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《材料导报》期刊社  2018, Vol. 32 Issue (13): 2202-2207    https://doi.org/10.11896/j.issn.1005-023X.2018.13.010
  无机非金属及其复合材料 |
脉冲电子束作用下热障涂层微观结构及热循环性能
吴健1, 关庆丰1, 蔡杰2,3, 吕鹏1, 张从林1, 李晨1
1 江苏大学材料科学与工程学院,镇江 212013;
2 江苏大学先进制造与现代装备技术工程研究院,镇江 212013;
3 江苏大学机械工程学院,镇江 212013
Microstructure and Thermal Cycling Behavior of the Surface-modified Thermal Barrier Coatings by High-current Pulsed Electron Beam
WU Jian1, GUAN Qingfeng1, CAI Jie2,3, LYU Peng1, ZHANG Conglin1, LI Chen1
1 School of Materials Science and Engineering, Jiangsu University, Zhenjiang 212013;
2 Institute of AdvancedManufacturing and Modern Equipment Technical, Jiangsu University, Zhenjiang 212013;
3 School of Mechanical Engineering, Jiangsu University, Zhenjiang 212013
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摘要 利用强流脉冲电子束 (HCPEB) 技术对大气等离子喷涂 (APS) 技术制备的热障涂层 (TBCs) 进行表面处理,探究HCPEB辐照对TBCs微观结构以及热循环性能的影响。热循环实验采用950 ℃炉温加热并随后水淬。采用X射线衍射,扫描电子显微镜详细分析了辐照前后涂层表面微观结构及相组成。X射线分析结果表明,HCPEB辐照后陶瓷层中单斜相m相含量降低;此外,衍射峰发生宽化及偏移说明伴随有晶粒细化以及残余应力产生。微观结构观察表明,HCPEB辐照后热喷涂缺陷消失,涂层发生重熔,涂层表面粗糙度降低,且重熔层内部有网状垂直微裂纹以及柱状晶产生。热循环实验表明,250次热循环后原始涂层发生整体剥落,涂层失效;而HCPEB辐照后涂层并未出现明显的剥落迹象,仅存在水平裂纹的扩展,涂层的热循环寿命明显提高。
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吴健
关庆丰
蔡杰
吕鹏
张从林
李晨
关键词:  YSZ陶瓷层  强流脉冲电子束  微观结构  热循环性能    
Abstract: High-current pulsed electron beam (HCPEB) treatment was conducted on thermal barrier coatings (TBCs) prepared by air plasma sprayed (APS) technology. The effects of HCPEB irradiation on the microstructure and thermal cycling behavior of TBCs were investigated. The thermal cycling test was carried out by using a muffle furnace, and each cycle consisted of holding at 950 ℃ in air and cooling by water quenching. The microstructure and phase composition of the coatings before and after HCPEB irradiation were characterized by scanning electron microscopy (SEM) and X-ray diffraction (XRD).The XRD results revealed that the content of monoclinic (m) phase in the yttria stabilized zirconia (YSZ) topcoat was reduced after HCPEB irradiation. Besides, the width of peaks became wider and peak locations slightly shifted, which indicated the grain refinement and residual stress generation. The remelting of the coating surface, the elimination of thermal sprayed defects, the reduced surface roughness, as well as a conti-nuous micro-crack network perpendicular to the surface and columnar grains in the remelted layer, could be observed by SEM for the HCPEB irradiated YSZ topcoat. Thermal cycling test results confirmed the failure of the initial YSZ coating after 250 cycles, as the overall spalling occurred. Contrastively, no obvious signs of spallation appeared for the irradiated coating, and only the propagation of horizontal cracks can be observed. Our experiment validated the higher thermal cycling resistance of the HCPEB-TBCs.
Key words:  YSZ topcoat    high-current pulsed electron beam (HCPEB)    microstructure    thermal cycling behavior
               出版日期:  2018-07-10      发布日期:  2018-08-01
ZTFLH:  TB321  
基金资助: 国家自然科学基金(51601072;U1233111);江苏省自然科学基金青年基金(BK20160530);中国博士后科学基金 (2016M601730);江苏省博士后基金(1601007C);江苏大学高级人才科研启动基金 (15JDG149);江苏大学青年英才培育计划
通讯作者:  蔡杰:通信作者,女,1987年生,助理研究员,主要研究方向为表面改性 E-mail:caijie@ujs.edu.cn   
作者简介:  吴健:男,1992年生,硕士研究生,主要研究方向为表面改性 E-mail:chriswinner@foxmail.com
引用本文:    
吴健, 关庆丰, 蔡杰, 吕鹏, 张从林, 李晨. 脉冲电子束作用下热障涂层微观结构及热循环性能[J]. 《材料导报》期刊社, 2018, 32(13): 2202-2207.
WU Jian, GUAN Qingfeng, CAI Jie, LYU Peng, ZHANG Conglin, LI Chen. Microstructure and Thermal Cycling Behavior of the Surface-modified Thermal Barrier Coatings by High-current Pulsed Electron Beam. Materials Reports, 2018, 32(13): 2202-2207.
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http://www.mater-rep.com/CN/10.11896/j.issn.1005-023X.2018.13.010  或          http://www.mater-rep.com/CN/Y2018/V32/I13/2202
1 Peters M, Fritscher K, Staniek G, et al. Design and properties of thermal barrier coatings for advanced turbine engines[J].Materialwissenschaft Und Werkstofftechnik,1997,28(8):357.
2 Wang Q W, Mao W G, Yu M. Analysis of heat-insulating perfor-mance of air plasma sprayed thermal barrier coating systems[J].Materials Review B:Research Papers,2011,25(9):125(in Chinese).
王千文,毛卫国,喻明.等离子喷涂热障涂层隔热性能分析方法[J].材料导报:研究篇,2011,25(9):125.
3 Padture N P, Gell M, Jordan E H. Thermal barrier coatings for gas-turbine engine applications[J].Science,2002,296(5566):280.
4 Stecura S. New ZrO2-Y2O3 plasma-sprayed coatings for thermal barrier applications[J].Thin Solid Films,1987,150(1):15.
5 Cai J, Guan Q F, Yang S Z, et al. Microstructural characterization of modified YSZ thermal barrier coatings by high-current pulsed electron beam[J].Surface & Coatings Technology,2014,254(18):187.
6 Gong W B, Sha C K, Sun D Q, et al. Microstructures and thermal insulation capability of plasma-sprayed nanostructured ceria stabilized zirconia coatings[J].Surface & Coatings Technology,2006,201(6):3109.
7 Drexler J M, Shinoda K, Ortiz A L, et al. Air-plasma-sprayed thermal ba-rrier coatings that are resistant to high-temperature attack by glassy deposits[J].Acta Materialia,2010,58(20):6835.
8 Rabiei A, Evans A G. Failure mechanisms associated with the thermally grown oxide in plasma-sprayed thermal barrier coatings[J].Acta Materialia,2000,48(15):3963.
9 Liu D X, Chen R H. Current status and development direction of aircraft power technology in the world[J].Journal of Beijing University of Aeronautics and Astronautics,2002,28(5):490(in Chinese).
刘大响,程荣辉.世界航空动力技术的现状及发展动向[J].北京航空航天大学学报,2002,28(5):490.
10 Ghasemi R, Shoja-Razavi R, Mozafarinia R, et al. The influence of laser treatment on thermal shock resistance of plasma-sprayed nanostructured yttria stabilized zirconia thermal barrier coatings[J].Ceramics International,2014,34(8):347.
11 Ahmadi-Pidani R, Shoja-Razavi R, Mozafarinia R, et al. Improving the thermal shock resistance of plasma sprayed CYSZ thermal bar-rier coatings by laser surface modification[J].Optics and Lasers in Engineering,2012,50(5):780.
12 Batista C, Portinha A, Ribeiro R M, et al. Morphological and microstructural characterization of laser-glazed plasma-sprayed thermal barrier coatings[J].Surface & Coatings Technology,2006,200(9):2929.
13 Grosdidier T, Zou J X, Bolle B, et al. Grain refinement, hardening and metastable phase formation by high current pulsed electron beam (HCPEB) treatment under heating and melting modes[J].Journal of Alloys and Compounds,2010,504(8):S508.
14 Cai J, Lv P, Guan Q F, et al. Thermal cycling behavior of thermal barrier coatings with MCrAlY bond coat irradiated by high-current pulsed electron beam[J].ACS Applied Materials & Interfaces,2016,8(47):32541.
15 Moon J, Choi H, Kim Y, et al. Cooling rate effect on phase transformation of plasma sprayed partially stabilized zirconia[J].Journal of Materials Science Letters,2001,20(17): 1611.
16 Zhu C, Li P, Javed A, et al. An investigation on the microstructure and oxidation behavior of laser remelted air plasma sprayed thermal barrier coatings[J].Surface & Coatings Technology,2012,206(18):3739.
17 Kim B K, Hahn J W, Han K R. Quantitative phase analysis in tetragonal-rich tetragonal/monoclinic two phase zirconia by raman spectroscopy[J].Journal of Materials Science Letters,1997,16(8):669.
18 Lima R S, Kucuk A, Berndt C C. Integrity of nanostructured partially stabilized zirconia after plasma spray processing[J].Materials Science and Engineering A,2001,313(1-2):75.
19 Cai J, Ji L, Yang S Z, et al. Deformation mechanism and microstructures on polycrystalline aluminum induced by high-current pulsed electron beam[J].Chinese Science Bulletin,2013,58(20):2507.
20 Wang C X. Surface modification of coating irradiation by high current plulsed electrom beam[D].Dalian:Dalian University of Technology,2011(in Chinese).
王存霞.强流脉冲电子束辐照陶瓷涂层表面改性[D].大连:大连理工大学,2011.
21 Cai J, Ji L, Yang S Z, et al. Surface microstructure and stress cha-racteristics inpure zirconium after high current pulsed electron beam irradiation[J].Acta Physica Sinica,2013,62(15):328(in Chinese).
蔡杰,季乐,杨盛志,等.强流脉冲电子束作用下金属锆的微观结构与应力状态[J].物理学报,2013,62(15):328.
22 Mou R D, Lu F, He L M, et al. Application and development of thermal barrier coating technology in aeroengine[J].Thermal Spray Technology,2009,1(1):53(in Chinese).
牟仁德,陆峰,何利民,等.热障涂层技术在航空发动机上的应用与发展[J].热喷涂技术,2009,1(1):53.
23 Zhang H S, Geng G Q, Du K K, et al. Application of thermal spraying and electron beam physical vapor deposition in preparation of thermal barrier coatings[J].Materials Review A:Review Papers,2009,23(7):98(in Chinese).
张红松,耿国强,杜可可,等.热喷涂及电子束物理气相沉积技术在热障涂层制备中的应用[J].材料导报:综述篇,2009,23(7):98.
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