface nanocrystalline of copper on Ti ions implantation[J]. J Funct Mater,2009(9):1552(in Chinese).
林万明,卫英慧,杜华云,等. 纯铜表面纳米化对Ti离子注入的影响[J]. 功能材料,2009(9):1552.
12 Xiong Dangsheng. Improve wear resistance of UHMWPE by O+ ion implanted[J]. J Biomed Eng,2003,20(4):583(in Chinese).
熊党生.氧离子注入增强人工关节软骨材料-UHMWPE的耐磨性[J].生物医学工程学杂志,2003,20(4):583.
13 Zhang Tonghe, Wu Yuguang, Liu Andong, ea al. Formation of nanostructure and its properties by metal ion implantation[J]. J Beijing Normal University,2002,38(5):620(in Chinese).
张通和,吴瑜光,刘安东,等. 金属离子注入纳米结构和特性[J].北京师范大学学报,2002,38(5):620.
14 Li Hengde, Wang Honghong, Zhang Xiaozhong, et al. Some experimental studies on metal ion implantation and ion beam mixing[J].Chin J Vacuum Sci Technol,1983(5):357(in Chinese).
李恒德,汪泓宏,张效忠,等. 离子注入和离子束混合金属表面改性的某些研究[J]. 真空科学与技术,1983(5):357.
15 王成焘. 人体生物摩擦学[M].北京:科学出版社,2008.
16 Chen Guoqing, Tian Tangyong, Zhang Xinhua, et al. Microstructure and fatigue properties of Ti6Al4V titanium alloy treated by wet shot peening of ceramic beads[J]. Chin J Nonferrous Met,2013,23(1):122(in Chinese).
陈国清,田唐永,张新华,等.Ti6Al4V钛合金陶瓷湿喷丸表面强化微观组织与疲劳性能[J]. 中国有色金属学报,2013,23(1):122.
17 Helmut W. Residual stress and stress relaxation [C]//Weiss V. Sagamore Army Materials Research Conference Proceedings. New York: Springer Publishing Company,1981:71.
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